Relationship between the properties of an interlayer formed by in situ Ti anodization and anaphoretically deposited hydroxyapatite
Authors
Pantović Pavlović, Marijana R.Pavlović, Miroslav M.
Eraković, Sanja
Barudžija, Tanja
Stevanović, Jasmina S.
Ignjatović, Nenad L.
Panić, Vladimir V.
Article (Published version)
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The optimization of the anodization process of Ti substrate for in situ synthesis of hydroxyapatite/titanium oxide composite coatings on titanium substrate was accomplished. The anodization was performed under 30, 60 and 90 V cell voltage, and the morphology of treated surface, as well as linear and surface roughness, were analysed by field emission-scanning electron microscopy, atomic force microscopy and roughness tester. It was shown by linear and surface roughness analyses that titanium anodized under 60 V has the highest roughness, whereas at 90 V the flattening of the surface occurs. As the highest surface roughness results emerged at 60 V, the novel process of composite anHAp/TiO2 coating synthesis, which comprises simultaneous processes of TiO2 formation and HAp deposition, as well as HAp impregnation within TiO2 surface layer, was performed at this voltage. Ti substrate surface was completely covered by composite coating, with no visible cracks. The adhesion quantified acc...ording to ASTM D3359-02 standard is considerably improved with respect to the coatings obtained by cathaphoretic processes, with no need of subsequent sintering.
Keywords:
adhesion / hyd-roxyapatite coating / in situ anaphoretic deposition / roughness / titanium anodization / titanium oxideSource:
Journal of the Serbian Chemical Society, 2019, 84, 11, 1305-1318Funding / projects:
- New approach in designing materials for energy conversion and energy storage systems (RS-MESTD-Basic Research (BR or ON)-172060)
DOI: 10.2298/JSC190730105P
ISSN: 1820-7421
WoS: 000500748300010
Scopus: 2-s2.0-85076257517
URI
https://www.shd-pub.org.rs/index.php/JSCS/article/view/8524https://vinar.vin.bg.ac.rs/handle/123456789/8671
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VinčaTY - JOUR AU - Pantović Pavlović, Marijana R. AU - Pavlović, Miroslav M. AU - Eraković, Sanja AU - Barudžija, Tanja AU - Stevanović, Jasmina S. AU - Ignjatović, Nenad L. AU - Panić, Vladimir V. PY - 2019 UR - https://www.shd-pub.org.rs/index.php/JSCS/article/view/8524 UR - https://vinar.vin.bg.ac.rs/handle/123456789/8671 AB - The optimization of the anodization process of Ti substrate for in situ synthesis of hydroxyapatite/titanium oxide composite coatings on titanium substrate was accomplished. The anodization was performed under 30, 60 and 90 V cell voltage, and the morphology of treated surface, as well as linear and surface roughness, were analysed by field emission-scanning electron microscopy, atomic force microscopy and roughness tester. It was shown by linear and surface roughness analyses that titanium anodized under 60 V has the highest roughness, whereas at 90 V the flattening of the surface occurs. As the highest surface roughness results emerged at 60 V, the novel process of composite anHAp/TiO2 coating synthesis, which comprises simultaneous processes of TiO2 formation and HAp deposition, as well as HAp impregnation within TiO2 surface layer, was performed at this voltage. Ti substrate surface was completely covered by composite coating, with no visible cracks. The adhesion quantified according to ASTM D3359-02 standard is considerably improved with respect to the coatings obtained by cathaphoretic processes, with no need of subsequent sintering. T2 - Journal of the Serbian Chemical Society T1 - Relationship between the properties of an interlayer formed by in situ Ti anodization and anaphoretically deposited hydroxyapatite VL - 84 IS - 11 SP - 1305 EP - 1318 DO - 10.2298/JSC190730105P ER -
@article{ author = "Pantović Pavlović, Marijana R. and Pavlović, Miroslav M. and Eraković, Sanja and Barudžija, Tanja and Stevanović, Jasmina S. and Ignjatović, Nenad L. and Panić, Vladimir V.", year = "2019", abstract = "The optimization of the anodization process of Ti substrate for in situ synthesis of hydroxyapatite/titanium oxide composite coatings on titanium substrate was accomplished. The anodization was performed under 30, 60 and 90 V cell voltage, and the morphology of treated surface, as well as linear and surface roughness, were analysed by field emission-scanning electron microscopy, atomic force microscopy and roughness tester. It was shown by linear and surface roughness analyses that titanium anodized under 60 V has the highest roughness, whereas at 90 V the flattening of the surface occurs. As the highest surface roughness results emerged at 60 V, the novel process of composite anHAp/TiO2 coating synthesis, which comprises simultaneous processes of TiO2 formation and HAp deposition, as well as HAp impregnation within TiO2 surface layer, was performed at this voltage. Ti substrate surface was completely covered by composite coating, with no visible cracks. The adhesion quantified according to ASTM D3359-02 standard is considerably improved with respect to the coatings obtained by cathaphoretic processes, with no need of subsequent sintering.", journal = "Journal of the Serbian Chemical Society", title = "Relationship between the properties of an interlayer formed by in situ Ti anodization and anaphoretically deposited hydroxyapatite", volume = "84", number = "11", pages = "1305-1318", doi = "10.2298/JSC190730105P" }
Pantović Pavlović, M. R., Pavlović, M. M., Eraković, S., Barudžija, T., Stevanović, J. S., Ignjatović, N. L.,& Panić, V. V.. (2019). Relationship between the properties of an interlayer formed by in situ Ti anodization and anaphoretically deposited hydroxyapatite. in Journal of the Serbian Chemical Society, 84(11), 1305-1318. https://doi.org/10.2298/JSC190730105P
Pantović Pavlović MR, Pavlović MM, Eraković S, Barudžija T, Stevanović JS, Ignjatović NL, Panić VV. Relationship between the properties of an interlayer formed by in situ Ti anodization and anaphoretically deposited hydroxyapatite. in Journal of the Serbian Chemical Society. 2019;84(11):1305-1318. doi:10.2298/JSC190730105P .
Pantović Pavlović, Marijana R., Pavlović, Miroslav M., Eraković, Sanja, Barudžija, Tanja, Stevanović, Jasmina S., Ignjatović, Nenad L., Panić, Vladimir V., "Relationship between the properties of an interlayer formed by in situ Ti anodization and anaphoretically deposited hydroxyapatite" in Journal of the Serbian Chemical Society, 84, no. 11 (2019):1305-1318, https://doi.org/10.2298/JSC190730105P . .