Comparison between different LiFePO4 synthesis routes
Abstract
Olivine-type lithium iron phosphate (LiFePO4) powders were synthesized applying three different methods: solid state reaction at high temperature, ultrasonic spray pyrolysis, and sonochemical treatment. The samples were characterized by X-ray powder diffraction (XRPD). Particle morphologies of the obtained powders were determined by scanning electron microscopy (SEM). It was found that structural and microstructural parameters of this material were strongly dependent on the synthesis conditions. We present here the results obtained upon optimization of each procedure for designing this cathode material.
Keywords:
cathode materials / LiFePO4 / refinement / sonochemistry / ultrasonic spray pyrolysisSource:
Materials Science Forum, 2007, 555, 225-+Funding / projects:
- Sinteza funkcionalnih materijala sa kontrolisanom strukturom na molekularnom i nano nivou (RS-MESTD-MPN2006-2010-142006)
Note:
- Research Trends in Contemporary Materials Science, 8th Conference of the Yugoslav-Materials-Research-Society (Yu-MRS), Sep 04-08, 2006, Herceg Novi, Montenegro
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Institution/Community
VinčaTY - CONF AU - Jugović, Dragana AU - Cvjetićanin, Nikola AU - Mitrić, Miodrag AU - Mentus, Slavko V. PY - 2007 UR - https://vinar.vin.bg.ac.rs/handle/123456789/6685 AB - Olivine-type lithium iron phosphate (LiFePO4) powders were synthesized applying three different methods: solid state reaction at high temperature, ultrasonic spray pyrolysis, and sonochemical treatment. The samples were characterized by X-ray powder diffraction (XRPD). Particle morphologies of the obtained powders were determined by scanning electron microscopy (SEM). It was found that structural and microstructural parameters of this material were strongly dependent on the synthesis conditions. We present here the results obtained upon optimization of each procedure for designing this cathode material. C3 - Materials Science Forum T1 - Comparison between different LiFePO4 synthesis routes VL - 555 SP - 225 EP - + DO - 10.4028/www.scientific.net/MSF.555.225 ER -
@conference{ author = "Jugović, Dragana and Cvjetićanin, Nikola and Mitrić, Miodrag and Mentus, Slavko V.", year = "2007", abstract = "Olivine-type lithium iron phosphate (LiFePO4) powders were synthesized applying three different methods: solid state reaction at high temperature, ultrasonic spray pyrolysis, and sonochemical treatment. The samples were characterized by X-ray powder diffraction (XRPD). Particle morphologies of the obtained powders were determined by scanning electron microscopy (SEM). It was found that structural and microstructural parameters of this material were strongly dependent on the synthesis conditions. We present here the results obtained upon optimization of each procedure for designing this cathode material.", journal = "Materials Science Forum", title = "Comparison between different LiFePO4 synthesis routes", volume = "555", pages = "225-+", doi = "10.4028/www.scientific.net/MSF.555.225" }
Jugović, D., Cvjetićanin, N., Mitrić, M.,& Mentus, S. V.. (2007). Comparison between different LiFePO4 synthesis routes. in Materials Science Forum, 555, 225-+. https://doi.org/10.4028/www.scientific.net/MSF.555.225
Jugović D, Cvjetićanin N, Mitrić M, Mentus SV. Comparison between different LiFePO4 synthesis routes. in Materials Science Forum. 2007;555:225-+. doi:10.4028/www.scientific.net/MSF.555.225 .
Jugović, Dragana, Cvjetićanin, Nikola, Mitrić, Miodrag, Mentus, Slavko V., "Comparison between different LiFePO4 synthesis routes" in Materials Science Forum, 555 (2007):225-+, https://doi.org/10.4028/www.scientific.net/MSF.555.225 . .