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dc.creatorMaletaškić, Jelena
dc.creatorTodorović, Bratislav
dc.creatorGilić, Martina
dc.creatorMarinović-Cincović, Milena
dc.creatorYoshida, Katsumi
dc.creatorGubarevich, Anna
dc.creatorMatović, Branko
dc.date.accessioned2021-02-24T07:45:43Z
dc.date.available2021-02-24T07:45:43Z
dc.date.issued2020
dc.identifier.issn0350-820X
dc.identifier.urihttps://vinar.vin.bg.ac.rs/handle/123456789/8983
dc.description.abstractSphene based glass-ceramics (CaTiSiO5), an excellent candidate for a host lattice of ceramic materials and for nuclear waste immobilization, has been prepared from a powder mixture of CaCO3, TiO2 and SiO2 using vibro-milling for homogenization. Starting powders were melted at 1400?C for 2 h, cooled to room temperature, grounded again, then crystallized by thermal treatment yielding a sphene glass-ceramic. The evolution of the phase composition during thermal treatment was investigated by X-ray powder diffraction (XRPD), FT-IR, Raman and thermal analyses (TG-DTA). Pure synthetic single phase sphene was formed at 800?C for 4 h, even it is very hard to obtain monophase powder at such low temperature. Powder morphology was analyzed by scanning electron microscopy (SEM).en
dc.language.isoen
dc.relationinfo:eu-repo/grantAgreement/MESTD/Integrated and Interdisciplinary Research (IIR or III)/45012/RS//
dc.relationTokyo Institute of Technology, Laboratory for Advanced Nuclear Energy, Institute of Innovative Research, O-okayama, Meguro-ku, Tokyo
dc.rightsopenAccess
dc.sourceScience of Sintering
dc.subjectSpheneen
dc.subjectGlass-ceramicsen
dc.subjectMechanochemistryen
dc.subjectXRPDen
dc.subjectTG-DTAen
dc.titleSynthesis and characterization of monophase CaO-TiO2-SiO2 (sphene) based glass-ceramicsen
dc.typearticleen
dc.rights.licenseBY
dcterms.abstractYосхида, Катсуми; Матовић, Бранко; Губаревицх, Aнна; Тодоровић, Братислав; Малеташкић, Јелена; Гилић, Мартина; Мариновић-Цинцовић, Милена;
dc.rights.holder© 2020 The Author(s)
dc.citation.volume52
dc.citation.issue1
dc.citation.spage41
dc.citation.epage52
dc.identifier.wos000573635500004
dc.identifier.doi10.2298/SOS2001041M
dc.type.versionpublishedVersion
dc.identifier.scopus2-s2.0-85083979057
dc.identifier.fulltexthttp://vinar.vin.bg.ac.rs/bitstream/id/22542/0350-820X2001041M.pdf


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