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An original LIBS system based on TEA CO2 laser as a tool for determination of glass surface hardness

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Authors
Momčilović, Miloš
Živković, Sanja
Petrović, Jelena
Cvijović-Alagić, Ivana
Ciganović, Jovan
Article (Published version)
,
© 2019, Springer-Verlag GmbH Germany, part of Springer Nature
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Abstract
This study was carried out to examine the applicability of original laser-induced breakdown spectroscopy (LIBS) setup for determination of the surface hardness of lead glass as a function of its chemical composition. For this purpose, a set of five lead glass samples with different amount of ZrO2 was prepared. The LIBS measurements were carried out using TEA CO2 laser in the air at atmospheric pressure and without sample preparation. A ratio of the intensity between the Zr(II) 355.66 nm and Zr(I) 360.12 nm emission lines has been used to examine the hardness of the material. In addition, the surface hardness of glass samples was determined by Vickers’s indentation tests. Obtained results indicate a linear relationship of the measurements of hardness in glass samples between the LIBS and Vickers method. To show that LIBS based on TEA CO2 laser is an almost nondestructive technique, profilometric surface analysis was used. The proposed LIBS system is suitable not only for a spectrochemic...al analysis but also as an easy to use and cost-effective way to measure the surface hardness for all types and shapes of glass samples which are in some cases difficult to examine by standard Vicker’s method. © 2019, Springer-Verlag GmbH Germany, part of Springer Nature.

Source:
Applied Physics B, 2019, 125, 11, 222-
Funding / projects:
  • Effects of laser radiation and plasma on novel materials in their synthesis, modification, and analysis (RS-172019)
  • Micromechanical criteria of damage and fracture (RS-174004)

DOI: 10.1007/s00340-019-7329-2

ISSN: 0946-2171

WoS: 000493772600001

Scopus: 2-s2.0-85074277507
[ Google Scholar ]
4
4
URI
https://vinar.vin.bg.ac.rs/handle/123456789/8620
Collections
  • Radovi istraživača
Institution/Community
Vinča
TY  - JOUR
AU  - Momčilović, Miloš
AU  - Živković, Sanja
AU  - Petrović, Jelena
AU  - Cvijović-Alagić, Ivana
AU  - Ciganović, Jovan
PY  - 2019
UR  - https://vinar.vin.bg.ac.rs/handle/123456789/8620
AB  - This study was carried out to examine the applicability of original laser-induced breakdown spectroscopy (LIBS) setup for determination of the surface hardness of lead glass as a function of its chemical composition. For this purpose, a set of five lead glass samples with different amount of ZrO2 was prepared. The LIBS measurements were carried out using TEA CO2 laser in the air at atmospheric pressure and without sample preparation. A ratio of the intensity between the Zr(II) 355.66 nm and Zr(I) 360.12 nm emission lines has been used to examine the hardness of the material. In addition, the surface hardness of glass samples was determined by Vickers’s indentation tests. Obtained results indicate a linear relationship of the measurements of hardness in glass samples between the LIBS and Vickers method. To show that LIBS based on TEA CO2 laser is an almost nondestructive technique, profilometric surface analysis was used. The proposed LIBS system is suitable not only for a spectrochemical analysis but also as an easy to use and cost-effective way to measure the surface hardness for all types and shapes of glass samples which are in some cases difficult to examine by standard Vicker’s method. © 2019, Springer-Verlag GmbH Germany, part of Springer Nature.
T2  - Applied Physics B
T1  - An original LIBS system based on TEA CO2 laser as a tool for determination of glass surface hardness
VL  - 125
IS  - 11
SP  - 222
DO  - 10.1007/s00340-019-7329-2
ER  - 
@article{
author = "Momčilović, Miloš and Živković, Sanja and Petrović, Jelena and Cvijović-Alagić, Ivana and Ciganović, Jovan",
year = "2019",
abstract = "This study was carried out to examine the applicability of original laser-induced breakdown spectroscopy (LIBS) setup for determination of the surface hardness of lead glass as a function of its chemical composition. For this purpose, a set of five lead glass samples with different amount of ZrO2 was prepared. The LIBS measurements were carried out using TEA CO2 laser in the air at atmospheric pressure and without sample preparation. A ratio of the intensity between the Zr(II) 355.66 nm and Zr(I) 360.12 nm emission lines has been used to examine the hardness of the material. In addition, the surface hardness of glass samples was determined by Vickers’s indentation tests. Obtained results indicate a linear relationship of the measurements of hardness in glass samples between the LIBS and Vickers method. To show that LIBS based on TEA CO2 laser is an almost nondestructive technique, profilometric surface analysis was used. The proposed LIBS system is suitable not only for a spectrochemical analysis but also as an easy to use and cost-effective way to measure the surface hardness for all types and shapes of glass samples which are in some cases difficult to examine by standard Vicker’s method. © 2019, Springer-Verlag GmbH Germany, part of Springer Nature.",
journal = "Applied Physics B",
title = "An original LIBS system based on TEA CO2 laser as a tool for determination of glass surface hardness",
volume = "125",
number = "11",
pages = "222",
doi = "10.1007/s00340-019-7329-2"
}
Momčilović, M., Živković, S., Petrović, J., Cvijović-Alagić, I.,& Ciganović, J.. (2019). An original LIBS system based on TEA CO2 laser as a tool for determination of glass surface hardness. in Applied Physics B, 125(11), 222.
https://doi.org/10.1007/s00340-019-7329-2
Momčilović M, Živković S, Petrović J, Cvijović-Alagić I, Ciganović J. An original LIBS system based on TEA CO2 laser as a tool for determination of glass surface hardness. in Applied Physics B. 2019;125(11):222.
doi:10.1007/s00340-019-7329-2 .
Momčilović, Miloš, Živković, Sanja, Petrović, Jelena, Cvijović-Alagić, Ivana, Ciganović, Jovan, "An original LIBS system based on TEA CO2 laser as a tool for determination of glass surface hardness" in Applied Physics B, 125, no. 11 (2019):222,
https://doi.org/10.1007/s00340-019-7329-2 . .

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