Synthesis and characterization of Co-Mo bimetallic carbides
Authors
Šaponjić, Aleksandra
Šaponjić, Đorđe

Perović, Ivana M.

Vuković, Marina

Nikolić, Vladimir M.

Marčeta Kaninski, Milica

Kokunešoski, Maja

Article (Published version)
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Co-Mo carbides were prepared by impregnation with aqueous solution of metal salts and sucrose into ordered mesoporous SBA-15 silica template using carbothermal hydrogen reduction. Bimetallic Co-Mo carbide obtained by using carbothermal hydrogen reduction of Co-Mo precursors is formed when the Co-Mo molar ratio is 1.0. The obtained samples were characterized by X-ray diffraction, scanning electron microscopy and energy dispersive X-ray analysis. Electrochemical characterization of obtained materials wеre performed by cyclic voltammetry in acid solution.
Keywords:
Co-Mo carbides / SBA-15 / Impregnation / Carbothermal-hydrogen reduction / Cyclic voltammetrySource:
Science of Sintering, 2019, 51, 3, 319-326Funding / projects:
- Synthesis, processing and characterization of nanostructured materials for application in the field of energy, mechanical engineering, environmental protection and biomedicine (RS-45012)
- Hydrogen Energy - Research and Development of New Materials: Electrolytic Hydrogen Production, Hydrogen Fuel Cells, Isotope Effects (RS-172045)
- Rational design and synthesis of biologically active and coordination compounds and functional materials, relevant for (bio)nanotechnology (RS-172035)
DOI: 10.2298/SOS1903319S
ISSN: 0350-820X
WoS: 000509869200008
Scopus: 2-s2.0-85073731520
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VinčaTY - JOUR AU - Šaponjić, Aleksandra AU - Šaponjić, Đorđe AU - Perović, Ivana M. AU - Vuković, Marina AU - Nikolić, Vladimir M. AU - Marčeta Kaninski, Milica AU - Kokunešoski, Maja PY - 2019 UR - https://vinar.vin.bg.ac.rs/handle/123456789/8598 AB - Co-Mo carbides were prepared by impregnation with aqueous solution of metal salts and sucrose into ordered mesoporous SBA-15 silica template using carbothermal hydrogen reduction. Bimetallic Co-Mo carbide obtained by using carbothermal hydrogen reduction of Co-Mo precursors is formed when the Co-Mo molar ratio is 1.0. The obtained samples were characterized by X-ray diffraction, scanning electron microscopy and energy dispersive X-ray analysis. Electrochemical characterization of obtained materials wеre performed by cyclic voltammetry in acid solution. T2 - Science of Sintering T1 - Synthesis and characterization of Co-Mo bimetallic carbides VL - 51 IS - 3 SP - 319 EP - 326 DO - 10.2298/SOS1903319S ER -
@article{ author = "Šaponjić, Aleksandra and Šaponjić, Đorđe and Perović, Ivana M. and Vuković, Marina and Nikolić, Vladimir M. and Marčeta Kaninski, Milica and Kokunešoski, Maja", year = "2019", abstract = "Co-Mo carbides were prepared by impregnation with aqueous solution of metal salts and sucrose into ordered mesoporous SBA-15 silica template using carbothermal hydrogen reduction. Bimetallic Co-Mo carbide obtained by using carbothermal hydrogen reduction of Co-Mo precursors is formed when the Co-Mo molar ratio is 1.0. The obtained samples were characterized by X-ray diffraction, scanning electron microscopy and energy dispersive X-ray analysis. Electrochemical characterization of obtained materials wеre performed by cyclic voltammetry in acid solution.", journal = "Science of Sintering", title = "Synthesis and characterization of Co-Mo bimetallic carbides", volume = "51", number = "3", pages = "319-326", doi = "10.2298/SOS1903319S" }
Šaponjić, A., Šaponjić, Đ., Perović, I. M., Vuković, M., Nikolić, V. M., Marčeta Kaninski, M.,& Kokunešoski, M.. (2019). Synthesis and characterization of Co-Mo bimetallic carbides. in Science of Sintering, 51(3), 319-326. https://doi.org/10.2298/SOS1903319S
Šaponjić A, Šaponjić Đ, Perović IM, Vuković M, Nikolić VM, Marčeta Kaninski M, Kokunešoski M. Synthesis and characterization of Co-Mo bimetallic carbides. in Science of Sintering. 2019;51(3):319-326. doi:10.2298/SOS1903319S .
Šaponjić, Aleksandra, Šaponjić, Đorđe, Perović, Ivana M., Vuković, Marina, Nikolić, Vladimir M., Marčeta Kaninski, Milica, Kokunešoski, Maja, "Synthesis and characterization of Co-Mo bimetallic carbides" in Science of Sintering, 51, no. 3 (2019):319-326, https://doi.org/10.2298/SOS1903319S . .