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Characterization of LiFePO4 samples obtained by pulse combustion under various conditions of synthesis

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Authors
Lazarević, Zorica Ž.
Križan, Gregor
Križan, Janez
Milutinović, Aleksandra N.
Ivanovski, Valentin N.
Mitrić, Miodrag
Gilić, Martina
Umićević, Ana
Kuryliszyn-Kudelska, Izabela
Romčević, Nebojša Ž.
Article (Published version)
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© 2019 Author(s)
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Abstract
Lithium iron phosphate (LiFePO4, LFP) is one of the widely used cathode materials for rechargeable lithium ion batteries. LFP batteries are widely used for electric vehicles and backup power due to their important advantages such as low cost, lifetime, efficiency, and reliability. There are still several technical challenges that need to be addressed: The increase of energy density or further reduction of their final cost. This paper concerned with the characterization of carbon coated LiFePO4 nanopowder cathode materials produced under different conditions by pulse combustion for providing energy to the reactor for the synthesis. The reactor was built according to the principles of the thermoacoustic burner on the basis of the Helmholtz resonator. The investigated nanopowders are synthesized by complete and incomplete combustion and calcined at 700 °C. The obtained samples were characterized by X-ray diffraction, Fourier transform infrared, Raman, and Mössbauer spectroscopy. Observed ...low-Temperature magnetic phase transitions definitively identified the crystal phases. The morphology of samples was controlled by scanning electron microscopy. The aim of this work is to show that it is possible to achieve a desired crystal phase by pulse combustion in a relatively cheap and fast way. The extremely rapid synthesis of almost pure phase material is possible due to the reduction in size of interacting particles and to an enormous number of collisions between them as a result of strong turbulent flow associated with explosive combustion. © 2019 Author(s).

Source:
Journal of Applied Physics, 2019, 126, 8, 085109-
Funding / projects:
  • Optoelectronics nanodimension systems - the rout towards applications (RS-45003)
  • Nanostructured multifunctional materials and nanocomposites (RS-45018)

DOI: 10.1063/1.5100358

ISSN: 0021-8979

WoS: 000483884600022

Scopus: 2-s2.0-85071522960
[ Google Scholar ]
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URI
https://vinar.vin.bg.ac.rs/handle/123456789/8501
Collections
  • Radovi istraživača
Institution/Community
Vinča
TY  - JOUR
AU  - Lazarević, Zorica Ž.
AU  - Križan, Gregor
AU  - Križan, Janez
AU  - Milutinović, Aleksandra N.
AU  - Ivanovski, Valentin N.
AU  - Mitrić, Miodrag
AU  - Gilić, Martina
AU  - Umićević, Ana
AU  - Kuryliszyn-Kudelska, Izabela
AU  - Romčević, Nebojša Ž.
PY  - 2019
UR  - https://vinar.vin.bg.ac.rs/handle/123456789/8501
AB  - Lithium iron phosphate (LiFePO4, LFP) is one of the widely used cathode materials for rechargeable lithium ion batteries. LFP batteries are widely used for electric vehicles and backup power due to their important advantages such as low cost, lifetime, efficiency, and reliability. There are still several technical challenges that need to be addressed: The increase of energy density or further reduction of their final cost. This paper concerned with the characterization of carbon coated LiFePO4 nanopowder cathode materials produced under different conditions by pulse combustion for providing energy to the reactor for the synthesis. The reactor was built according to the principles of the thermoacoustic burner on the basis of the Helmholtz resonator. The investigated nanopowders are synthesized by complete and incomplete combustion and calcined at 700 °C. The obtained samples were characterized by X-ray diffraction, Fourier transform infrared, Raman, and Mössbauer spectroscopy. Observed low-Temperature magnetic phase transitions definitively identified the crystal phases. The morphology of samples was controlled by scanning electron microscopy. The aim of this work is to show that it is possible to achieve a desired crystal phase by pulse combustion in a relatively cheap and fast way. The extremely rapid synthesis of almost pure phase material is possible due to the reduction in size of interacting particles and to an enormous number of collisions between them as a result of strong turbulent flow associated with explosive combustion. © 2019 Author(s).
T2  - Journal of Applied Physics
T1  - Characterization of LiFePO4 samples obtained by pulse combustion under various conditions of synthesis
VL  - 126
IS  - 8
SP  - 085109
DO  - 10.1063/1.5100358
ER  - 
@article{
author = "Lazarević, Zorica Ž. and Križan, Gregor and Križan, Janez and Milutinović, Aleksandra N. and Ivanovski, Valentin N. and Mitrić, Miodrag and Gilić, Martina and Umićević, Ana and Kuryliszyn-Kudelska, Izabela and Romčević, Nebojša Ž.",
year = "2019",
abstract = "Lithium iron phosphate (LiFePO4, LFP) is one of the widely used cathode materials for rechargeable lithium ion batteries. LFP batteries are widely used for electric vehicles and backup power due to their important advantages such as low cost, lifetime, efficiency, and reliability. There are still several technical challenges that need to be addressed: The increase of energy density or further reduction of their final cost. This paper concerned with the characterization of carbon coated LiFePO4 nanopowder cathode materials produced under different conditions by pulse combustion for providing energy to the reactor for the synthesis. The reactor was built according to the principles of the thermoacoustic burner on the basis of the Helmholtz resonator. The investigated nanopowders are synthesized by complete and incomplete combustion and calcined at 700 °C. The obtained samples were characterized by X-ray diffraction, Fourier transform infrared, Raman, and Mössbauer spectroscopy. Observed low-Temperature magnetic phase transitions definitively identified the crystal phases. The morphology of samples was controlled by scanning electron microscopy. The aim of this work is to show that it is possible to achieve a desired crystal phase by pulse combustion in a relatively cheap and fast way. The extremely rapid synthesis of almost pure phase material is possible due to the reduction in size of interacting particles and to an enormous number of collisions between them as a result of strong turbulent flow associated with explosive combustion. © 2019 Author(s).",
journal = "Journal of Applied Physics",
title = "Characterization of LiFePO4 samples obtained by pulse combustion under various conditions of synthesis",
volume = "126",
number = "8",
pages = "085109",
doi = "10.1063/1.5100358"
}
Lazarević, Z. Ž., Križan, G., Križan, J., Milutinović, A. N., Ivanovski, V. N., Mitrić, M., Gilić, M., Umićević, A., Kuryliszyn-Kudelska, I.,& Romčević, N. Ž.. (2019). Characterization of LiFePO4 samples obtained by pulse combustion under various conditions of synthesis. in Journal of Applied Physics, 126(8), 085109.
https://doi.org/10.1063/1.5100358
Lazarević ZŽ, Križan G, Križan J, Milutinović AN, Ivanovski VN, Mitrić M, Gilić M, Umićević A, Kuryliszyn-Kudelska I, Romčević NŽ. Characterization of LiFePO4 samples obtained by pulse combustion under various conditions of synthesis. in Journal of Applied Physics. 2019;126(8):085109.
doi:10.1063/1.5100358 .
Lazarević, Zorica Ž., Križan, Gregor, Križan, Janez, Milutinović, Aleksandra N., Ivanovski, Valentin N., Mitrić, Miodrag, Gilić, Martina, Umićević, Ana, Kuryliszyn-Kudelska, Izabela, Romčević, Nebojša Ž., "Characterization of LiFePO4 samples obtained by pulse combustion under various conditions of synthesis" in Journal of Applied Physics, 126, no. 8 (2019):085109,
https://doi.org/10.1063/1.5100358 . .

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