Hydroxyapatite/iron oxide nanocomposite prepared by high energy ball milling
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Nanocomposites (HAp/iron oxide), made of hydroxyapatite (HAp) and ferrimagnetic iron oxide, were synthesized by high-energy ball milling a mixture consisting of iron oxide nanoparticles and the starting materials used for the HAp synthesis: calcium hydrogen phosphate anhydrous (CaHPO4), and calcium hydroxide (Ca(OH)2). Two HAp/iron oxide samples with the magnetic phase content of 12 and 30 wt.% were prepared and their microstructure, morphology and magnetic properties were analysed by X-ray diffraction and transmission electron microscopy. Furthermore, the measurement of particle size distribution was performed by laser scattering, and temperature/field dependence on magnetization was determined. X-ray diffraction data confirmed the formation of two-phased samples (HAp and spinel iron oxide) without the presence of any other parasite phase. The shape of particles was nearly spherical in both samples, ranging from only a few to several tens of nanometres in diameter. These particles for...med agglomerates with the most common value of the number-based particle size distribution of 380 and 310 nm for the sample with 12 and 30 wt.% of iron oxide, respectively. Magnetization data showed that both HAp/iron oxide composites had superparamagnetic behaviour at room temperature. © 2019 University of Novi Sad, Faculty of Technology. All rights reserved.
Кључне речи:
nanocomposites / hydoxyapatite / milling / X-ray diffraction (XRD) / magnetic measurementsИзвор:
Processing and Application of Ceramics, 2019, 13, 2, 210-217Финансирање / пројекти:
DOI: 10.2298/PAC1902210V
ISSN: 1820-6131
WoS: 000475961200012
Scopus: 2-s2.0-85070695471
Институција/група
VinčaTY - JOUR AU - Vučinić-Vasić, Milica AU - Antić, Bratislav AU - Bošković, Marko AU - Antić, Aleksandar AU - Blanuša, Jovan PY - 2019 UR - https://vinar.vin.bg.ac.rs/handle/123456789/8461 AB - Nanocomposites (HAp/iron oxide), made of hydroxyapatite (HAp) and ferrimagnetic iron oxide, were synthesized by high-energy ball milling a mixture consisting of iron oxide nanoparticles and the starting materials used for the HAp synthesis: calcium hydrogen phosphate anhydrous (CaHPO4), and calcium hydroxide (Ca(OH)2). Two HAp/iron oxide samples with the magnetic phase content of 12 and 30 wt.% were prepared and their microstructure, morphology and magnetic properties were analysed by X-ray diffraction and transmission electron microscopy. Furthermore, the measurement of particle size distribution was performed by laser scattering, and temperature/field dependence on magnetization was determined. X-ray diffraction data confirmed the formation of two-phased samples (HAp and spinel iron oxide) without the presence of any other parasite phase. The shape of particles was nearly spherical in both samples, ranging from only a few to several tens of nanometres in diameter. These particles formed agglomerates with the most common value of the number-based particle size distribution of 380 and 310 nm for the sample with 12 and 30 wt.% of iron oxide, respectively. Magnetization data showed that both HAp/iron oxide composites had superparamagnetic behaviour at room temperature. © 2019 University of Novi Sad, Faculty of Technology. All rights reserved. T2 - Processing and Application of Ceramics T1 - Hydroxyapatite/iron oxide nanocomposite prepared by high energy ball milling VL - 13 IS - 2 SP - 210 EP - 217 DO - 10.2298/PAC1902210V ER -
@article{ author = "Vučinić-Vasić, Milica and Antić, Bratislav and Bošković, Marko and Antić, Aleksandar and Blanuša, Jovan", year = "2019", abstract = "Nanocomposites (HAp/iron oxide), made of hydroxyapatite (HAp) and ferrimagnetic iron oxide, were synthesized by high-energy ball milling a mixture consisting of iron oxide nanoparticles and the starting materials used for the HAp synthesis: calcium hydrogen phosphate anhydrous (CaHPO4), and calcium hydroxide (Ca(OH)2). Two HAp/iron oxide samples with the magnetic phase content of 12 and 30 wt.% were prepared and their microstructure, morphology and magnetic properties were analysed by X-ray diffraction and transmission electron microscopy. Furthermore, the measurement of particle size distribution was performed by laser scattering, and temperature/field dependence on magnetization was determined. X-ray diffraction data confirmed the formation of two-phased samples (HAp and spinel iron oxide) without the presence of any other parasite phase. The shape of particles was nearly spherical in both samples, ranging from only a few to several tens of nanometres in diameter. These particles formed agglomerates with the most common value of the number-based particle size distribution of 380 and 310 nm for the sample with 12 and 30 wt.% of iron oxide, respectively. Magnetization data showed that both HAp/iron oxide composites had superparamagnetic behaviour at room temperature. © 2019 University of Novi Sad, Faculty of Technology. All rights reserved.", journal = "Processing and Application of Ceramics", title = "Hydroxyapatite/iron oxide nanocomposite prepared by high energy ball milling", volume = "13", number = "2", pages = "210-217", doi = "10.2298/PAC1902210V" }
Vučinić-Vasić, M., Antić, B., Bošković, M., Antić, A.,& Blanuša, J.. (2019). Hydroxyapatite/iron oxide nanocomposite prepared by high energy ball milling. in Processing and Application of Ceramics, 13(2), 210-217. https://doi.org/10.2298/PAC1902210V
Vučinić-Vasić M, Antić B, Bošković M, Antić A, Blanuša J. Hydroxyapatite/iron oxide nanocomposite prepared by high energy ball milling. in Processing and Application of Ceramics. 2019;13(2):210-217. doi:10.2298/PAC1902210V .
Vučinić-Vasić, Milica, Antić, Bratislav, Bošković, Marko, Antić, Aleksandar, Blanuša, Jovan, "Hydroxyapatite/iron oxide nanocomposite prepared by high energy ball milling" in Processing and Application of Ceramics, 13, no. 2 (2019):210-217, https://doi.org/10.2298/PAC1902210V . .