Synthesis and spectroscopic characterisation of LiFePO4 cathode materials

Lazarević, Zorica Ž.; Križan, Gregor; Križan, Janez; Mitrić, Miodrag; Paunović, Novica M.; Milutinović, Aleksandra N.; Romčević, Nebojša Ž.

No Thumbnail

Authors

Lazarević, Zorica Ž.
Križan, Gregor

Križan, Janez
Mitrić, Miodrag

Paunović, Novica M.
Milutinović, Aleksandra N.
Romčević, Nebojša Ž.

Article (Published version)

Metadata

Show full item record

Abstract

Lithium iron phosphate (LiFePO4) are synthesized in complete and incomplete combustion and calcined at 700°C. The obtained samples were characterized by XRD, IR spectroscopy and magnetic measurement. Morphology of samples was controlled by SEM. The aim of this work is to show that it is possible to achieve a desired crystal phase by pulse combustion in a relatively cheap and fast way. The extremely rapid synthesis of almost pure phase material is possible due to the reduction in size of interacting particles and to an enormous number of collisions between them as a result of the strong turbulent flow associated with explosive combustion. © 2019 Optoelectronics and Advanced Materials, Rapid Communications. All rights reserved.

Keywords:

Lithium iron phosphate / IR spectroscopy / Magnetic measurements

Source:
Optoelectronics and Advanced Materials, Rapid Communications, 2019, 13, 3-4, 228-234

Funding / projects:

Optoelectronics nanodimension systems - the rout towards applications (RS-45003)

ISSN: 1842-6573

WoS: 000475814900013

TY  - JOUR
AU  - Lazarević, Zorica Ž.
AU  - Križan, Gregor
AU  - Križan, Janez
AU  - Mitrić, Miodrag
AU  - Paunović, Novica M.
AU  - Milutinović, Aleksandra N.
AU  - Romčević, Nebojša Ž.
PY  - 2019
UR  - https://vinar.vin.bg.ac.rs/handle/123456789/8437
AB  - Lithium iron phosphate (LiFePO4) are synthesized in complete and incomplete combustion and calcined at 700°C. The obtained samples were characterized by XRD, IR spectroscopy and magnetic measurement. Morphology of samples was controlled by SEM. The aim of this work is to show that it is possible to achieve a desired crystal phase by pulse combustion in a relatively cheap and fast way. The extremely rapid synthesis of almost pure phase material is possible due to the reduction in size of interacting particles and to an enormous number of collisions between them as a result of the strong turbulent flow associated with explosive combustion. © 2019 Optoelectronics and Advanced Materials, Rapid Communications. All rights reserved.
T2  - Optoelectronics and Advanced Materials, Rapid Communications
T1  - Synthesis and spectroscopic characterisation of LiFePO4 cathode materials
VL  - 13
IS  - 3-4
SP  - 228
EP  - 234
ER  -

@article{
author = "Lazarević, Zorica Ž. and Križan, Gregor and Križan, Janez and Mitrić, Miodrag and Paunović, Novica M. and Milutinović, Aleksandra N. and Romčević, Nebojša Ž.",
year = "2019",
abstract = "Lithium iron phosphate (LiFePO4) are synthesized in complete and incomplete combustion and calcined at 700°C. The obtained samples were characterized by XRD, IR spectroscopy and magnetic measurement. Morphology of samples was controlled by SEM. The aim of this work is to show that it is possible to achieve a desired crystal phase by pulse combustion in a relatively cheap and fast way. The extremely rapid synthesis of almost pure phase material is possible due to the reduction in size of interacting particles and to an enormous number of collisions between them as a result of the strong turbulent flow associated with explosive combustion. © 2019 Optoelectronics and Advanced Materials, Rapid Communications. All rights reserved.",
journal = "Optoelectronics and Advanced Materials, Rapid Communications",
title = "Synthesis and spectroscopic characterisation of LiFePO4 cathode materials",
volume = "13",
number = "3-4",
pages = "228-234"
}

Lazarević, Z. Ž., Križan, G., Križan, J., Mitrić, M., Paunović, N. M., Milutinović, A. N.,& Romčević, N. Ž.. (2019). Synthesis and spectroscopic characterisation of LiFePO4 cathode materials. in Optoelectronics and Advanced Materials, Rapid Communications, 13(3-4), 228-234.

Lazarević ZŽ, Križan G, Križan J, Mitrić M, Paunović NM, Milutinović AN, Romčević NŽ. Synthesis and spectroscopic characterisation of LiFePO4 cathode materials. in Optoelectronics and Advanced Materials, Rapid Communications. 2019;13(3-4):228-234..

Lazarević, Zorica Ž., Križan, Gregor, Križan, Janez, Mitrić, Miodrag, Paunović, Novica M., Milutinović, Aleksandra N., Romčević, Nebojša Ž., "Synthesis and spectroscopic characterisation of LiFePO4 cathode materials" in Optoelectronics and Advanced Materials, Rapid Communications, 13, no. 3-4 (2019):228-234.