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Combined magnetic and structural characterization of hidrothermal bismuth ferrite (BiFeO3) nanoparticles

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2019
0350-820X1901071M.pdf (910.3Kb)
Authors
Maletaškić, Jelena
Čebela, Maria
Prekajski-Đorđević, Marija D.
Kozlenko, Denis
Kichanov, Sergey
Mitrić, Miodrag
Matović, Branko
Article (Published version)
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© 2018 Authors
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Abstract
Bismuth ferrite (BiFeO3) was synthesized by hydrothermal method. The crystal and magnetic structures of BiFeO3 have been studied by means of X-ray diffraction and neutron powder diffraction at ambient temperature. Microstructure was analysed by scanning electron microscopy. Quantitative phase analysis by the Rietveld method was conducted and crystallite sizes of 27 nm were determined from the XRD line broadening. The magnetic structure of BiFeO3 is described by the G-type antiferromagnetic order with magnetic peak located at 4.6 Å and a noticeable magnetic contribution to a reflection located at 2.4 Å in the diffraction pattern. The values of the ordered magnetic moment of Fe ions μFe=3.8(1) μB, obtained at ambient conditions, are consistent with those determined earlier. The magnetic moments in the crystal plane z = const are arranged in parallel, changing the direction from [100] to [ 110 ] when moving from one to the other z = const plane. © 2018 Authors. Published by the Internatio...nal Institute for the Science of Sintering.

Keywords:
Bismuth ferrite / Magnetic structures / Neutron powder diffraction
Source:
Science of Sintering, 2019, 51, 1, 71-79
Funding / projects:
  • Synthesis, processing and characterization of nanostructured materials for application in the field of energy, mechanical engineering, environmental protection and biomedicine (RS-45012)

DOI: 10.2298/SOS1901071M

ISSN: 0350-820X

WoS: 000496247800006

Scopus: 2-s2.0-85069854570
[ Google Scholar ]
2
2
URI
https://vinar.vin.bg.ac.rs/handle/123456789/8429
Collections
  • Radovi istraživača
Institution/Community
Vinča
TY  - JOUR
AU  - Maletaškić, Jelena
AU  - Čebela, Maria
AU  - Prekajski-Đorđević, Marija D.
AU  - Kozlenko, Denis
AU  - Kichanov, Sergey
AU  - Mitrić, Miodrag
AU  - Matović, Branko
PY  - 2019
UR  - https://vinar.vin.bg.ac.rs/handle/123456789/8429
AB  - Bismuth ferrite (BiFeO3) was synthesized by hydrothermal method. The crystal and magnetic structures of BiFeO3 have been studied by means of X-ray diffraction and neutron powder diffraction at ambient temperature. Microstructure was analysed by scanning electron microscopy. Quantitative phase analysis by the Rietveld method was conducted and crystallite sizes of 27 nm were determined from the XRD line broadening. The magnetic structure of BiFeO3 is described by the G-type antiferromagnetic order with magnetic peak located at 4.6 Å and a noticeable magnetic contribution to a reflection located at 2.4 Å in the diffraction pattern. The values of the ordered magnetic moment of Fe ions μFe=3.8(1) μB, obtained at ambient conditions, are consistent with those determined earlier. The magnetic moments in the crystal plane z = const are arranged in parallel, changing the direction from [100] to [ 110 ] when moving from one to the other z = const plane. © 2018 Authors. Published by the International Institute for the Science of Sintering.
T2  - Science of Sintering
T1  - Combined magnetic and structural characterization of hidrothermal bismuth ferrite (BiFeO3) nanoparticles
VL  - 51
IS  - 1
SP  - 71
EP  - 79
DO  - 10.2298/SOS1901071M
ER  - 
@article{
author = "Maletaškić, Jelena and Čebela, Maria and Prekajski-Đorđević, Marija D. and Kozlenko, Denis and Kichanov, Sergey and Mitrić, Miodrag and Matović, Branko",
year = "2019",
abstract = "Bismuth ferrite (BiFeO3) was synthesized by hydrothermal method. The crystal and magnetic structures of BiFeO3 have been studied by means of X-ray diffraction and neutron powder diffraction at ambient temperature. Microstructure was analysed by scanning electron microscopy. Quantitative phase analysis by the Rietveld method was conducted and crystallite sizes of 27 nm were determined from the XRD line broadening. The magnetic structure of BiFeO3 is described by the G-type antiferromagnetic order with magnetic peak located at 4.6 Å and a noticeable magnetic contribution to a reflection located at 2.4 Å in the diffraction pattern. The values of the ordered magnetic moment of Fe ions μFe=3.8(1) μB, obtained at ambient conditions, are consistent with those determined earlier. The magnetic moments in the crystal plane z = const are arranged in parallel, changing the direction from [100] to [ 110 ] when moving from one to the other z = const plane. © 2018 Authors. Published by the International Institute for the Science of Sintering.",
journal = "Science of Sintering",
title = "Combined magnetic and structural characterization of hidrothermal bismuth ferrite (BiFeO3) nanoparticles",
volume = "51",
number = "1",
pages = "71-79",
doi = "10.2298/SOS1901071M"
}
Maletaškić, J., Čebela, M., Prekajski-Đorđević, M. D., Kozlenko, D., Kichanov, S., Mitrić, M.,& Matović, B.. (2019). Combined magnetic and structural characterization of hidrothermal bismuth ferrite (BiFeO3) nanoparticles. in Science of Sintering, 51(1), 71-79.
https://doi.org/10.2298/SOS1901071M
Maletaškić J, Čebela M, Prekajski-Đorđević MD, Kozlenko D, Kichanov S, Mitrić M, Matović B. Combined magnetic and structural characterization of hidrothermal bismuth ferrite (BiFeO3) nanoparticles. in Science of Sintering. 2019;51(1):71-79.
doi:10.2298/SOS1901071M .
Maletaškić, Jelena, Čebela, Maria, Prekajski-Đorđević, Marija D., Kozlenko, Denis, Kichanov, Sergey, Mitrić, Miodrag, Matović, Branko, "Combined magnetic and structural characterization of hidrothermal bismuth ferrite (BiFeO3) nanoparticles" in Science of Sintering, 51, no. 1 (2019):71-79,
https://doi.org/10.2298/SOS1901071M . .

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