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dc.creatorMatović, Branko
dc.creatorŠaponjić, Aleksandra
dc.creatorPošarac, Milica B.
dc.creatorDevečerski, Aleksandar
dc.creatorRadosavljević-Mihajlović, Ana S.
dc.creatorVolceanov, E.
dc.creatorBošković, Snežana B.
dc.date.accessioned2018-03-03T14:30:58Z
dc.date.available2018-03-03T14:30:58Z
dc.date.issued2008
dc.identifier.issn1454-4164 (print)
dc.identifier.urihttp://vinar.vin.bg.ac.rs/handle/123456789/6749
dc.description.abstractThe possibility of using Mg-exchanged zeolite as additive for densification of Si3N4 ceramic was studied. The zeolitic precursor was previously heated at 800 degrees C to obtain an amorphous powder with a composition corresponding to MgO center dot Al2O3-nSiO(2). The powder was mixed with Si3N4 and the sintering additive was homogenized by attrition milling in the presence of isopropanol and finally compacted by cold isostatic pressure. Pushrod dilatometry was used to measure the shrinkage behaviour of green bodies under a nitrogen atmosphere from room temperature to 1500 degrees C. The chemical reactions and phase evolution during pressureless sintering were also followed by means of X-ray and dilatometric analysis. Results show that the first liquid forms as low as 1070 degrees C, sharing in a significant reduction of sintering temperature. The final phase composition obtained at 1500 degrees C consist of crystalline alpha-Si3N4 phase which is emended in oxynitride glassy phase The results show that the Mg-exchanged zeolite is a very effective low-temperature sintering additive for silicon nitride.en
dc.rightsrestrictedAccessen
dc.sourceJournal of Optoelectronics and Advanced Materialsen
dc.subjectsilicon nitrideen
dc.subjectzeoliteen
dc.subjectdilatometryen
dc.subjectsinteringen
dc.titleSintering of silicon nitride with Mg-exchange zeolite additiveen
dc.typearticleen
dcterms.abstractБошковић Снежана; Волцеанов, Е.; Матовић Бранко; Шапоњић, Aлександра; Пошарац-Марковић Милица; Девечерски Aлександар; Радосављевић-Михајловић Aна;
dc.citation.volume10
dc.citation.issue4
dc.citation.spage880
dc.citation.epage882
dc.identifier.wos000255210300036
dc.citation.rankM23
dc.description.other5th International Conference on New Research Trends in Materials Science, Sep, 2007, Sibiu, Romaniaen


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