Ternary chalcogenide nanoparticles, CuInS2 and CuInSe2, were synthesized in a high-temperature boiling non-polar organic solvent. X-Ray diffraction analysis revealed that both materials had a tetragonal (chalcopyrite) crystal structure. The morphology of the obtained materials was revealed by transmission electron microscopy. Agglomerated spherical CuInS2 nanoparticles with broad size distribution in the range from 2 to 20 nm were obtained. In the case of CuInSe2, isolated particles with a spherical or prismatic shape in the size range from 10 to 25 nm were obtained, as well as agglomerates consisting of much smaller particles with a diameter of about 2-5 nm. The particles with the smallest diameters of both materials exhibited quantum size effects.
TY - JOUR
AU - Abazović, Nadica
AU - Jovanović, Dragana J.
AU - Stoiljković, Milovan
AU - Mitrić, Miodrag
AU - Ahrenkiel, Scott Phillip
AU - Nedeljković, Jovan
AU - Čomor, Mirjana
PY - 2012
UR - http://vinar.vin.bg.ac.rs/handle/123456789/4938
AB - Ternary chalcogenide nanoparticles, CuInS2 and CuInSe2, were synthesized in a high-temperature boiling non-polar organic solvent. X-Ray diffraction analysis revealed that both materials had a tetragonal (chalcopyrite) crystal structure. The morphology of the obtained materials was revealed by transmission electron microscopy. Agglomerated spherical CuInS2 nanoparticles with broad size distribution in the range from 2 to 20 nm were obtained. In the case of CuInSe2, isolated particles with a spherical or prismatic shape in the size range from 10 to 25 nm were obtained, as well as agglomerates consisting of much smaller particles with a diameter of about 2-5 nm. The particles with the smallest diameters of both materials exhibited quantum size effects.
T2 - Journal of the Serbian Chemical Society
T1 - Colloidal chemistry-based synthesis of quantized CuInS2/Se-2 nanoparticles
VL - 77
IS - 6
SP - 789
EP - 797
DO - 10.2298/JSC110420220A
ER -
@article{
author = "Abazović, Nadica and Jovanović, Dragana J. and Stoiljković, Milovan and Mitrić, Miodrag and Ahrenkiel, Scott Phillip and Nedeljković, Jovan and Čomor, Mirjana",
year = "2012",
url = "http://vinar.vin.bg.ac.rs/handle/123456789/4938",
abstract = "Ternary chalcogenide nanoparticles, CuInS2 and CuInSe2, were synthesized in a high-temperature boiling non-polar organic solvent. X-Ray diffraction analysis revealed that both materials had a tetragonal (chalcopyrite) crystal structure. The morphology of the obtained materials was revealed by transmission electron microscopy. Agglomerated spherical CuInS2 nanoparticles with broad size distribution in the range from 2 to 20 nm were obtained. In the case of CuInSe2, isolated particles with a spherical or prismatic shape in the size range from 10 to 25 nm were obtained, as well as agglomerates consisting of much smaller particles with a diameter of about 2-5 nm. The particles with the smallest diameters of both materials exhibited quantum size effects.",
journal = "Journal of the Serbian Chemical Society",
title = "Colloidal chemistry-based synthesis of quantized CuInS2/Se-2 nanoparticles",
volume = "77",
number = "6",
pages = "789-797",
doi = "10.2298/JSC110420220A"
}
Abazović N, Jovanović DJ, Stoiljković M, Mitrić M, Ahrenkiel SP, Nedeljković J, Čomor M. Colloidal chemistry-based synthesis of quantized CuInS2/Se-2 nanoparticles. Journal of the Serbian Chemical Society. 2012;77(6):789-797
Abazović, N., Jovanović, D. J., Stoiljković, M., Mitrić, M., Ahrenkiel, S. P., Nedeljković, J.,& Čomor, M. (2012). Colloidal chemistry-based synthesis of quantized CuInS2/Se-2 nanoparticles.
Journal of the Serbian Chemical Society, 77(6), 789-797.
https://doi.org/10.2298/JSC110420220A
