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Transition metal complexes with Girard reagent-based ligands. Part V. Synthesis, characterization and crystal structure of pentagonal-bipyramidal manganese(II) complex with 2,6-diacetylpyridine bis(Girard-T hydrazone)

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Authors
Vojinović-Ješić, Ljiljana S.
Češljević, Valerija I.
Bogdanović, Goran A.
Leovac, Vukadin M.
Szecsenyi, Katalin Meszaros
Divjakovic, Vladimir
Joksović, Milan D.
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Abstract
The article describes the synthesis and crystal structure of the Mn(II) complex with 2,6-diacetylpyridine bis (Girard-T hydrazone), (H(2)dap(GT)(2))(2+), of the formula [Mn(H(2)dap(GT)(2))(NCS)(2)](NCS)(2)center dot MeOH. The complex has a pentagonal-bipyramidal coordination geometry, with pentadentate N(3)O(2) ligand in the equatorial plane and two isothiocyanato groups in the axial positions. Both the ligand and the complex are characterized by their FT-IR spectra and thermal data. (C) 2010 Elsevier B.V. All rights reserved.
Keywords:
Mn(II) complex / bis(Girard-T hydrazone) / Crystal structure / Pentagonal-bipyramidal coordination
Source:
Inorganic Chemistry Communications, 2010, 13, 9, 1085-1088
Funding / projects:
  • Ministry of Science and Technological Development of the Republic of Serbia [142028], Provincial Secretariat for Science and Technological Development of Vojvodina

DOI: 10.1016/j.inoche.2010.06.022

ISSN: 1387-7003

WoS: 000281011900021

Scopus: 2-s2.0-77955424448
[ Google Scholar ]
15
12
URI
https://vinar.vin.bg.ac.rs/handle/123456789/4079
Collections
  • WoS Import
Institution/Community
Vinča
TY  - JOUR
AU  - Vojinović-Ješić, Ljiljana S.
AU  - Češljević, Valerija I.
AU  - Bogdanović, Goran A.
AU  - Leovac, Vukadin M.
AU  - Szecsenyi, Katalin Meszaros
AU  - Divjakovic, Vladimir
AU  - Joksović, Milan D.
PY  - 2010
UR  - https://vinar.vin.bg.ac.rs/handle/123456789/4079
AB  - The article describes the synthesis and crystal structure of the Mn(II) complex with 2,6-diacetylpyridine bis (Girard-T hydrazone), (H(2)dap(GT)(2))(2+), of the formula [Mn(H(2)dap(GT)(2))(NCS)(2)](NCS)(2)center dot MeOH. The complex has a pentagonal-bipyramidal coordination geometry, with pentadentate N(3)O(2) ligand in the equatorial plane and two isothiocyanato groups in the axial positions. Both the ligand and the complex are characterized by their FT-IR spectra and thermal data. (C) 2010 Elsevier B.V. All rights reserved.
T2  - Inorganic Chemistry Communications
T1  - Transition metal complexes with Girard reagent-based ligands. Part V. Synthesis, characterization and crystal structure of pentagonal-bipyramidal manganese(II) complex with 2,6-diacetylpyridine bis(Girard-T hydrazone)
VL  - 13
IS  - 9
SP  - 1085
EP  - 1088
DO  - 10.1016/j.inoche.2010.06.022
ER  - 
@article{
author = "Vojinović-Ješić, Ljiljana S. and Češljević, Valerija I. and Bogdanović, Goran A. and Leovac, Vukadin M. and Szecsenyi, Katalin Meszaros and Divjakovic, Vladimir and Joksović, Milan D.",
year = "2010",
abstract = "The article describes the synthesis and crystal structure of the Mn(II) complex with 2,6-diacetylpyridine bis (Girard-T hydrazone), (H(2)dap(GT)(2))(2+), of the formula [Mn(H(2)dap(GT)(2))(NCS)(2)](NCS)(2)center dot MeOH. The complex has a pentagonal-bipyramidal coordination geometry, with pentadentate N(3)O(2) ligand in the equatorial plane and two isothiocyanato groups in the axial positions. Both the ligand and the complex are characterized by their FT-IR spectra and thermal data. (C) 2010 Elsevier B.V. All rights reserved.",
journal = "Inorganic Chemistry Communications",
title = "Transition metal complexes with Girard reagent-based ligands. Part V. Synthesis, characterization and crystal structure of pentagonal-bipyramidal manganese(II) complex with 2,6-diacetylpyridine bis(Girard-T hydrazone)",
volume = "13",
number = "9",
pages = "1085-1088",
doi = "10.1016/j.inoche.2010.06.022"
}
Vojinović-Ješić, L. S., Češljević, V. I., Bogdanović, G. A., Leovac, V. M., Szecsenyi, K. M., Divjakovic, V.,& Joksović, M. D.. (2010). Transition metal complexes with Girard reagent-based ligands. Part V. Synthesis, characterization and crystal structure of pentagonal-bipyramidal manganese(II) complex with 2,6-diacetylpyridine bis(Girard-T hydrazone). in Inorganic Chemistry Communications, 13(9), 1085-1088.
https://doi.org/10.1016/j.inoche.2010.06.022
Vojinović-Ješić LS, Češljević VI, Bogdanović GA, Leovac VM, Szecsenyi KM, Divjakovic V, Joksović MD. Transition metal complexes with Girard reagent-based ligands. Part V. Synthesis, characterization and crystal structure of pentagonal-bipyramidal manganese(II) complex with 2,6-diacetylpyridine bis(Girard-T hydrazone). in Inorganic Chemistry Communications. 2010;13(9):1085-1088.
doi:10.1016/j.inoche.2010.06.022 .
Vojinović-Ješić, Ljiljana S., Češljević, Valerija I., Bogdanović, Goran A., Leovac, Vukadin M., Szecsenyi, Katalin Meszaros, Divjakovic, Vladimir, Joksović, Milan D., "Transition metal complexes with Girard reagent-based ligands. Part V. Synthesis, characterization and crystal structure of pentagonal-bipyramidal manganese(II) complex with 2,6-diacetylpyridine bis(Girard-T hydrazone)" in Inorganic Chemistry Communications, 13, no. 9 (2010):1085-1088,
https://doi.org/10.1016/j.inoche.2010.06.022 . .

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