Laser-Induced Breakdown Spectroscopy (LIBS) micro-mapping is an important analytical tool for the study of geomaterials. In this work, this technique was applied, for the first time, to the analysis of alkali-activated materials and geopolymers, as well as rocks, mortars and bricks. The results obtained were compared with the ones obtained using Energy-Dispersive X-Ray Fluorescence (ED-XRF) macro-mapping and the advantages of the LIBS approach (speed, lateral and in-depth resolution, capability of light elements analysis) were highlighted. The issues associated with the quantitative determination of the samples' composition from the analysis of the LIBS spectra were also briefly discussed.
TY - JOUR
AU - Raneri, Simona
AU - Botto, Asia
AU - Campanella, Beatrice
AU - Momčilović, Miloš
AU - Palleschi, Vincenzo
AU - Poggialini, Francesco
AU - Sciuto, Claudia
AU - Gattiglia, Gabriele
AU - Volpintesta, Francesco
AU - Selvaraj, Thirumalini
AU - Živković, Sanja
AU - Lorenzetti, Giulia
AU - Legnaioli, Stefano
PY - 2022
UR - https://vinar.vin.bg.ac.rs/handle/123456789/10338
AB - Laser-Induced Breakdown Spectroscopy (LIBS) micro-mapping is an important analytical tool for the study of geomaterials. In this work, this technique was applied, for the first time, to the analysis of alkali-activated materials and geopolymers, as well as rocks, mortars and bricks. The results obtained were compared with the ones obtained using Energy-Dispersive X-Ray Fluorescence (ED-XRF) macro-mapping and the advantages of the LIBS approach (speed, lateral and in-depth resolution, capability of light elements analysis) were highlighted. The issues associated with the quantitative determination of the samples' composition from the analysis of the LIBS spectra were also briefly discussed.
T2 - Spectrochimica Acta Part B: Atomic Spectroscopy
T1 - Increasing resolution in chemical mapping of geomaterials: From X-ray fluorescence to laser-induced breakdown spectroscopy
VL - 194
SP - 106482
DO - 10.1016/j.sab.2022.106482
ER -
@article{
author = "Raneri, Simona and Botto, Asia and Campanella, Beatrice and Momčilović, Miloš and Palleschi, Vincenzo and Poggialini, Francesco and Sciuto, Claudia and Gattiglia, Gabriele and Volpintesta, Francesco and Selvaraj, Thirumalini and Živković, Sanja and Lorenzetti, Giulia and Legnaioli, Stefano",
year = "2022",
abstract = "Laser-Induced Breakdown Spectroscopy (LIBS) micro-mapping is an important analytical tool for the study of geomaterials. In this work, this technique was applied, for the first time, to the analysis of alkali-activated materials and geopolymers, as well as rocks, mortars and bricks. The results obtained were compared with the ones obtained using Energy-Dispersive X-Ray Fluorescence (ED-XRF) macro-mapping and the advantages of the LIBS approach (speed, lateral and in-depth resolution, capability of light elements analysis) were highlighted. The issues associated with the quantitative determination of the samples' composition from the analysis of the LIBS spectra were also briefly discussed.",
journal = "Spectrochimica Acta Part B: Atomic Spectroscopy",
title = "Increasing resolution in chemical mapping of geomaterials: From X-ray fluorescence to laser-induced breakdown spectroscopy",
volume = "194",
pages = "106482",
doi = "10.1016/j.sab.2022.106482"
}
Raneri, S., Botto, A., Campanella, B., Momčilović, M., Palleschi, V., Poggialini, F., Sciuto, C., Gattiglia, G., Volpintesta, F., Selvaraj, T., Živković, S., Lorenzetti, G.,& Legnaioli, S.. (2022). Increasing resolution in chemical mapping of geomaterials: From X-ray fluorescence to laser-induced breakdown spectroscopy. in Spectrochimica Acta Part B: Atomic Spectroscopy, 194, 106482.
https://doi.org/10.1016/j.sab.2022.106482
Raneri S, Botto A, Campanella B, Momčilović M, Palleschi V, Poggialini F, Sciuto C, Gattiglia G, Volpintesta F, Selvaraj T, Živković S, Lorenzetti G, Legnaioli S. Increasing resolution in chemical mapping of geomaterials: From X-ray fluorescence to laser-induced breakdown spectroscopy. in Spectrochimica Acta Part B: Atomic Spectroscopy. 2022;194:106482.
doi:10.1016/j.sab.2022.106482 .
Raneri, Simona, Botto, Asia, Campanella, Beatrice, Momčilović, Miloš, Palleschi, Vincenzo, Poggialini, Francesco, Sciuto, Claudia, Gattiglia, Gabriele, Volpintesta, Francesco, Selvaraj, Thirumalini, Živković, Sanja, Lorenzetti, Giulia, Legnaioli, Stefano, "Increasing resolution in chemical mapping of geomaterials: From X-ray fluorescence to laser-induced breakdown spectroscopy" in Spectrochimica Acta Part B: Atomic Spectroscopy, 194 (2022):106482,
https://doi.org/10.1016/j.sab.2022.106482 . .
