TY  - JOUR
AU  - Matović, Branko
AU  - Maletaškić, Jelena
AU  - Zagorac, Jelena B.
AU  - Pavkov, Vladimir
AU  - Maki, Ryosuke S.S.
AU  - Yoshida, Katsumi
AU  - Yano, Toyohiko
PY  - 2020
UR  - https://vinar.vin.bg.ac.rs/handle/123456789/8668
AB  - Three different lanthanide zirconate powders: Pr2Zr2O7, Sm2Zr2O7 and PrSmZr2O7 were prepared by combustion synthesis. The synthesis initially yielded amorphous powders, which crystallized after subsequent thermal treatment. Well-crystallized compounds were formed after calcination at temperature as low as 950 °C. Effect of the thermal treatment on the phase evolution was studied by X-ray powder diffraction (XRD). The powders calcined at the highest temperature (1550 °C) showed that all compositions possess the pyrochlore structure with the space group No. 227. The obtained powders were compacted and pressureless sintered without additive at 1600 °C for 4 h in the air. Microstructure development was examined by field emission scanning electron microscopy, as well as by transmission electron microscopy. It was found that the lowest value for thermal conductivity, 1.2 W/m K, was obtained for mixed lanthanide composition with pyrochlore structure (PrSmZr2O7). The effect of chemical composition on micro-hardness and thermal conductivity of the obtained zirconates was studied. © 2019 Elsevier Ltd
T2  - Journal of the European Ceramic Society
T1  - Synthesis and characterization of pyrochlore lanthanide (Pr, Sm) zirconate ceramics
VL  - 40
IS  - 7
SP  - 2652
EP  - 2657
DO  - 10.1016/j.jeurceramsoc.2019.11.012
ER  - 

@article{
author = "Matović, Branko and Maletaškić, Jelena and Zagorac, Jelena B. and Pavkov, Vladimir and Maki, Ryosuke S.S. and Yoshida, Katsumi and Yano, Toyohiko",
year = "2020",
abstract = "Three different lanthanide zirconate powders: Pr2Zr2O7, Sm2Zr2O7 and PrSmZr2O7 were prepared by combustion synthesis. The synthesis initially yielded amorphous powders, which crystallized after subsequent thermal treatment. Well-crystallized compounds were formed after calcination at temperature as low as 950 °C. Effect of the thermal treatment on the phase evolution was studied by X-ray powder diffraction (XRD). The powders calcined at the highest temperature (1550 °C) showed that all compositions possess the pyrochlore structure with the space group No. 227. The obtained powders were compacted and pressureless sintered without additive at 1600 °C for 4 h in the air. Microstructure development was examined by field emission scanning electron microscopy, as well as by transmission electron microscopy. It was found that the lowest value for thermal conductivity, 1.2 W/m K, was obtained for mixed lanthanide composition with pyrochlore structure (PrSmZr2O7). The effect of chemical composition on micro-hardness and thermal conductivity of the obtained zirconates was studied. © 2019 Elsevier Ltd",
journal = "Journal of the European Ceramic Society",
title = "Synthesis and characterization of pyrochlore lanthanide (Pr, Sm) zirconate ceramics",
volume = "40",
number = "7",
pages = "2652-2657",
doi = "10.1016/j.jeurceramsoc.2019.11.012"
}

Matović, B., Maletaškić, J., Zagorac, J. B., Pavkov, V., Maki, R. S.S., Yoshida, K.,& Yano, T.. (2020). Synthesis and characterization of pyrochlore lanthanide (Pr, Sm) zirconate ceramics. in Journal of the European Ceramic Society, 40(7), 2652-2657.
https://doi.org/10.1016/j.jeurceramsoc.2019.11.012

Matović B, Maletaškić J, Zagorac JB, Pavkov V, Maki RS, Yoshida K, Yano T. Synthesis and characterization of pyrochlore lanthanide (Pr, Sm) zirconate ceramics. in Journal of the European Ceramic Society. 2020;40(7):2652-2657.
doi:10.1016/j.jeurceramsoc.2019.11.012 .

Matović, Branko, Maletaškić, Jelena, Zagorac, Jelena B., Pavkov, Vladimir, Maki, Ryosuke S.S., Yoshida, Katsumi, Yano, Toyohiko, "Synthesis and characterization of pyrochlore lanthanide (Pr, Sm) zirconate ceramics" in Journal of the European Ceramic Society, 40, no. 7 (2020):2652-2657,
https://doi.org/10.1016/j.jeurceramsoc.2019.11.012 . .