Romhanji, Endre L.

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Identification of Fe-bearing phases in the as-cast microstructure of AA6026 alloy and their evolution during homogenization treatment

Radetić, Tamara; Popović, Miljana M.; Novaković, Mirjana M.; Rajić, Vladimir; Romhanji, Endre L.

(2023)

TY  - JOUR
AU  - Radetić, Tamara
AU  - Popović, Miljana M.
AU  - Novaković, Mirjana M.
AU  - Rajić, Vladimir
AU  - Romhanji, Endre L.
PY  - 2023
UR  - https://vinar.vin.bg.ac.rs/handle/123456789/12726
AB  - The Fe-bearing intermetallic phases present in the as-cast AA6026 alloy and their evolution during homogenization treatments at 480-550°C were investigated using optical microscopy, SEM, and TEM techniques in combination with EDS analysis. In addition to the α-Al(Fe,Mn)Si phase with dendritic morphology, two types of plate-like Fe-bearing microconstituents were revealed in the microstructure of the as-cast alloy. The EDS microanalysis and electron diffraction showed that one set of platelets represented thin sections of α-Al(Fe,Mn)Si microconstituent. The other set of plate-like microconstituents was identified as a tetragonal, silicon-rich δ-Al4(Fe,Mn)Si2 phase. The formation of the δ-Al4(Fe,Mn)Si2 phase was attributed to the chemical composition of the alloy. During homogenization, the metastable δ-Al4(Fe,Mn)Si2 transformed into the α-Al(Fe,Mn)Si phase and fragmented. The dendritic α-Al(Fe,Mn)Si microconstituents underwent fragmentation. However, while the α-Al(Fe,Mn)Si microconstituents preserved a b.c.c. crystal lattice throughout the process, the product of the transformation of the δ-Al4(Fe,Mn)Si2 phase exhibited primitive cubic lattice.
AB  - Ispitivanje prisustva faza koje sadrže Fe u mikrostrukturi livene legure AA6026, kao i njihova evolucija tokom postupaka homogenizacije na temperaturama od 480-550 °C, sprovedena su korišćenjem optičke mikroskopije, skenirajuće elektronske mikroskopije (SEM) i transmisione elektronske mikroskopije (TEM) u kombinaciji sa analizom EDS-a. Osim faze α-Al(Fe,Mn)Si sa dendritskom morfologijom, identifikovane su dve vrste pločastih mikrokonstituenata koji sadrže Fe u mikrostrukturi livene legure. EDS mikroanaliza i elektronska difrakcija pokazali su da jedan skup ploča predstavlja samo tanke sekcije mikrokonstituente α-Al(Fe,Mn)Si. Drugi skup pločastih mikrokonstituenata identifikovan je kao četvrtasta, silicijumom bogata faza δ-Al4 (Fe,Mn)Si2 . Formiranje faze δ-Al4 (Fe,Mn)Si2 povezano je sa hemijskim sastavom legure. Tokom homogenizacije, metastabilna faza δ-Al4 (Fe,Mn)Si2 transformisala se u fazu α-Al(Fe,Mn)Si i fragmentirala. Dendritski mikrokonstituenti α-Al(Fe,Mn)Si takođe su fragmentirali. Međutim, dok su mikrokonstituenti α-Al(Fe,Mn)Si sačuvali kubnu kristalnu rešetku tipa b.c.c. tokom procesa, proizvod transformacije faze δ-Al4 (Fe,Mn)Si2 pokazao je prostu kubnu rešetku.
T2  - Journal of Mining and Metallurgy, Section B: Metallurgy
T1  - Identification of Fe-bearing phases in the as-cast microstructure of AA6026 alloy and their evolution during homogenization treatment
T1  - Prepoznavanje faza koje sadrže Fe u mikrostrukturi livene legure AA6026 i njihova evolucija tokom postupka homogenizacije
VL  - 59
IS  - 2
SP  - 327
EP  - 338
DO  - 10.2298/JMMB230611028R
ER  - 
@article{
author = "Radetić, Tamara and Popović, Miljana M. and Novaković, Mirjana M. and Rajić, Vladimir and Romhanji, Endre L.",
year = "2023",
abstract = "The Fe-bearing intermetallic phases present in the as-cast AA6026 alloy and their evolution during homogenization treatments at 480-550°C were investigated using optical microscopy, SEM, and TEM techniques in combination with EDS analysis. In addition to the α-Al(Fe,Mn)Si phase with dendritic morphology, two types of plate-like Fe-bearing microconstituents were revealed in the microstructure of the as-cast alloy. The EDS microanalysis and electron diffraction showed that one set of platelets represented thin sections of α-Al(Fe,Mn)Si microconstituent. The other set of plate-like microconstituents was identified as a tetragonal, silicon-rich δ-Al4(Fe,Mn)Si2 phase. The formation of the δ-Al4(Fe,Mn)Si2 phase was attributed to the chemical composition of the alloy. During homogenization, the metastable δ-Al4(Fe,Mn)Si2 transformed into the α-Al(Fe,Mn)Si phase and fragmented. The dendritic α-Al(Fe,Mn)Si microconstituents underwent fragmentation. However, while the α-Al(Fe,Mn)Si microconstituents preserved a b.c.c. crystal lattice throughout the process, the product of the transformation of the δ-Al4(Fe,Mn)Si2 phase exhibited primitive cubic lattice., Ispitivanje prisustva faza koje sadrže Fe u mikrostrukturi livene legure AA6026, kao i njihova evolucija tokom postupaka homogenizacije na temperaturama od 480-550 °C, sprovedena su korišćenjem optičke mikroskopije, skenirajuće elektronske mikroskopije (SEM) i transmisione elektronske mikroskopije (TEM) u kombinaciji sa analizom EDS-a. Osim faze α-Al(Fe,Mn)Si sa dendritskom morfologijom, identifikovane su dve vrste pločastih mikrokonstituenata koji sadrže Fe u mikrostrukturi livene legure. EDS mikroanaliza i elektronska difrakcija pokazali su da jedan skup ploča predstavlja samo tanke sekcije mikrokonstituente α-Al(Fe,Mn)Si. Drugi skup pločastih mikrokonstituenata identifikovan je kao četvrtasta, silicijumom bogata faza δ-Al4 (Fe,Mn)Si2 . Formiranje faze δ-Al4 (Fe,Mn)Si2 povezano je sa hemijskim sastavom legure. Tokom homogenizacije, metastabilna faza δ-Al4 (Fe,Mn)Si2 transformisala se u fazu α-Al(Fe,Mn)Si i fragmentirala. Dendritski mikrokonstituenti α-Al(Fe,Mn)Si takođe su fragmentirali. Međutim, dok su mikrokonstituenti α-Al(Fe,Mn)Si sačuvali kubnu kristalnu rešetku tipa b.c.c. tokom procesa, proizvod transformacije faze δ-Al4 (Fe,Mn)Si2 pokazao je prostu kubnu rešetku.",
journal = "Journal of Mining and Metallurgy, Section B: Metallurgy",
title = "Identification of Fe-bearing phases in the as-cast microstructure of AA6026 alloy and their evolution during homogenization treatment, Prepoznavanje faza koje sadrže Fe u mikrostrukturi livene legure AA6026 i njihova evolucija tokom postupka homogenizacije",
volume = "59",
number = "2",
pages = "327-338",
doi = "10.2298/JMMB230611028R"
}
Radetić, T., Popović, M. M., Novaković, M. M., Rajić, V.,& Romhanji, E. L.. (2023). Identification of Fe-bearing phases in the as-cast microstructure of AA6026 alloy and their evolution during homogenization treatment. in Journal of Mining and Metallurgy, Section B: Metallurgy, 59(2), 327-338.
https://doi.org/10.2298/JMMB230611028R
Radetić T, Popović MM, Novaković MM, Rajić V, Romhanji EL. Identification of Fe-bearing phases in the as-cast microstructure of AA6026 alloy and their evolution during homogenization treatment. in Journal of Mining and Metallurgy, Section B: Metallurgy. 2023;59(2):327-338.
doi:10.2298/JMMB230611028R .
Radetić, Tamara, Popović, Miljana M., Novaković, Mirjana M., Rajić, Vladimir, Romhanji, Endre L., "Identification of Fe-bearing phases in the as-cast microstructure of AA6026 alloy and their evolution during homogenization treatment" in Journal of Mining and Metallurgy, Section B: Metallurgy, 59, no. 2 (2023):327-338,
https://doi.org/10.2298/JMMB230611028R . .