Radičić, Rafaela

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  • Radičić, Rafaela (3)
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Author's Bibliography

Enhancement of Methylene Blue Photodegradation Rate Using Laser Synthesized Ag-Doped ZnO Nanoparticles

Blažeka, Damjan; Radičić, Rafaela; Maletić, Dejan; Živković, Sanja; Momčilović, Miloš; Krstulović, Nikša

(2022)

TY  - JOUR
AU  - Blažeka, Damjan
AU  - Radičić, Rafaela
AU  - Maletić, Dejan
AU  - Živković, Sanja
AU  - Momčilović, Miloš
AU  - Krstulović, Nikša
PY  - 2022
UR  - https://vinar.vin.bg.ac.rs/handle/123456789/10407
AB  - In this work, Ag-doped ZnO nanoparticles are obtained via pulsed laser ablation of the Ag-coated ZnO target in water. The ratio of Ag dopant in ZnO nanoparticles strongly depends on the thickness of the Ag layer at the ZnO target. Synthesized nanoparticles were characterized by XRD, XPS, SEM, EDS, ICP-OES, and UV–VIS spectrophotometry to obtain their crystal structure, elemental composition, morphology and size distribution, mass concentration, and optical properties, respectively. The photocatalytic studies showed photodegradation of methylene blue (MB) under UV irradiation. Different ratios of Ag dopant in ZnO nanoparticles influence the photodegradation rate. The ZnO nanoparticles doped with 0.32% silver show the most efficient photodegradation rate, with the chemical reaction constant of 0.0233 min−1. It exhibits an almost twice as large photodegradation rate compared to pure ZnO nanoparticles, showing the doping effect on the photocatalytic activity.
T2  - Nanomaterials
T1  - Enhancement of Methylene Blue Photodegradation Rate Using Laser Synthesized Ag-Doped ZnO Nanoparticles
VL  - 12
IS  - 15
SP  - 2677
DO  - 10.3390/nano12152677
ER  - 
@article{
author = "Blažeka, Damjan and Radičić, Rafaela and Maletić, Dejan and Živković, Sanja and Momčilović, Miloš and Krstulović, Nikša",
year = "2022",
abstract = "In this work, Ag-doped ZnO nanoparticles are obtained via pulsed laser ablation of the Ag-coated ZnO target in water. The ratio of Ag dopant in ZnO nanoparticles strongly depends on the thickness of the Ag layer at the ZnO target. Synthesized nanoparticles were characterized by XRD, XPS, SEM, EDS, ICP-OES, and UV–VIS spectrophotometry to obtain their crystal structure, elemental composition, morphology and size distribution, mass concentration, and optical properties, respectively. The photocatalytic studies showed photodegradation of methylene blue (MB) under UV irradiation. Different ratios of Ag dopant in ZnO nanoparticles influence the photodegradation rate. The ZnO nanoparticles doped with 0.32% silver show the most efficient photodegradation rate, with the chemical reaction constant of 0.0233 min−1. It exhibits an almost twice as large photodegradation rate compared to pure ZnO nanoparticles, showing the doping effect on the photocatalytic activity.",
journal = "Nanomaterials",
title = "Enhancement of Methylene Blue Photodegradation Rate Using Laser Synthesized Ag-Doped ZnO Nanoparticles",
volume = "12",
number = "15",
pages = "2677",
doi = "10.3390/nano12152677"
}
Blažeka, D., Radičić, R., Maletić, D., Živković, S., Momčilović, M.,& Krstulović, N.. (2022). Enhancement of Methylene Blue Photodegradation Rate Using Laser Synthesized Ag-Doped ZnO Nanoparticles. in Nanomaterials, 12(15), 2677.
https://doi.org/10.3390/nano12152677
Blažeka D, Radičić R, Maletić D, Živković S, Momčilović M, Krstulović N. Enhancement of Methylene Blue Photodegradation Rate Using Laser Synthesized Ag-Doped ZnO Nanoparticles. in Nanomaterials. 2022;12(15):2677.
doi:10.3390/nano12152677 .
Blažeka, Damjan, Radičić, Rafaela, Maletić, Dejan, Živković, Sanja, Momčilović, Miloš, Krstulović, Nikša, "Enhancement of Methylene Blue Photodegradation Rate Using Laser Synthesized Ag-Doped ZnO Nanoparticles" in Nanomaterials, 12, no. 15 (2022):2677,
https://doi.org/10.3390/nano12152677 . .
14
9

Laser ablation and chemical synthesis of bicomponent ZnO nanoparticles

Maletić, Dejan; Čebela, Maria; Blažeka, Damjan; Radičić, Rafaela; Pajić, Damir; Krstulović, Nikša

(Slovenia : Slovenian Society for Vacuum Technique, 2021)

TY  - CONF
AU  - Maletić, Dejan
AU  - Čebela, Maria
AU  - Blažeka, Damjan
AU  - Radičić, Rafaela
AU  - Pajić, Damir
AU  - Krstulović, Nikša
PY  - 2021
UR  - https://vinar.vin.bg.ac.rs/handle/123456789/11526
AB  - The bicomponent nano particles draw attention of the researchers because introducing the second component into the crystal lattice of the nanoparticle we can tune physical properties of the material. One of the simplest and fastest method for synthesis of various bicomponent nanoparticles is by pulsed lasers ablation of the bulk material in water. For the synthesis of our bicomponent nanoparticles we use twostep process. The first step is to deposit a thin film of metal onto ZnO substrate using pulsed laser deposition in vacuum (PLD). The second step is to produce colloidal solution of nanoparticles by laser ablation in water (LAL) of metal coated ZnO. The ablating target was then scanned with laser beam in order to avoid heating of the target and to produce the high yield of bicomponent nanoparticles. The obtained nanoparticles were characterized using UV-VIS, XPS, SEM and XRD diagnostics. The second process that we used for synthetizing bicomponent zinc oxide nanoparticles was self-propagating room temperature reaction of zinc nitrate with sodium hydroxide with addition of (x=1; 3 and 5%) of AgNO3. The chemical composition of the produced nanoparticles is Zn1−xAgxO (x=0.01;0.05 and 0.05). After the reaction, obtained powder was calcinated at 1100 °C for 4 h in a furnace. The diffraction patterns were recorded at room temperature and atmospheric pressure in the absence of any re-heating of the samples. From the XRD spectra we found that no second phase were formed in the samples, the ions of silver are embedded into the crystal lattice of the nanoparticles. The bicomponent nanoparticles produced with these two methods are tested for the photocatalytic activity. We used UV lamp for irradiation of nanoparticle and organic dye (methylene blue – MB) mixture in a cuvette. The nanoparticles synthetized with both methods show good photocatalytic activity for degradation of organic dye.
PB  - Slovenia : Slovenian Society for Vacuum Technique
C3  - 27th International scientific meeting on vacuum science and technique : programme and the book of abstracts; September 9-10, Gozd Martuljek, Slovenia
T1  - Laser ablation and chemical synthesis of bicomponent ZnO nanoparticles
SP  - 26
UR  - https://hdl.handle.net/21.15107/rcub_vinar_11526
ER  - 
@conference{
author = "Maletić, Dejan and Čebela, Maria and Blažeka, Damjan and Radičić, Rafaela and Pajić, Damir and Krstulović, Nikša",
year = "2021",
abstract = "The bicomponent nano particles draw attention of the researchers because introducing the second component into the crystal lattice of the nanoparticle we can tune physical properties of the material. One of the simplest and fastest method for synthesis of various bicomponent nanoparticles is by pulsed lasers ablation of the bulk material in water. For the synthesis of our bicomponent nanoparticles we use twostep process. The first step is to deposit a thin film of metal onto ZnO substrate using pulsed laser deposition in vacuum (PLD). The second step is to produce colloidal solution of nanoparticles by laser ablation in water (LAL) of metal coated ZnO. The ablating target was then scanned with laser beam in order to avoid heating of the target and to produce the high yield of bicomponent nanoparticles. The obtained nanoparticles were characterized using UV-VIS, XPS, SEM and XRD diagnostics. The second process that we used for synthetizing bicomponent zinc oxide nanoparticles was self-propagating room temperature reaction of zinc nitrate with sodium hydroxide with addition of (x=1; 3 and 5%) of AgNO3. The chemical composition of the produced nanoparticles is Zn1−xAgxO (x=0.01;0.05 and 0.05). After the reaction, obtained powder was calcinated at 1100 °C for 4 h in a furnace. The diffraction patterns were recorded at room temperature and atmospheric pressure in the absence of any re-heating of the samples. From the XRD spectra we found that no second phase were formed in the samples, the ions of silver are embedded into the crystal lattice of the nanoparticles. The bicomponent nanoparticles produced with these two methods are tested for the photocatalytic activity. We used UV lamp for irradiation of nanoparticle and organic dye (methylene blue – MB) mixture in a cuvette. The nanoparticles synthetized with both methods show good photocatalytic activity for degradation of organic dye.",
publisher = "Slovenia : Slovenian Society for Vacuum Technique",
journal = "27th International scientific meeting on vacuum science and technique : programme and the book of abstracts; September 9-10, Gozd Martuljek, Slovenia",
title = "Laser ablation and chemical synthesis of bicomponent ZnO nanoparticles",
pages = "26",
url = "https://hdl.handle.net/21.15107/rcub_vinar_11526"
}
Maletić, D., Čebela, M., Blažeka, D., Radičić, R., Pajić, D.,& Krstulović, N.. (2021). Laser ablation and chemical synthesis of bicomponent ZnO nanoparticles. in 27th International scientific meeting on vacuum science and technique : programme and the book of abstracts; September 9-10, Gozd Martuljek, Slovenia
Slovenia : Slovenian Society for Vacuum Technique., 26.
https://hdl.handle.net/21.15107/rcub_vinar_11526
Maletić D, Čebela M, Blažeka D, Radičić R, Pajić D, Krstulović N. Laser ablation and chemical synthesis of bicomponent ZnO nanoparticles. in 27th International scientific meeting on vacuum science and technique : programme and the book of abstracts; September 9-10, Gozd Martuljek, Slovenia. 2021;:26.
https://hdl.handle.net/21.15107/rcub_vinar_11526 .
Maletić, Dejan, Čebela, Maria, Blažeka, Damjan, Radičić, Rafaela, Pajić, Damir, Krstulović, Nikša, "Laser ablation and chemical synthesis of bicomponent ZnO nanoparticles" in 27th International scientific meeting on vacuum science and technique : programme and the book of abstracts; September 9-10, Gozd Martuljek, Slovenia (2021):26,
https://hdl.handle.net/21.15107/rcub_vinar_11526 .

Structural, magnetic and photocatalytic properties of ZnO nanopowder

Maletić, Dejan; Čebela, Maria; Blažeka, Damjan; Radičić, Rafaela; Šenjug, Pavla; Barišić, Dario; Pajić, Damir

(Belgrade : Serbian Ceramic Society, 2021)

TY  - CONF
AU  - Maletić, Dejan
AU  - Čebela, Maria
AU  - Blažeka, Damjan
AU  - Radičić, Rafaela
AU  - Šenjug, Pavla
AU  - Barišić, Dario
AU  - Pajić, Damir
PY  - 2021
UR  - https://vinar.vin.bg.ac.rs/handle/123456789/10837
AB  - Removal of organic pollutants from the waste water will bethemost challenging objective in the future. The photodegradation using the zinc oxide (ZnO)is one of the bestpromising material due to low price and high efficiency. Zinc oxide nanoparticles were synthetized by self propagatingroom temperature reaction of zincnitratewith sodium hydroxide.After reaction powder wascalcinated at 1100°C for 4 h in furnace. The diffraction patterns were recorded at room temperature and atmospheric pressure in the absence of any re-heating of the samples. The temperature dependence of magnetization was measured in the field of 1000 Oe and temperature range from 2 to 300 K using MPMS5 SQUID magnetometer. Photocatalytic properties were determined using the degradation of organic dye Methylene Blue (MB). Hg UV lap was used for irradiating the solution of MB and ZnOnanopowder. The photodegradation of MB was monitored by decreasing 664 nm peak during 120 min, after this period of time we observed 95% of reduction from the starting dye concentration. Nanopowder of ZnO show strong photocatalytic performance and can be used for further investigation and applications.
PB  - Belgrade : Serbian Ceramic Society
C3  - Advanced Ceramics and Application : 9th Serbian Ceramic Society Conference : program and the book of abstracts; September 20-21, 2021; Belgrade
T1  - Structural, magnetic and photocatalytic properties of ZnO nanopowder
SP  - 78
UR  - https://hdl.handle.net/21.15107/rcub_vinar_10837
ER  - 
@conference{
author = "Maletić, Dejan and Čebela, Maria and Blažeka, Damjan and Radičić, Rafaela and Šenjug, Pavla and Barišić, Dario and Pajić, Damir",
year = "2021",
abstract = "Removal of organic pollutants from the waste water will bethemost challenging objective in the future. The photodegradation using the zinc oxide (ZnO)is one of the bestpromising material due to low price and high efficiency. Zinc oxide nanoparticles were synthetized by self propagatingroom temperature reaction of zincnitratewith sodium hydroxide.After reaction powder wascalcinated at 1100°C for 4 h in furnace. The diffraction patterns were recorded at room temperature and atmospheric pressure in the absence of any re-heating of the samples. The temperature dependence of magnetization was measured in the field of 1000 Oe and temperature range from 2 to 300 K using MPMS5 SQUID magnetometer. Photocatalytic properties were determined using the degradation of organic dye Methylene Blue (MB). Hg UV lap was used for irradiating the solution of MB and ZnOnanopowder. The photodegradation of MB was monitored by decreasing 664 nm peak during 120 min, after this period of time we observed 95% of reduction from the starting dye concentration. Nanopowder of ZnO show strong photocatalytic performance and can be used for further investigation and applications.",
publisher = "Belgrade : Serbian Ceramic Society",
journal = "Advanced Ceramics and Application : 9th Serbian Ceramic Society Conference : program and the book of abstracts; September 20-21, 2021; Belgrade",
title = "Structural, magnetic and photocatalytic properties of ZnO nanopowder",
pages = "78",
url = "https://hdl.handle.net/21.15107/rcub_vinar_10837"
}
Maletić, D., Čebela, M., Blažeka, D., Radičić, R., Šenjug, P., Barišić, D.,& Pajić, D.. (2021). Structural, magnetic and photocatalytic properties of ZnO nanopowder. in Advanced Ceramics and Application : 9th Serbian Ceramic Society Conference : program and the book of abstracts; September 20-21, 2021; Belgrade
Belgrade : Serbian Ceramic Society., 78.
https://hdl.handle.net/21.15107/rcub_vinar_10837
Maletić D, Čebela M, Blažeka D, Radičić R, Šenjug P, Barišić D, Pajić D. Structural, magnetic and photocatalytic properties of ZnO nanopowder. in Advanced Ceramics and Application : 9th Serbian Ceramic Society Conference : program and the book of abstracts; September 20-21, 2021; Belgrade. 2021;:78.
https://hdl.handle.net/21.15107/rcub_vinar_10837 .
Maletić, Dejan, Čebela, Maria, Blažeka, Damjan, Radičić, Rafaela, Šenjug, Pavla, Barišić, Dario, Pajić, Damir, "Structural, magnetic and photocatalytic properties of ZnO nanopowder" in Advanced Ceramics and Application : 9th Serbian Ceramic Society Conference : program and the book of abstracts; September 20-21, 2021; Belgrade (2021):78,
https://hdl.handle.net/21.15107/rcub_vinar_10837 .