TY  - JOUR
AU  - Filipović, Suzana
AU  - Obradović, Nina
AU  - Fahrenholtz, William G.
AU  - Smith, Steven
AU  - Mirković, Miljana M.
AU  - Peleš Tadić, Adriana
AU  - Petrović, Jovana
AU  - Đorđević, Antonije
PY  - 2024
UR  - https://vinar.vin.bg.ac.rs/handle/123456789/12795
AB  - Magnesium titanate ceramics were prepared by reactive spark plasma sintering (SPS) at 1200 °C for 5 min. Prior to sintering, MgO and TiO2 powders were mixed by high energy ball milling (HEBM) for 15, 30, or 60 min. The effect of milling time on phase composition was analyzed by X-ray diffraction (XRD) for milled powders and sintered specimens. The morphology of the sintered ceramics was investigated by scanning electron microscopy (SEM), while elemental distribution was determined by energy dispersive spectroscopy (EDS). The presence of the MgTi2O5 phase was detected in XRD and was confirmed by EDS analysis. Microcracking was observed for specimens prepared with longer milling times and attributed to the coefficient of thermal expansion (CTE) mismatch dominantly due to the anisotropic crystal structure of MgTiO3 phase. The sample milled for 15 min showed the highest Vickers hardness due to less or no microcracking and nearly full density. The dielectric measurements in the range of 10 Hz–250 MHz demonstrated extremely high dielectric permittivity, as high as 104 at 1 kHz. An increase in loss tangents was observed due to oxygen vacancy formation, which was promoted by the vacuum environment during SPS. Oxygen vacancy-related dielectric relaxation was also detected and explained.
T2  - Ceramics International
T1  - Spark plasma sintering of magnesium titanate ceramics
IS  - InPress
DO  - 10.1016/j.ceramint.2024.02.004
ER  - 

@article{
author = "Filipović, Suzana and Obradović, Nina and Fahrenholtz, William G. and Smith, Steven and Mirković, Miljana M. and Peleš Tadić, Adriana and Petrović, Jovana and Đorđević, Antonije",
year = "2024",
abstract = "Magnesium titanate ceramics were prepared by reactive spark plasma sintering (SPS) at 1200 °C for 5 min. Prior to sintering, MgO and TiO2 powders were mixed by high energy ball milling (HEBM) for 15, 30, or 60 min. The effect of milling time on phase composition was analyzed by X-ray diffraction (XRD) for milled powders and sintered specimens. The morphology of the sintered ceramics was investigated by scanning electron microscopy (SEM), while elemental distribution was determined by energy dispersive spectroscopy (EDS). The presence of the MgTi2O5 phase was detected in XRD and was confirmed by EDS analysis. Microcracking was observed for specimens prepared with longer milling times and attributed to the coefficient of thermal expansion (CTE) mismatch dominantly due to the anisotropic crystal structure of MgTiO3 phase. The sample milled for 15 min showed the highest Vickers hardness due to less or no microcracking and nearly full density. The dielectric measurements in the range of 10 Hz–250 MHz demonstrated extremely high dielectric permittivity, as high as 104 at 1 kHz. An increase in loss tangents was observed due to oxygen vacancy formation, which was promoted by the vacuum environment during SPS. Oxygen vacancy-related dielectric relaxation was also detected and explained.",
journal = "Ceramics International",
title = "Spark plasma sintering of magnesium titanate ceramics",
number = "InPress",
doi = "10.1016/j.ceramint.2024.02.004"
}

Filipović, S., Obradović, N., Fahrenholtz, W. G., Smith, S., Mirković, M. M., Peleš Tadić, A., Petrović, J.,& Đorđević, A.. (2024). Spark plasma sintering of magnesium titanate ceramics. in Ceramics International(InPress).
https://doi.org/10.1016/j.ceramint.2024.02.004

Filipović S, Obradović N, Fahrenholtz WG, Smith S, Mirković MM, Peleš Tadić A, Petrović J, Đorđević A. Spark plasma sintering of magnesium titanate ceramics. in Ceramics International. 2024;(InPress).
doi:10.1016/j.ceramint.2024.02.004 .

Filipović, Suzana, Obradović, Nina, Fahrenholtz, William G., Smith, Steven, Mirković, Miljana M., Peleš Tadić, Adriana, Petrović, Jovana, Đorđević, Antonije, "Spark plasma sintering of magnesium titanate ceramics" in Ceramics International, no. InPress (2024),
https://doi.org/10.1016/j.ceramint.2024.02.004 . .

TY  - JOUR
AU  - Filipović, Suzana
AU  - Obradović, Nina
AU  - Corlett, Cole
AU  - Fahrenholtz, William G.
AU  - Rosenschon, Martin
AU  - Füglein, Ekkehard
AU  - Dojčilović, Radovan
AU  - Tošić, Dragana
AU  - Petrović, Jovana
AU  - Đorđević, Antonije
AU  - Vlahović, Branislav
AU  - Pavlović, Vladimir B.
PY  - 2023
UR  - https://vinar.vin.bg.ac.rs/handle/123456789/12400
AB  - Ceramic/polymer composites can be chemically stable, mechanically strong, and flexible, which make them candidates for electric devices, such as pressure or temperature sensors, energy storage or harvesting devices, actuators, and so forth. Depending on the application, various electrical properties are of importance. Polymers usually have low dielectric permittivity, but increased dielectric permittivity can be achieved by the addition of the ceramic fillers with high dielectric constant. With the aim to enhance dielectric properties of the composite without loss of flexibility, 5 wt% of BaTiO3-Fe2O3 powder was added into a polyvinylidene fluoride matrix. The powder was prepared by different synthesis conditions to produce core/shell structures. The effect of the phase composition and morphology of the BaTiO3-Fe2O3 core/shell filler on the structure and lattice dynamics of the polymer composites was investigated. Based on the results of the thermal analysis, various parameters of ceramic/polymer composites were determined. Differences in the phase composition and morphology of the filler have an influence on the formation of various polyvinylidene fluoride allomorphs and the degree of crystallinity. Furthermore, the dielectric performances of pure polyvinylidene fluoride and the polymer/ceramic composites were measured.
T2  - Journal of Applied Polymer Science
T1  - Effect of the filler morphology on the crystallization behavior and dielectric properties of the polyvinylidene fluoride‐based composite
DO  - 10.1002/app.55040
ER  - 

@article{
author = "Filipović, Suzana and Obradović, Nina and Corlett, Cole and Fahrenholtz, William G. and Rosenschon, Martin and Füglein, Ekkehard and Dojčilović, Radovan and Tošić, Dragana and Petrović, Jovana and Đorđević, Antonije and Vlahović, Branislav and Pavlović, Vladimir B.",
year = "2023",
abstract = "Ceramic/polymer composites can be chemically stable, mechanically strong, and flexible, which make them candidates for electric devices, such as pressure or temperature sensors, energy storage or harvesting devices, actuators, and so forth. Depending on the application, various electrical properties are of importance. Polymers usually have low dielectric permittivity, but increased dielectric permittivity can be achieved by the addition of the ceramic fillers with high dielectric constant. With the aim to enhance dielectric properties of the composite without loss of flexibility, 5 wt% of BaTiO3-Fe2O3 powder was added into a polyvinylidene fluoride matrix. The powder was prepared by different synthesis conditions to produce core/shell structures. The effect of the phase composition and morphology of the BaTiO3-Fe2O3 core/shell filler on the structure and lattice dynamics of the polymer composites was investigated. Based on the results of the thermal analysis, various parameters of ceramic/polymer composites were determined. Differences in the phase composition and morphology of the filler have an influence on the formation of various polyvinylidene fluoride allomorphs and the degree of crystallinity. Furthermore, the dielectric performances of pure polyvinylidene fluoride and the polymer/ceramic composites were measured.",
journal = "Journal of Applied Polymer Science",
title = "Effect of the filler morphology on the crystallization behavior and dielectric properties of the polyvinylidene fluoride‐based composite",
doi = "10.1002/app.55040"
}

Filipović, S., Obradović, N., Corlett, C., Fahrenholtz, W. G., Rosenschon, M., Füglein, E., Dojčilović, R., Tošić, D., Petrović, J., Đorđević, A., Vlahović, B.,& Pavlović, V. B.. (2023). Effect of the filler morphology on the crystallization behavior and dielectric properties of the polyvinylidene fluoride‐based composite. in Journal of Applied Polymer Science.
https://doi.org/10.1002/app.55040

Filipović S, Obradović N, Corlett C, Fahrenholtz WG, Rosenschon M, Füglein E, Dojčilović R, Tošić D, Petrović J, Đorđević A, Vlahović B, Pavlović VB. Effect of the filler morphology on the crystallization behavior and dielectric properties of the polyvinylidene fluoride‐based composite. in Journal of Applied Polymer Science. 2023;.
doi:10.1002/app.55040 .

Filipović, Suzana, Obradović, Nina, Corlett, Cole, Fahrenholtz, William G., Rosenschon, Martin, Füglein, Ekkehard, Dojčilović, Radovan, Tošić, Dragana, Petrović, Jovana, Đorđević, Antonije, Vlahović, Branislav, Pavlović, Vladimir B., "Effect of the filler morphology on the crystallization behavior and dielectric properties of the polyvinylidene fluoride‐based composite" in Journal of Applied Polymer Science (2023),
https://doi.org/10.1002/app.55040 . .

TY  - CONF
AU  - Filipović, Suzana
AU  - Obradović, Nina
AU  - Fahrenholtz, William G.
AU  - Smith, Steven
AU  - Mirković, M.
AU  - Peleš, Adriana
AU  - Tadić, Nenad
AU  - Đorđević, Antonije
PY  - 2022
UR  - https://vinar.vin.bg.ac.rs/handle/123456789/10825
AB  - Perovskite ceramic material based on MgTiO3 is used in various types of electronic devices owing to its dielectric properties, high dielectric constant, and low losses. These features can be tailored by setting preparation conditions. Densification of magnesium titanate by Spark Plasma Sintering (SPS) was the aim of this work. First, the mechanical activation in the highenergy ball mill was applied on the powder of MgO-TiO2 mixed in mole ratio 1:1. Prepared powder mixtures, activated for different times, were SPS sintered, at 1200 o C with a heating rate of 100o C/min. After reaching the desired temperature, a uniaxial pressure of 50 MPa was applied, and dwelled at this condition for 5 min, followed by cooling to room temperature at 5o C/min. The starting powders, activated mixtures, and sintered ceramics bodies were investigated by X-ray diffraction, scanning electron microscopy (SEM), and energy dispersive spectroscopy (EDS). The presence of the MgTi2O5 phase was noticed for the nonmilled ceramics. In the samples obtained from milled powders, MgTi2O5 was detected in EDS spectra in a lower amount, below the threshold of the XRD method. Dielectric measurements were performed at a wide range of frequencies and temperatures. The highest value of the hardness was obtained from powder milled for 15 min before SPS.
PB  - Belgrade : Serbian Ceramic Society
C3  - Advanced Ceramics and Application : 10th Serbian Ceramic Society Conference : program and the book of abstracts; September 26-27, 2022; Belgrade
T1  - Effect of high energy ball milling on sintering of MgO-TiO2 system
SP  - 88
UR  - https://hdl.handle.net/21.15107/rcub_vinar_10825
ER  - 

@conference{
author = "Filipović, Suzana and Obradović, Nina and Fahrenholtz, William G. and Smith, Steven and Mirković, M. and Peleš, Adriana and Tadić, Nenad and Đorđević, Antonije",
year = "2022",
abstract = "Perovskite ceramic material based on MgTiO3 is used in various types of electronic devices owing to its dielectric properties, high dielectric constant, and low losses. These features can be tailored by setting preparation conditions. Densification of magnesium titanate by Spark Plasma Sintering (SPS) was the aim of this work. First, the mechanical activation in the highenergy ball mill was applied on the powder of MgO-TiO2 mixed in mole ratio 1:1. Prepared powder mixtures, activated for different times, were SPS sintered, at 1200 o C with a heating rate of 100o C/min. After reaching the desired temperature, a uniaxial pressure of 50 MPa was applied, and dwelled at this condition for 5 min, followed by cooling to room temperature at 5o C/min. The starting powders, activated mixtures, and sintered ceramics bodies were investigated by X-ray diffraction, scanning electron microscopy (SEM), and energy dispersive spectroscopy (EDS). The presence of the MgTi2O5 phase was noticed for the nonmilled ceramics. In the samples obtained from milled powders, MgTi2O5 was detected in EDS spectra in a lower amount, below the threshold of the XRD method. Dielectric measurements were performed at a wide range of frequencies and temperatures. The highest value of the hardness was obtained from powder milled for 15 min before SPS.",
publisher = "Belgrade : Serbian Ceramic Society",
journal = "Advanced Ceramics and Application : 10th Serbian Ceramic Society Conference : program and the book of abstracts; September 26-27, 2022; Belgrade",
title = "Effect of high energy ball milling on sintering of MgO-TiO2 system",
pages = "88",
url = "https://hdl.handle.net/21.15107/rcub_vinar_10825"
}

Filipović, S., Obradović, N., Fahrenholtz, W. G., Smith, S., Mirković, M., Peleš, A., Tadić, N.,& Đorđević, A.. (2022). Effect of high energy ball milling on sintering of MgO-TiO2 system. in Advanced Ceramics and Application : 10th Serbian Ceramic Society Conference : program and the book of abstracts; September 26-27, 2022; Belgrade
Belgrade : Serbian Ceramic Society., 88.
https://hdl.handle.net/21.15107/rcub_vinar_10825

Filipović S, Obradović N, Fahrenholtz WG, Smith S, Mirković M, Peleš A, Tadić N, Đorđević A. Effect of high energy ball milling on sintering of MgO-TiO2 system. in Advanced Ceramics and Application : 10th Serbian Ceramic Society Conference : program and the book of abstracts; September 26-27, 2022; Belgrade. 2022;:88.
https://hdl.handle.net/21.15107/rcub_vinar_10825 .

Filipović, Suzana, Obradović, Nina, Fahrenholtz, William G., Smith, Steven, Mirković, M., Peleš, Adriana, Tadić, Nenad, Đorđević, Antonije, "Effect of high energy ball milling on sintering of MgO-TiO2 system" in Advanced Ceramics and Application : 10th Serbian Ceramic Society Conference : program and the book of abstracts; September 26-27, 2022; Belgrade (2022):88,
https://hdl.handle.net/21.15107/rcub_vinar_10825 .

TY  - CONF
AU  - Stojanović, Nemanja
AU  - Kalezić-Glišović, Aleksandra
AU  - Obradović, Nina
AU  - Lojpur, Vesna
AU  - Kesić, Željka
AU  - Maričić, Aleksa
PY  - 2022
UR  - https://vinar.vin.bg.ac.rs/handle/123456789/10826
AB  - Refractory devices composed of ceramics are employed wherever there is contact with molten metals as in crucibles filters, furnaces or systems for flow control. The mechanical properties of these materials are very different from metals. The presentation focuses on basic equations related to thermal and mechanical transmission conditions across an interface between two different materials. These equations are linked to the development of material instabilities and crack propagation within the ceramics, in the view of application to refractories operating at high-temperature conditions in steel plants.
PB  - Belgrade : Serbian Ceramic Society
C3  - Advanced Ceramics and Application : 10th Serbian Ceramic Society Conference : program and the book of abstracts; September 26-27, 2022; Belgrade
T1  - Piezoelectric And Pyroelectric Properties Of Fe/Pb/Zr-co-doped Barium Titanate Ceramics
SP  - 91
UR  - https://hdl.handle.net/21.15107/rcub_vinar_10826
ER  - 

@conference{
author = "Stojanović, Nemanja and Kalezić-Glišović, Aleksandra and Obradović, Nina and Lojpur, Vesna and Kesić, Željka and Maričić, Aleksa",
year = "2022",
abstract = "Refractory devices composed of ceramics are employed wherever there is contact with molten metals as in crucibles filters, furnaces or systems for flow control. The mechanical properties of these materials are very different from metals. The presentation focuses on basic equations related to thermal and mechanical transmission conditions across an interface between two different materials. These equations are linked to the development of material instabilities and crack propagation within the ceramics, in the view of application to refractories operating at high-temperature conditions in steel plants.",
publisher = "Belgrade : Serbian Ceramic Society",
journal = "Advanced Ceramics and Application : 10th Serbian Ceramic Society Conference : program and the book of abstracts; September 26-27, 2022; Belgrade",
title = "Piezoelectric And Pyroelectric Properties Of Fe/Pb/Zr-co-doped Barium Titanate Ceramics",
pages = "91",
url = "https://hdl.handle.net/21.15107/rcub_vinar_10826"
}

Stojanović, N., Kalezić-Glišović, A., Obradović, N., Lojpur, V., Kesić, Ž.,& Maričić, A.. (2022). Piezoelectric And Pyroelectric Properties Of Fe/Pb/Zr-co-doped Barium Titanate Ceramics. in Advanced Ceramics and Application : 10th Serbian Ceramic Society Conference : program and the book of abstracts; September 26-27, 2022; Belgrade
Belgrade : Serbian Ceramic Society., 91.
https://hdl.handle.net/21.15107/rcub_vinar_10826

Stojanović N, Kalezić-Glišović A, Obradović N, Lojpur V, Kesić Ž, Maričić A. Piezoelectric And Pyroelectric Properties Of Fe/Pb/Zr-co-doped Barium Titanate Ceramics. in Advanced Ceramics and Application : 10th Serbian Ceramic Society Conference : program and the book of abstracts; September 26-27, 2022; Belgrade. 2022;:91.
https://hdl.handle.net/21.15107/rcub_vinar_10826 .

Stojanović, Nemanja, Kalezić-Glišović, Aleksandra, Obradović, Nina, Lojpur, Vesna, Kesić, Željka, Maričić, Aleksa, "Piezoelectric And Pyroelectric Properties Of Fe/Pb/Zr-co-doped Barium Titanate Ceramics" in Advanced Ceramics and Application : 10th Serbian Ceramic Society Conference : program and the book of abstracts; September 26-27, 2022; Belgrade (2022):91,
https://hdl.handle.net/21.15107/rcub_vinar_10826 .

TY  - CONF
AU  - Stojanović, Nemanja
AU  - Zagorac, Dejan
AU  - Butulija, Svetlana
AU  - Lojpur, Vesna
AU  - Kalezić-Glišović, Aleksandra
AU  - Obradović, Nina
AU  - Maričić, Aleksa
PY  - 2021
UR  - https://vinar.vin.bg.ac.rs/handle/123456789/10836
AB  - Mixtures of high purity powders of 50 mass% Fe, 4 mass% Pb, 3 mass% Zr and 43 mass% BaTiO3 were activated in a rotary ball mill for durations ranging from 30 min to 300 min; samples were then sintered in the air atmosphere for 2 hours at 1200 °C. Crystal structure prediction has been performed using Bond ValenceCalculation (BVC) method.Moreover, theoretical stability of theperovskite structure for synthesized and calculated Fe/Pb/Zr-co- doped barium titanatecompounds has been investigated using the Goldschmidttolerance factor (Gt) and global instability index (GII).It was observed that magnetization of the system decreased after the sintering, with the most dramatic drop of 90.11% belonging to the sample activated for 150 min. In comparison with initial powders, X-ray powder diffractiondata confirmed the presence of newphases of BaFe 12 O19 and Ba1.696 Ti0.228 O3 in sintered samples. Utilizing the field emission scanning electron microscopy (FESEM), it was found that with the increase of activation time the morphology of the samples progressed from irregural, spherical grains to mostly rod-like ones. Energy dispersive X-ray (EDX) analysis identified the presence of Pb and Zr occupying the same locations on the surface of sintered samples, whilst Fe was uniformly deployed regardless of the activation time.
PB  - Belgrade : Serbian Ceramic Society
C3  - Advanced Ceramics and Application : 9th Serbian Ceramic Society Conference : program and the book of abstracts; September 20-21, 2021; Belgrade
T1  - Structural And Functional Investigation Of Fe/Pb/Zr-co-doped Barium Titanate Ceramics: From Theory To The Experiment
SP  - 77
UR  - https://hdl.handle.net/21.15107/rcub_vinar_10836
ER  - 

@conference{
author = "Stojanović, Nemanja and Zagorac, Dejan and Butulija, Svetlana and Lojpur, Vesna and Kalezić-Glišović, Aleksandra and Obradović, Nina and Maričić, Aleksa",
year = "2021",
abstract = "Mixtures of high purity powders of 50 mass% Fe, 4 mass% Pb, 3 mass% Zr and 43 mass% BaTiO3 were activated in a rotary ball mill for durations ranging from 30 min to 300 min; samples were then sintered in the air atmosphere for 2 hours at 1200 °C. Crystal structure prediction has been performed using Bond ValenceCalculation (BVC) method.Moreover, theoretical stability of theperovskite structure for synthesized and calculated Fe/Pb/Zr-co- doped barium titanatecompounds has been investigated using the Goldschmidttolerance factor (Gt) and global instability index (GII).It was observed that magnetization of the system decreased after the sintering, with the most dramatic drop of 90.11% belonging to the sample activated for 150 min. In comparison with initial powders, X-ray powder diffractiondata confirmed the presence of newphases of BaFe 12 O19 and Ba1.696 Ti0.228 O3 in sintered samples. Utilizing the field emission scanning electron microscopy (FESEM), it was found that with the increase of activation time the morphology of the samples progressed from irregural, spherical grains to mostly rod-like ones. Energy dispersive X-ray (EDX) analysis identified the presence of Pb and Zr occupying the same locations on the surface of sintered samples, whilst Fe was uniformly deployed regardless of the activation time.",
publisher = "Belgrade : Serbian Ceramic Society",
journal = "Advanced Ceramics and Application : 9th Serbian Ceramic Society Conference : program and the book of abstracts; September 20-21, 2021; Belgrade",
title = "Structural And Functional Investigation Of Fe/Pb/Zr-co-doped Barium Titanate Ceramics: From Theory To The Experiment",
pages = "77",
url = "https://hdl.handle.net/21.15107/rcub_vinar_10836"
}

Stojanović, N., Zagorac, D., Butulija, S., Lojpur, V., Kalezić-Glišović, A., Obradović, N.,& Maričić, A.. (2021). Structural And Functional Investigation Of Fe/Pb/Zr-co-doped Barium Titanate Ceramics: From Theory To The Experiment. in Advanced Ceramics and Application : 9th Serbian Ceramic Society Conference : program and the book of abstracts; September 20-21, 2021; Belgrade
Belgrade : Serbian Ceramic Society., 77.
https://hdl.handle.net/21.15107/rcub_vinar_10836

Stojanović N, Zagorac D, Butulija S, Lojpur V, Kalezić-Glišović A, Obradović N, Maričić A. Structural And Functional Investigation Of Fe/Pb/Zr-co-doped Barium Titanate Ceramics: From Theory To The Experiment. in Advanced Ceramics and Application : 9th Serbian Ceramic Society Conference : program and the book of abstracts; September 20-21, 2021; Belgrade. 2021;:77.
https://hdl.handle.net/21.15107/rcub_vinar_10836 .

Stojanović, Nemanja, Zagorac, Dejan, Butulija, Svetlana, Lojpur, Vesna, Kalezić-Glišović, Aleksandra, Obradović, Nina, Maričić, Aleksa, "Structural And Functional Investigation Of Fe/Pb/Zr-co-doped Barium Titanate Ceramics: From Theory To The Experiment" in Advanced Ceramics and Application : 9th Serbian Ceramic Society Conference : program and the book of abstracts; September 20-21, 2021; Belgrade (2021):77,
https://hdl.handle.net/21.15107/rcub_vinar_10836 .

TY  - JOUR
AU  - Filipović, Suzana
AU  - Obradović, Nina
AU  - Anđelković, Ljubica
AU  - Olćan, Dragan
AU  - Petrović, Jovana S.
AU  - Mirković, Miljana M.
AU  - Pavlović, Vladimir B.
AU  - Jeremić, Dejan
AU  - Vlahović, Branislav
AU  - Đorđević, Antonije
PY  - 2021
UR  - https://vinar.vin.bg.ac.rs/handle/123456789/9410
AB  - Solid-state reaction between BaTiO3and Fe2O3was used to produce a multiferroic heterostructure composite. Commercial BaTiO3and Fe(NO3)3•9H2O were suspended in ethanol for 30 minutes in an ultrasound bath. The prepared mixture was thermally processed at 300°C for 6 h. Sintering at 1300 °C for 1 h resulted in a mixture of different phases, BaTiO3, BaFe12O19and Ba12Ti28Fe15O84, which were confirmed by x-ray powder diffraction. A dense microstructure with a small volume fraction of closed porosity was indicated by the scanning electron microscopy, while a homogeneous distribution of Fe ions over BaTiO3phase was visible from energy dispersive spectroscopy mapping. Doping of BaTiO3with Fe2O3resulted in formation of magnetic hexaferrite phases, as confirmed by dielectric measurements that showed a broadened maximum of the permittivity measured as a function of temperature. © 2021 Authors. Published by association for ETRAN Society.
T2  - Science of Sintering
T1  - Multiferroic heterostructure BaTiO3/ε-Fe2O3 composite obtained by in situ reaction
VL  - 53
IS  - 1
SP  - 1
EP  - 8
DO  - 10.2298/SOS2101001F
ER  - 

@article{
author = "Filipović, Suzana and Obradović, Nina and Anđelković, Ljubica and Olćan, Dragan and Petrović, Jovana S. and Mirković, Miljana M. and Pavlović, Vladimir B. and Jeremić, Dejan and Vlahović, Branislav and Đorđević, Antonije",
year = "2021",
abstract = "Solid-state reaction between BaTiO3and Fe2O3was used to produce a multiferroic heterostructure composite. Commercial BaTiO3and Fe(NO3)3•9H2O were suspended in ethanol for 30 minutes in an ultrasound bath. The prepared mixture was thermally processed at 300°C for 6 h. Sintering at 1300 °C for 1 h resulted in a mixture of different phases, BaTiO3, BaFe12O19and Ba12Ti28Fe15O84, which were confirmed by x-ray powder diffraction. A dense microstructure with a small volume fraction of closed porosity was indicated by the scanning electron microscopy, while a homogeneous distribution of Fe ions over BaTiO3phase was visible from energy dispersive spectroscopy mapping. Doping of BaTiO3with Fe2O3resulted in formation of magnetic hexaferrite phases, as confirmed by dielectric measurements that showed a broadened maximum of the permittivity measured as a function of temperature. © 2021 Authors. Published by association for ETRAN Society.",
journal = "Science of Sintering",
title = "Multiferroic heterostructure BaTiO3/ε-Fe2O3 composite obtained by in situ reaction",
volume = "53",
number = "1",
pages = "1-8",
doi = "10.2298/SOS2101001F"
}

Filipović, S., Obradović, N., Anđelković, L., Olćan, D., Petrović, J. S., Mirković, M. M., Pavlović, V. B., Jeremić, D., Vlahović, B.,& Đorđević, A.. (2021). Multiferroic heterostructure BaTiO3/ε-Fe2O3 composite obtained by in situ reaction. in Science of Sintering, 53(1), 1-8.
https://doi.org/10.2298/SOS2101001F

Filipović S, Obradović N, Anđelković L, Olćan D, Petrović JS, Mirković MM, Pavlović VB, Jeremić D, Vlahović B, Đorđević A. Multiferroic heterostructure BaTiO3/ε-Fe2O3 composite obtained by in situ reaction. in Science of Sintering. 2021;53(1):1-8.
doi:10.2298/SOS2101001F .

Filipović, Suzana, Obradović, Nina, Anđelković, Ljubica, Olćan, Dragan, Petrović, Jovana S., Mirković, Miljana M., Pavlović, Vladimir B., Jeremić, Dejan, Vlahović, Branislav, Đorđević, Antonije, "Multiferroic heterostructure BaTiO3/ε-Fe2O3 composite obtained by in situ reaction" in Science of Sintering, 53, no. 1 (2021):1-8,
https://doi.org/10.2298/SOS2101001F . .

TY  - CONF
AU  - Filipović, Suzana
AU  - Obradović, Nina
AU  - Rosenschon, M.
AU  - Füglein, E.
AU  - Dojčilović, Radovan
AU  - Đorđević, Antonije
AU  - Petrović, J.
AU  - Pavlović, Vladimir B.
PY  - 2021
UR  - https://vinar.vin.bg.ac.rs/handle/123456789/10796
AB  - The increase in the utilization of ceramic/polymer composites as components for electric devices is mainly based on their high chemical stability, mechanical strength, and flexibility. The polymers usually have poor dielectric performances. In order to increase the dielectric permittivity, ceramic fillers with high dielectric constant have been used as active fillers, and usually in large amounts, which have a detrimental effect on the mechanical properties of the composite. With the aim to enhance the dielectric properties of the composite without loss of polymer’s flexibility, 5 wt.% of BaTiO3/Fe2O3 core/shell powders, prepared by different synthesis conditions, was added into the PVDF matrix. The effect of the phase composition and morphology of the starting BaTiO3/Fe2O3 core/shell filler on the crystal structure and lattice dynamics was investigated. Based on the results of the thermal analysis, TG/DSC, various parameters of ceramic/polymer composites were determined. We were able to corroborate that differences in the phase composition and morphology of BaTiO3/Fe2O3 core/shell filler have an influence on the formation of various PVDF allomorph modifications, as well as the level of crystallinity. The dielectric performances of the pure PVDF and polymer/ceramic composites were measured. An enhancement in the dielectric permittivity and decrease in the loss tangent were revealed.
PB  - Belgrade : Serbian Ceramic Society
C3  - Advanced Ceramics and Application : 9th Serbian Ceramic Society Conference : program and the book of abstracts; September 20-21, 2021; Belgrade
T1  - Enhanced dielectric properties of PVDF-based composites with BaTiO3 ceramic decorated with Fe2O3
SP  - 58
UR  - https://hdl.handle.net/21.15107/rcub_vinar_10796
ER  - 

@conference{
author = "Filipović, Suzana and Obradović, Nina and Rosenschon, M. and Füglein, E. and Dojčilović, Radovan and Đorđević, Antonije and Petrović, J. and Pavlović, Vladimir B.",
year = "2021",
abstract = "The increase in the utilization of ceramic/polymer composites as components for electric devices is mainly based on their high chemical stability, mechanical strength, and flexibility. The polymers usually have poor dielectric performances. In order to increase the dielectric permittivity, ceramic fillers with high dielectric constant have been used as active fillers, and usually in large amounts, which have a detrimental effect on the mechanical properties of the composite. With the aim to enhance the dielectric properties of the composite without loss of polymer’s flexibility, 5 wt.% of BaTiO3/Fe2O3 core/shell powders, prepared by different synthesis conditions, was added into the PVDF matrix. The effect of the phase composition and morphology of the starting BaTiO3/Fe2O3 core/shell filler on the crystal structure and lattice dynamics was investigated. Based on the results of the thermal analysis, TG/DSC, various parameters of ceramic/polymer composites were determined. We were able to corroborate that differences in the phase composition and morphology of BaTiO3/Fe2O3 core/shell filler have an influence on the formation of various PVDF allomorph modifications, as well as the level of crystallinity. The dielectric performances of the pure PVDF and polymer/ceramic composites were measured. An enhancement in the dielectric permittivity and decrease in the loss tangent were revealed.",
publisher = "Belgrade : Serbian Ceramic Society",
journal = "Advanced Ceramics and Application : 9th Serbian Ceramic Society Conference : program and the book of abstracts; September 20-21, 2021; Belgrade",
title = "Enhanced dielectric properties of PVDF-based composites with BaTiO3 ceramic decorated with Fe2O3",
pages = "58",
url = "https://hdl.handle.net/21.15107/rcub_vinar_10796"
}

Filipović, S., Obradović, N., Rosenschon, M., Füglein, E., Dojčilović, R., Đorđević, A., Petrović, J.,& Pavlović, V. B.. (2021). Enhanced dielectric properties of PVDF-based composites with BaTiO3 ceramic decorated with Fe2O3. in Advanced Ceramics and Application : 9th Serbian Ceramic Society Conference : program and the book of abstracts; September 20-21, 2021; Belgrade
Belgrade : Serbian Ceramic Society., 58.
https://hdl.handle.net/21.15107/rcub_vinar_10796

Filipović S, Obradović N, Rosenschon M, Füglein E, Dojčilović R, Đorđević A, Petrović J, Pavlović VB. Enhanced dielectric properties of PVDF-based composites with BaTiO3 ceramic decorated with Fe2O3. in Advanced Ceramics and Application : 9th Serbian Ceramic Society Conference : program and the book of abstracts; September 20-21, 2021; Belgrade. 2021;:58.
https://hdl.handle.net/21.15107/rcub_vinar_10796 .

Filipović, Suzana, Obradović, Nina, Rosenschon, M., Füglein, E., Dojčilović, Radovan, Đorđević, Antonije, Petrović, J., Pavlović, Vladimir B., "Enhanced dielectric properties of PVDF-based composites with BaTiO3 ceramic decorated with Fe2O3" in Advanced Ceramics and Application : 9th Serbian Ceramic Society Conference : program and the book of abstracts; September 20-21, 2021; Belgrade (2021):58,
https://hdl.handle.net/21.15107/rcub_vinar_10796 .

TY  - JOUR
AU  - Rusmirović, Jelena D.
AU  - Obradović, Nina
AU  - Perendija, Jovana
AU  - Umićević, Ana
AU  - Kapidžić, Ana
AU  - Vlahović, Branislav
AU  - Pavlović, Vera P.
AU  - Marinković, Aleksandar D.
AU  - Pavlović, Vladimir B.
PY  - 2019
UR  - https://vinar.vin.bg.ac.rs/handle/123456789/8096
AB  - Iron oxide, in the form of magnetite (MG)–functionalized porous wollastonite (WL), was used as an adsorbent for heavy metal ions (cadmium and nickel) and oxyanions (chromate and phosphate) removal from water. The porous WL was synthesized from calcium carbonate and siloxane by controlled sintering process using low molecular weight submicrosized poly(methyl methacrylate) as a pore-forming agent. The precipitation of MG nanoparticles was carried out directly by a polyol-medium solvothermal method or via branched amino/carboxylic acid cross-linker by solvent/nonsolvent method producing WL/MG and WL-?-APS/MG adsorbents, respectively. The structure/properties of MG functionalized WL was confirmed by applying FTIR, Raman, XRD, Mössbauer, and SEM analysis. Higher adsorption capacities of 73.126, 66.144, 64.168, and 63.456 mg g -1 for WL-?-APS/MG in relation to WL/MG of 55.450, 52.019, 48.132, and 47.382 mg g -1 for Cd 2+ , Ni 2+ , phosphate, and chromate, respectively, were obtained using nonlinear Langmuir model fitting. Adsorption phenomena were analyzed using monolayer statistical physics model for single adsorption with one energy. Kinetic study showed exceptionally higher pseudo-second-order rate constants for WL-?-APS/MG, e.g., 1.17–13.4 times, with respect to WL/MG indicating importance of both WL surface modification and controllable precipitation of MG on WL-?-APS. © 2019, Springer-Verlag GmbH Germany, part of Springer Nature.
T2  - Environmental Science and Pollution Research
T1  - Controllable synthesis of Fe3O4-wollastonite adsorbents for efficient heavy metal ions/oxyanions removal
VL  - 26
IS  - 12
SP  - 12379
EP  - 12398
DO  - 10.1007/s11356-019-04625-0
ER  - 

@article{
author = "Rusmirović, Jelena D. and Obradović, Nina and Perendija, Jovana and Umićević, Ana and Kapidžić, Ana and Vlahović, Branislav and Pavlović, Vera P. and Marinković, Aleksandar D. and Pavlović, Vladimir B.",
year = "2019",
abstract = "Iron oxide, in the form of magnetite (MG)–functionalized porous wollastonite (WL), was used as an adsorbent for heavy metal ions (cadmium and nickel) and oxyanions (chromate and phosphate) removal from water. The porous WL was synthesized from calcium carbonate and siloxane by controlled sintering process using low molecular weight submicrosized poly(methyl methacrylate) as a pore-forming agent. The precipitation of MG nanoparticles was carried out directly by a polyol-medium solvothermal method or via branched amino/carboxylic acid cross-linker by solvent/nonsolvent method producing WL/MG and WL-?-APS/MG adsorbents, respectively. The structure/properties of MG functionalized WL was confirmed by applying FTIR, Raman, XRD, Mössbauer, and SEM analysis. Higher adsorption capacities of 73.126, 66.144, 64.168, and 63.456 mg g -1 for WL-?-APS/MG in relation to WL/MG of 55.450, 52.019, 48.132, and 47.382 mg g -1 for Cd 2+ , Ni 2+ , phosphate, and chromate, respectively, were obtained using nonlinear Langmuir model fitting. Adsorption phenomena were analyzed using monolayer statistical physics model for single adsorption with one energy. Kinetic study showed exceptionally higher pseudo-second-order rate constants for WL-?-APS/MG, e.g., 1.17–13.4 times, with respect to WL/MG indicating importance of both WL surface modification and controllable precipitation of MG on WL-?-APS. © 2019, Springer-Verlag GmbH Germany, part of Springer Nature.",
journal = "Environmental Science and Pollution Research",
title = "Controllable synthesis of Fe3O4-wollastonite adsorbents for efficient heavy metal ions/oxyanions removal",
volume = "26",
number = "12",
pages = "12379-12398",
doi = "10.1007/s11356-019-04625-0"
}

Rusmirović, J. D., Obradović, N., Perendija, J., Umićević, A., Kapidžić, A., Vlahović, B., Pavlović, V. P., Marinković, A. D.,& Pavlović, V. B.. (2019). Controllable synthesis of Fe3O4-wollastonite adsorbents for efficient heavy metal ions/oxyanions removal. in Environmental Science and Pollution Research, 26(12), 12379-12398.
https://doi.org/10.1007/s11356-019-04625-0

Rusmirović JD, Obradović N, Perendija J, Umićević A, Kapidžić A, Vlahović B, Pavlović VP, Marinković AD, Pavlović VB. Controllable synthesis of Fe3O4-wollastonite adsorbents for efficient heavy metal ions/oxyanions removal. in Environmental Science and Pollution Research. 2019;26(12):12379-12398.
doi:10.1007/s11356-019-04625-0 .

Rusmirović, Jelena D., Obradović, Nina, Perendija, Jovana, Umićević, Ana, Kapidžić, Ana, Vlahović, Branislav, Pavlović, Vera P., Marinković, Aleksandar D., Pavlović, Vladimir B., "Controllable synthesis of Fe3O4-wollastonite adsorbents for efficient heavy metal ions/oxyanions removal" in Environmental Science and Pollution Research, 26, no. 12 (2019):12379-12398,
https://doi.org/10.1007/s11356-019-04625-0 . .

TY  - JOUR
AU  - Rusmirović, Jelena D.
AU  - Obradović, Nina
AU  - Perendija, Jovana
AU  - Umićević, Ana
AU  - Kapidžić, Ana
AU  - Vlahović, Branislav
AU  - Pavlović, Vera P.
AU  - Marinković, Aleksandar D.
AU  - Pavlović, Vladimir B.
PY  - 2019
UR  - https://vinar.vin.bg.ac.rs/handle/123456789/8101
AB  - Iron oxide, in the form of magnetite (MG)–functionalized porous wollastonite (WL), was used as an adsorbent for heavy metal ions (cadmium and nickel) and oxyanions (chromate and phosphate) removal from water. The porous WL was synthesized from calcium carbonate and siloxane by controlled sintering process using low molecular weight submicrosized poly(methyl methacrylate) as a pore-forming agent. The precipitation of MG nanoparticles was carried out directly by a polyol-medium solvothermal method or via branched amino/carboxylic acid cross-linker by solvent/nonsolvent method producing WL/MG and WL-γ-APS/MG adsorbents, respectively. The structure/properties of MG functionalized WL was confirmed by applying FTIR, Raman, XRD, Mössbauer, and SEM analysis. Higher adsorption capacities of 73.126, 66.144, 64.168, and 63.456 mg g−1 for WL-γ-APS/MG in relation to WL/MG of 55.450, 52.019, 48.132, and 47.382 mg g−1 for Cd2+, Ni2+, phosphate, and chromate, respectively, were obtained using nonlinear Langmuir model fitting. Adsorption phenomena were analyzed using monolayer statistical physics model for single adsorption with one energy. Kinetic study showed exceptionally higher pseudo-second-order rate constants for WL-γ-APS/MG, e.g., 1.17–13.4 times, with respect to WL/MG indicating importance of both WL surface modification and controllable precipitation of MG on WL-γ-APS.
T2  - Environmental Science and Pollution Research
T1  - Controllable synthesis of Fe3O4-wollastonite adsorbents for efficient heavy metal ions/oxyanions removal
VL  - 26
IS  - 12
SP  - 12379
EP  - 12398
DO  - 10.1007/s11356-019-04625-0
ER  - 

@article{
author = "Rusmirović, Jelena D. and Obradović, Nina and Perendija, Jovana and Umićević, Ana and Kapidžić, Ana and Vlahović, Branislav and Pavlović, Vera P. and Marinković, Aleksandar D. and Pavlović, Vladimir B.",
year = "2019",
abstract = "Iron oxide, in the form of magnetite (MG)–functionalized porous wollastonite (WL), was used as an adsorbent for heavy metal ions (cadmium and nickel) and oxyanions (chromate and phosphate) removal from water. The porous WL was synthesized from calcium carbonate and siloxane by controlled sintering process using low molecular weight submicrosized poly(methyl methacrylate) as a pore-forming agent. The precipitation of MG nanoparticles was carried out directly by a polyol-medium solvothermal method or via branched amino/carboxylic acid cross-linker by solvent/nonsolvent method producing WL/MG and WL-γ-APS/MG adsorbents, respectively. The structure/properties of MG functionalized WL was confirmed by applying FTIR, Raman, XRD, Mössbauer, and SEM analysis. Higher adsorption capacities of 73.126, 66.144, 64.168, and 63.456 mg g−1 for WL-γ-APS/MG in relation to WL/MG of 55.450, 52.019, 48.132, and 47.382 mg g−1 for Cd2+, Ni2+, phosphate, and chromate, respectively, were obtained using nonlinear Langmuir model fitting. Adsorption phenomena were analyzed using monolayer statistical physics model for single adsorption with one energy. Kinetic study showed exceptionally higher pseudo-second-order rate constants for WL-γ-APS/MG, e.g., 1.17–13.4 times, with respect to WL/MG indicating importance of both WL surface modification and controllable precipitation of MG on WL-γ-APS.",
journal = "Environmental Science and Pollution Research",
title = "Controllable synthesis of Fe3O4-wollastonite adsorbents for efficient heavy metal ions/oxyanions removal",
volume = "26",
number = "12",
pages = "12379-12398",
doi = "10.1007/s11356-019-04625-0"
}

Rusmirović, J. D., Obradović, N., Perendija, J., Umićević, A., Kapidžić, A., Vlahović, B., Pavlović, V. P., Marinković, A. D.,& Pavlović, V. B.. (2019). Controllable synthesis of Fe3O4-wollastonite adsorbents for efficient heavy metal ions/oxyanions removal. in Environmental Science and Pollution Research, 26(12), 12379-12398.
https://doi.org/10.1007/s11356-019-04625-0

Rusmirović JD, Obradović N, Perendija J, Umićević A, Kapidžić A, Vlahović B, Pavlović VP, Marinković AD, Pavlović VB. Controllable synthesis of Fe3O4-wollastonite adsorbents for efficient heavy metal ions/oxyanions removal. in Environmental Science and Pollution Research. 2019;26(12):12379-12398.
doi:10.1007/s11356-019-04625-0 .

Rusmirović, Jelena D., Obradović, Nina, Perendija, Jovana, Umićević, Ana, Kapidžić, Ana, Vlahović, Branislav, Pavlović, Vera P., Marinković, Aleksandar D., Pavlović, Vladimir B., "Controllable synthesis of Fe3O4-wollastonite adsorbents for efficient heavy metal ions/oxyanions removal" in Environmental Science and Pollution Research, 26, no. 12 (2019):12379-12398,
https://doi.org/10.1007/s11356-019-04625-0 . .

TY  - JOUR
AU  - Filipović, Suzana
AU  - Obradović, Nina
AU  - Marković, Smilja
AU  - Mitrić, Miodrag
AU  - Balać, Igor
AU  - Đorđević, Antonije
AU  - Pavlović, Vladimir B.
PY  - 2019
UR  - https://vinar.vin.bg.ac.rs/handle/123456789/8441
AB  - Alumina-based compounds have many technological applications and attract great attention even after decades of investigation, due to their good chemical, electrical, and mechanical properties. A mixture of several alumina modifications (α-, κ-, γ-Al2O3) doped with 1 wt% of Mn2O3 was used for this experiment. The powder was mechanically activated for 60 min in an ethanol medium. After compaction, green bodies were sintered in the temperature range from 1200 to 1400 °C. Microstructures of the obtained specimens were investigated by scanning electron microscopy (SEM) and Energy-dispersive X-ray spectroscopy (EDS). The influence of morphological changes on electrical and mechanical properties was examined in detail. We have developed a test fixture and corresponding software for measurement of the relative dielectric permittivity and the loss tangent of ceramic specimens. This new method overcomes the problems of dimensions and shape of samples, as well as the problem of applying silver paste. The accuracy is around 2% for ε'r and 0.003 for tanδ. We demonstrate that the mechanical activation (MA) has the dominant influence on lowering the characteristic temperatures and microstructure development, which further leads to increased permittivity and tensile strength.
T2  - Advanced Powder Technology
T1  - The effect of ball milling on properties of sintered manganese-doped alumina
VL  - 30
IS  - 11
SP  - 2533
EP  - 2540
DO  - 10.1016/j.apt.2019.07.033
ER  - 

@article{
author = "Filipović, Suzana and Obradović, Nina and Marković, Smilja and Mitrić, Miodrag and Balać, Igor and Đorđević, Antonije and Pavlović, Vladimir B.",
year = "2019",
abstract = "Alumina-based compounds have many technological applications and attract great attention even after decades of investigation, due to their good chemical, electrical, and mechanical properties. A mixture of several alumina modifications (α-, κ-, γ-Al2O3) doped with 1 wt% of Mn2O3 was used for this experiment. The powder was mechanically activated for 60 min in an ethanol medium. After compaction, green bodies were sintered in the temperature range from 1200 to 1400 °C. Microstructures of the obtained specimens were investigated by scanning electron microscopy (SEM) and Energy-dispersive X-ray spectroscopy (EDS). The influence of morphological changes on electrical and mechanical properties was examined in detail. We have developed a test fixture and corresponding software for measurement of the relative dielectric permittivity and the loss tangent of ceramic specimens. This new method overcomes the problems of dimensions and shape of samples, as well as the problem of applying silver paste. The accuracy is around 2% for ε'r and 0.003 for tanδ. We demonstrate that the mechanical activation (MA) has the dominant influence on lowering the characteristic temperatures and microstructure development, which further leads to increased permittivity and tensile strength.",
journal = "Advanced Powder Technology",
title = "The effect of ball milling on properties of sintered manganese-doped alumina",
volume = "30",
number = "11",
pages = "2533-2540",
doi = "10.1016/j.apt.2019.07.033"
}

Filipović, S., Obradović, N., Marković, S., Mitrić, M., Balać, I., Đorđević, A.,& Pavlović, V. B.. (2019). The effect of ball milling on properties of sintered manganese-doped alumina. in Advanced Powder Technology, 30(11), 2533-2540.
https://doi.org/10.1016/j.apt.2019.07.033

Filipović S, Obradović N, Marković S, Mitrić M, Balać I, Đorđević A, Pavlović VB. The effect of ball milling on properties of sintered manganese-doped alumina. in Advanced Powder Technology. 2019;30(11):2533-2540.
doi:10.1016/j.apt.2019.07.033 .

Filipović, Suzana, Obradović, Nina, Marković, Smilja, Mitrić, Miodrag, Balać, Igor, Đorđević, Antonije, Pavlović, Vladimir B., "The effect of ball milling on properties of sintered manganese-doped alumina" in Advanced Powder Technology, 30, no. 11 (2019):2533-2540,
https://doi.org/10.1016/j.apt.2019.07.033 . .

TY  - JOUR
AU  - Filipović, Suzana
AU  - Obradović, Nina
AU  - Marković, Smilja
AU  - Mitrić, Miodrag
AU  - Balać, Igor
AU  - Đorđević, Antonije
AU  - Pavlović, Vladimir B.
PY  - 2019
UR  - https://vinar.vin.bg.ac.rs/handle/123456789/8442
AB  - Alumina-based compounds have many technological applications and attract great attention even after decades of investigation, due to their good chemical, electrical, and mechanical properties. A mixture of several alumina modifications (α-, κ-, γ-Al2O3) doped with 1 wt% of Mn2O3 was used for this experiment. The powder was mechanically activated for 60 min in an ethanol medium. After compaction, green bodies were sintered in the temperature range from 1200 to 1400 °C. Microstructures of the obtained specimens were investigated by scanning electron microscopy (SEM) and Energy-dispersive X-ray spectroscopy (EDS). The influence of morphological changes on electrical and mechanical properties was examined in detail. We have developed a test fixture and corresponding software for measurement of the relative dielectric permittivity and the loss tangent of ceramic specimens. This new method overcomes the problems of dimensions and shape of samples, as well as the problem of applying silver paste. The accuracy is around 2% for ε'r and 0.003 for tanδ. We demonstrate that the mechanical activation (MA) has the dominant influence on lowering the characteristic temperatures and microstructure development, which further leads to increased permittivity and tensile strength.
T2  - Advanced Powder Technology
T1  - The effect of ball milling on properties of sintered manganese-doped alumina
VL  - 30
IS  - 11
SP  - 2533
EP  - 2540
DO  - 10.1016/j.apt.2019.07.033
ER  - 

@article{
author = "Filipović, Suzana and Obradović, Nina and Marković, Smilja and Mitrić, Miodrag and Balać, Igor and Đorđević, Antonije and Pavlović, Vladimir B.",
year = "2019",
abstract = "Alumina-based compounds have many technological applications and attract great attention even after decades of investigation, due to their good chemical, electrical, and mechanical properties. A mixture of several alumina modifications (α-, κ-, γ-Al2O3) doped with 1 wt% of Mn2O3 was used for this experiment. The powder was mechanically activated for 60 min in an ethanol medium. After compaction, green bodies were sintered in the temperature range from 1200 to 1400 °C. Microstructures of the obtained specimens were investigated by scanning electron microscopy (SEM) and Energy-dispersive X-ray spectroscopy (EDS). The influence of morphological changes on electrical and mechanical properties was examined in detail. We have developed a test fixture and corresponding software for measurement of the relative dielectric permittivity and the loss tangent of ceramic specimens. This new method overcomes the problems of dimensions and shape of samples, as well as the problem of applying silver paste. The accuracy is around 2% for ε'r and 0.003 for tanδ. We demonstrate that the mechanical activation (MA) has the dominant influence on lowering the characteristic temperatures and microstructure development, which further leads to increased permittivity and tensile strength.",
journal = "Advanced Powder Technology",
title = "The effect of ball milling on properties of sintered manganese-doped alumina",
volume = "30",
number = "11",
pages = "2533-2540",
doi = "10.1016/j.apt.2019.07.033"
}

Filipović, S., Obradović, N., Marković, S., Mitrić, M., Balać, I., Đorđević, A.,& Pavlović, V. B.. (2019). The effect of ball milling on properties of sintered manganese-doped alumina. in Advanced Powder Technology, 30(11), 2533-2540.
https://doi.org/10.1016/j.apt.2019.07.033

Filipović S, Obradović N, Marković S, Mitrić M, Balać I, Đorđević A, Pavlović VB. The effect of ball milling on properties of sintered manganese-doped alumina. in Advanced Powder Technology. 2019;30(11):2533-2540.
doi:10.1016/j.apt.2019.07.033 .

Filipović, Suzana, Obradović, Nina, Marković, Smilja, Mitrić, Miodrag, Balać, Igor, Đorđević, Antonije, Pavlović, Vladimir B., "The effect of ball milling on properties of sintered manganese-doped alumina" in Advanced Powder Technology, 30, no. 11 (2019):2533-2540,
https://doi.org/10.1016/j.apt.2019.07.033 . .

TY  - JOUR
AU  - Obradović, Nina
AU  - Gigov, Mihajlo
AU  - Đorđević, Aleksandar
AU  - Kern, Frank
AU  - Dmitrović, Svetlana
AU  - Matović, Branko
AU  - Ðorđević, Antonije
AU  - Tshantshapanyan, Ani
AU  - Vlahović, Branislav
AU  - Petrović, Predrag
AU  - Pavlović, Vladimir B.
PY  - 2019
UR  - https://vinar.vin.bg.ac.rs/handle/123456789/8443
AB  - The paper presents results of the influence of mechanical activation of shungite, a carbon-mineral rock material rich in silica and carbon, on its sintering behaviour, and obtaining of pure SiC ceramics. The mechanical activation of the starting powder was performed in a high-energy ball mill in time intervals from 30 to 480 min. The phase composition of the starting powders and sintered samples was analysed by the X-ray diffraction method. The first traces of SiC were detected after sintering at 1350 °C for 2 h in an Ar atmosphere, along with traces of unreacted SiO2. The scanning electron microscopy was performed in order to determine changes in the microstructure. Sintering was performed at various temperatures for 2 h, in an Ar atmosphere and a vacuum. Dielectric properties of the sintered samples were measured in the frequency range from 1 to 500 MHz. The obtained results indicate that the sintered powder is a good candidate for applications as an absorber of electromagnetic waves in microwave engineering. © 2019 University of Novi Sad, Faculty of Technology. All rights reserved.
T2  - Processing and Application of Ceramics
T1  - Shungite – a carbon-mineral rock material: Its sinterability and possible applications
VL  - 13
IS  - 1
SP  - 89
EP  - 97
DO  - 10.2298/PAC1901089O
ER  - 

@article{
author = "Obradović, Nina and Gigov, Mihajlo and Đorđević, Aleksandar and Kern, Frank and Dmitrović, Svetlana and Matović, Branko and Ðorđević, Antonije and Tshantshapanyan, Ani and Vlahović, Branislav and Petrović, Predrag and Pavlović, Vladimir B.",
year = "2019",
abstract = "The paper presents results of the influence of mechanical activation of shungite, a carbon-mineral rock material rich in silica and carbon, on its sintering behaviour, and obtaining of pure SiC ceramics. The mechanical activation of the starting powder was performed in a high-energy ball mill in time intervals from 30 to 480 min. The phase composition of the starting powders and sintered samples was analysed by the X-ray diffraction method. The first traces of SiC were detected after sintering at 1350 °C for 2 h in an Ar atmosphere, along with traces of unreacted SiO2. The scanning electron microscopy was performed in order to determine changes in the microstructure. Sintering was performed at various temperatures for 2 h, in an Ar atmosphere and a vacuum. Dielectric properties of the sintered samples were measured in the frequency range from 1 to 500 MHz. The obtained results indicate that the sintered powder is a good candidate for applications as an absorber of electromagnetic waves in microwave engineering. © 2019 University of Novi Sad, Faculty of Technology. All rights reserved.",
journal = "Processing and Application of Ceramics",
title = "Shungite – a carbon-mineral rock material: Its sinterability and possible applications",
volume = "13",
number = "1",
pages = "89-97",
doi = "10.2298/PAC1901089O"
}

Obradović, N., Gigov, M., Đorđević, A., Kern, F., Dmitrović, S., Matović, B., Ðorđević, A., Tshantshapanyan, A., Vlahović, B., Petrović, P.,& Pavlović, V. B.. (2019). Shungite – a carbon-mineral rock material: Its sinterability and possible applications. in Processing and Application of Ceramics, 13(1), 89-97.
https://doi.org/10.2298/PAC1901089O

Obradović N, Gigov M, Đorđević A, Kern F, Dmitrović S, Matović B, Ðorđević A, Tshantshapanyan A, Vlahović B, Petrović P, Pavlović VB. Shungite – a carbon-mineral rock material: Its sinterability and possible applications. in Processing and Application of Ceramics. 2019;13(1):89-97.
doi:10.2298/PAC1901089O .

Obradović, Nina, Gigov, Mihajlo, Đorđević, Aleksandar, Kern, Frank, Dmitrović, Svetlana, Matović, Branko, Ðorđević, Antonije, Tshantshapanyan, Ani, Vlahović, Branislav, Petrović, Predrag, Pavlović, Vladimir B., "Shungite – a carbon-mineral rock material: Its sinterability and possible applications" in Processing and Application of Ceramics, 13, no. 1 (2019):89-97,
https://doi.org/10.2298/PAC1901089O . .

TY  - JOUR
AU  - Obradović, Nina
AU  - Filipović, Suzana
AU  - Marković, Smilja
AU  - Mitrić, Miodrag
AU  - Rusmirović, Jelena D.
AU  - Marinković, Aleksandar D.
AU  - Antić, Vesna
AU  - Pavlović, Vladimir B.
PY  - 2017
UR  - https://vinar.vin.bg.ac.rs/handle/123456789/1558
AB  - In this study, porous macro- and micro-cellular wollastonite-based ceramics was synthesized. A ceramic precursor, methylhydrocyclosiloxane, together with micro-sized CaCO3, was used as a starting material. After 20 min of ultrasound treatment, and calcination at 250 degrees C for 30 min, different pore-forming agents were added to the as-obtained powders. Differential thermal analysis was used to determine characteristic temperatures of processes occurring within powders during heating. Based on the obtained results, the sintering regime was set up. The prepared mixtures were pressed into pallets and sintered at 900 degrees C. During the sintering regime, porous wollastonite-based ceramics was obtained. The phase composition of the sintered samples, as well as the microstructures, were analyzed by using X-ray diffraction and SEM. A two-phase system was detected in all samples, CaSiO3 wollastonite and Ca2SiO4 larnite, and their ratio varied with each pore-forming agent. It was observed that the addition of different pore-forming agents resulted in significantly different microstructures. In a batch test, the influence of pH, the contact time and the initial ion concentration on the adsorption efficiency of As+5, Cr(+6)and phosphate ions on the synthesized adsorbents were studied. Time-dependent adsorption is best described by the pseudo-second-order kinetic model and the Weber-Morris model, which predict intra-particle diffusion as a rate-controlling step of the overall process. High adsorption capacities, 21.93, 23.88, and 27.29 mg g(-1), were obtained for the CaCO3-siloxane-nanocellulose sorbent, and similar/lower capacities were obtained for the CaCO3-siloxane-PMMA and CaCO3-siloxane-cotton wool adsorbents.
T2  - Ceramics International
T1  - Influence of different pore-forming agents on wollastonite microstructures and adsorption capacities
VL  - 43
IS  - 10
SP  - 7461
EP  - 7468
DO  - 10.1016/j.ceramint.2017.03.021
ER  - 

@article{
author = "Obradović, Nina and Filipović, Suzana and Marković, Smilja and Mitrić, Miodrag and Rusmirović, Jelena D. and Marinković, Aleksandar D. and Antić, Vesna and Pavlović, Vladimir B.",
year = "2017",
abstract = "In this study, porous macro- and micro-cellular wollastonite-based ceramics was synthesized. A ceramic precursor, methylhydrocyclosiloxane, together with micro-sized CaCO3, was used as a starting material. After 20 min of ultrasound treatment, and calcination at 250 degrees C for 30 min, different pore-forming agents were added to the as-obtained powders. Differential thermal analysis was used to determine characteristic temperatures of processes occurring within powders during heating. Based on the obtained results, the sintering regime was set up. The prepared mixtures were pressed into pallets and sintered at 900 degrees C. During the sintering regime, porous wollastonite-based ceramics was obtained. The phase composition of the sintered samples, as well as the microstructures, were analyzed by using X-ray diffraction and SEM. A two-phase system was detected in all samples, CaSiO3 wollastonite and Ca2SiO4 larnite, and their ratio varied with each pore-forming agent. It was observed that the addition of different pore-forming agents resulted in significantly different microstructures. In a batch test, the influence of pH, the contact time and the initial ion concentration on the adsorption efficiency of As+5, Cr(+6)and phosphate ions on the synthesized adsorbents were studied. Time-dependent adsorption is best described by the pseudo-second-order kinetic model and the Weber-Morris model, which predict intra-particle diffusion as a rate-controlling step of the overall process. High adsorption capacities, 21.93, 23.88, and 27.29 mg g(-1), were obtained for the CaCO3-siloxane-nanocellulose sorbent, and similar/lower capacities were obtained for the CaCO3-siloxane-PMMA and CaCO3-siloxane-cotton wool adsorbents.",
journal = "Ceramics International",
title = "Influence of different pore-forming agents on wollastonite microstructures and adsorption capacities",
volume = "43",
number = "10",
pages = "7461-7468",
doi = "10.1016/j.ceramint.2017.03.021"
}

Obradović, N., Filipović, S., Marković, S., Mitrić, M., Rusmirović, J. D., Marinković, A. D., Antić, V.,& Pavlović, V. B.. (2017). Influence of different pore-forming agents on wollastonite microstructures and adsorption capacities. in Ceramics International, 43(10), 7461-7468.
https://doi.org/10.1016/j.ceramint.2017.03.021

Obradović N, Filipović S, Marković S, Mitrić M, Rusmirović JD, Marinković AD, Antić V, Pavlović VB. Influence of different pore-forming agents on wollastonite microstructures and adsorption capacities. in Ceramics International. 2017;43(10):7461-7468.
doi:10.1016/j.ceramint.2017.03.021 .

Obradović, Nina, Filipović, Suzana, Marković, Smilja, Mitrić, Miodrag, Rusmirović, Jelena D., Marinković, Aleksandar D., Antić, Vesna, Pavlović, Vladimir B., "Influence of different pore-forming agents on wollastonite microstructures and adsorption capacities" in Ceramics International, 43, no. 10 (2017):7461-7468,
https://doi.org/10.1016/j.ceramint.2017.03.021 . .

TY  - JOUR
AU  - Brković, Danijela V.
AU  - Pavlović, Vladimir B.
AU  - Pavlović, Vera P.
AU  - Obradović, Nina
AU  - Mitrić, Miodrag
AU  - Stevanović, Sanja
AU  - Vlahović, Branislav
AU  - Uskoković, Petar S.
AU  - Marinković, Aleksandar D.
PY  - 2017
UR  - https://vinar.vin.bg.ac.rs/handle/123456789/1753
AB  - The structural characteristics of polymer nanocomposites with functionalized multiwall carbon nanotubes (MWCNTs) in poly(methyl methacrylate) matrix have been studied in relation to nanofiller loading and surface functionality. Different functional groups have been covalently attached on the MWCNTs sidewalls in order to induce interfacial interactions at nanofiller/polymer interface, which resulted in an improved nanomechanical features. Structural properties of nanocomposites, studied with XRD and Raman analysis, indicated the most pronounced decrease in a degree of amorphousness for samples containing 0.5 and 1 wt% of MWCNTs functionalized with dapsone (dapson-MWCNT) and diethyl malonate (dem-MWCNT). SEM and TEM micrographs confirmed improved dispersibility of the MWCNTs modified with aromatic structure of dapsone inside PMMA matrix. A significant increase in a glass transition temperature of over 60 degrees C has been found for the 1 wt% dapson-MWCNT nanocomposite. Additional modification of dapson-MWCNT by further increasing aromaticity and voluminosity of attached moiety (fid-MWCNT), showed 30 degrees C increases in a glass transition temperature at 4 wt% of nanofiller loading, which is similar to shift of 37 degrees C with loading of MWCNTs modified with ester terminal group. A maximum increase of 56% of reduced modulus and 86% of hardness was obtained for 1 wt% loading of dapson-MWCNT nanofiller. (C) 2016 Society of Plastics Engineers
T2  - Polymer Composites
T1  - Structural Properties of the Multiwall Carbon Nanotubes/Poly(Methyl Methacrylate) Nanocomposites: Effect of the Multiwall Carbon Nanotubes Covalent Functionalization
VL  - 38
IS  - SI
SP  - E472
EP  - E489
DO  - 10.1002/pc.23996
ER  - 

@article{
author = "Brković, Danijela V. and Pavlović, Vladimir B. and Pavlović, Vera P. and Obradović, Nina and Mitrić, Miodrag and Stevanović, Sanja and Vlahović, Branislav and Uskoković, Petar S. and Marinković, Aleksandar D.",
year = "2017",
abstract = "The structural characteristics of polymer nanocomposites with functionalized multiwall carbon nanotubes (MWCNTs) in poly(methyl methacrylate) matrix have been studied in relation to nanofiller loading and surface functionality. Different functional groups have been covalently attached on the MWCNTs sidewalls in order to induce interfacial interactions at nanofiller/polymer interface, which resulted in an improved nanomechanical features. Structural properties of nanocomposites, studied with XRD and Raman analysis, indicated the most pronounced decrease in a degree of amorphousness for samples containing 0.5 and 1 wt% of MWCNTs functionalized with dapsone (dapson-MWCNT) and diethyl malonate (dem-MWCNT). SEM and TEM micrographs confirmed improved dispersibility of the MWCNTs modified with aromatic structure of dapsone inside PMMA matrix. A significant increase in a glass transition temperature of over 60 degrees C has been found for the 1 wt% dapson-MWCNT nanocomposite. Additional modification of dapson-MWCNT by further increasing aromaticity and voluminosity of attached moiety (fid-MWCNT), showed 30 degrees C increases in a glass transition temperature at 4 wt% of nanofiller loading, which is similar to shift of 37 degrees C with loading of MWCNTs modified with ester terminal group. A maximum increase of 56% of reduced modulus and 86% of hardness was obtained for 1 wt% loading of dapson-MWCNT nanofiller. (C) 2016 Society of Plastics Engineers",
journal = "Polymer Composites",
title = "Structural Properties of the Multiwall Carbon Nanotubes/Poly(Methyl Methacrylate) Nanocomposites: Effect of the Multiwall Carbon Nanotubes Covalent Functionalization",
volume = "38",
number = "SI",
pages = "E472-E489",
doi = "10.1002/pc.23996"
}

Brković, D. V., Pavlović, V. B., Pavlović, V. P., Obradović, N., Mitrić, M., Stevanović, S., Vlahović, B., Uskoković, P. S.,& Marinković, A. D.. (2017). Structural Properties of the Multiwall Carbon Nanotubes/Poly(Methyl Methacrylate) Nanocomposites: Effect of the Multiwall Carbon Nanotubes Covalent Functionalization. in Polymer Composites, 38(SI), E472-E489.
https://doi.org/10.1002/pc.23996

Brković DV, Pavlović VB, Pavlović VP, Obradović N, Mitrić M, Stevanović S, Vlahović B, Uskoković PS, Marinković AD. Structural Properties of the Multiwall Carbon Nanotubes/Poly(Methyl Methacrylate) Nanocomposites: Effect of the Multiwall Carbon Nanotubes Covalent Functionalization. in Polymer Composites. 2017;38(SI):E472-E489.
doi:10.1002/pc.23996 .

Brković, Danijela V., Pavlović, Vladimir B., Pavlović, Vera P., Obradović, Nina, Mitrić, Miodrag, Stevanović, Sanja, Vlahović, Branislav, Uskoković, Petar S., Marinković, Aleksandar D., "Structural Properties of the Multiwall Carbon Nanotubes/Poly(Methyl Methacrylate) Nanocomposites: Effect of the Multiwall Carbon Nanotubes Covalent Functionalization" in Polymer Composites, 38, no. SI (2017):E472-E489,
https://doi.org/10.1002/pc.23996 . .

TY  - CONF
AU  - Obradović, Nina
AU  - Filipović, Suzana
AU  - Marković, Smilja
AU  - Mitrić, Miodrag
AU  - Antić, Vesna
AU  - Pavlović, Vladimir B.
PY  - 2016
UR  - https://vinar.vin.bg.ac.rs/handle/123456789/7548
AB  - In this study, highly porous macro- and micro-cellular wollastonite-based ceramics was synthesized. Ceramic precursor, methylhydrocyclosiloxane, together with micro-sized CaCO3, was used as starting material. After 20 min of ultrasound treatment, and calcination at 250 oC for 30 min, different pore-forming agents were added to the as-obtained powders. Differential thermal analysis was used to determine characteristic temperatures of processes occurring within powders during heating. Based on the obtained results, sintering regime was set up. Prepared mixtures were pressed into pallets and sintered at 900 oC. During the sintering regime, highly porous wollastonite-based ceramics was obtained. The phase composition of the sintered samples as well as microstructures was analyzed by the means of X-ray diffraction method and SEM. Two-phase system was detected in all samples, CaSiO3 wollastonite and Ca2SiO4 larnite, and their ratio varied with each pore-forming agent. It was observed that addition of different pore-forming agent resulted in significantly different microstructures.
PB  - Belgrade : Serbian Ceramic Society
C3  - Advanced Ceramics and Application : 5th Serbian Ceramic Society Conference : program and the book of abstracts; September 21-23, 2016; Belgrade
T1  - Influence of different pore-forming agents on wollastonite microstructures
SP  - 42
UR  - https://hdl.handle.net/21.15107/rcub_vinar_7548
ER  - 

@conference{
author = "Obradović, Nina and Filipović, Suzana and Marković, Smilja and Mitrić, Miodrag and Antić, Vesna and Pavlović, Vladimir B.",
year = "2016",
abstract = "In this study, highly porous macro- and micro-cellular wollastonite-based ceramics was synthesized. Ceramic precursor, methylhydrocyclosiloxane, together with micro-sized CaCO3, was used as starting material. After 20 min of ultrasound treatment, and calcination at 250 oC for 30 min, different pore-forming agents were added to the as-obtained powders. Differential thermal analysis was used to determine characteristic temperatures of processes occurring within powders during heating. Based on the obtained results, sintering regime was set up. Prepared mixtures were pressed into pallets and sintered at 900 oC. During the sintering regime, highly porous wollastonite-based ceramics was obtained. The phase composition of the sintered samples as well as microstructures was analyzed by the means of X-ray diffraction method and SEM. Two-phase system was detected in all samples, CaSiO3 wollastonite and Ca2SiO4 larnite, and their ratio varied with each pore-forming agent. It was observed that addition of different pore-forming agent resulted in significantly different microstructures.",
publisher = "Belgrade : Serbian Ceramic Society",
journal = "Advanced Ceramics and Application : 5th Serbian Ceramic Society Conference : program and the book of abstracts; September 21-23, 2016; Belgrade",
title = "Influence of different pore-forming agents on wollastonite microstructures",
pages = "42",
url = "https://hdl.handle.net/21.15107/rcub_vinar_7548"
}

Obradović, N., Filipović, S., Marković, S., Mitrić, M., Antić, V.,& Pavlović, V. B.. (2016). Influence of different pore-forming agents on wollastonite microstructures. in Advanced Ceramics and Application : 5th Serbian Ceramic Society Conference : program and the book of abstracts; September 21-23, 2016; Belgrade
Belgrade : Serbian Ceramic Society., 42.
https://hdl.handle.net/21.15107/rcub_vinar_7548

Obradović N, Filipović S, Marković S, Mitrić M, Antić V, Pavlović VB. Influence of different pore-forming agents on wollastonite microstructures. in Advanced Ceramics and Application : 5th Serbian Ceramic Society Conference : program and the book of abstracts; September 21-23, 2016; Belgrade. 2016;:42.
https://hdl.handle.net/21.15107/rcub_vinar_7548 .

Obradović, Nina, Filipović, Suzana, Marković, Smilja, Mitrić, Miodrag, Antić, Vesna, Pavlović, Vladimir B., "Influence of different pore-forming agents on wollastonite microstructures" in Advanced Ceramics and Application : 5th Serbian Ceramic Society Conference : program and the book of abstracts; September 21-23, 2016; Belgrade (2016):42,
https://hdl.handle.net/21.15107/rcub_vinar_7548 .

TY  - CONF
AU  - Đorđević, Nataša
AU  - Obradović, Nina
AU  - Filipović, Suzana
AU  - Kosanović, Darko
AU  - Marković, Smilja
AU  - Mitrić, Miodrag
AU  - Pavlović, Vladimir B.
PY  - 2016
UR  - https://vinar.vin.bg.ac.rs/handle/123456789/7552
AB  - Cordierite 2MgO+2Al2O3+5SiO2 is frequently used ceramic material, that is commonly used as a carrier of electrical components due to its low dielectric constant (~ 5), and low temperature thermal expansion coefficient (20•10-7 ºC-1). In order to accelerate the process of sintering, 5.00 mass% TeO2 was added to the starting mixtures. System was tested in two parallel mixtures, one with no added additives, and the other one with TeO2. The mechanical activation of the both mixtures was performed in a high-energy ball mill in time intervals from 0 to 40 min with ball to powder mass ratio 1:40. The particle size analysis (PSA) was employed in order to determine the changes in the particle size of the mechanically treated powders. The phase composition of the starting powders as well as microstructures was analyzed by the means of X-ray diffraction method and SEM.
PB  - Belgrade : Materials Research Society of Serbia
C3  - YUCOMAT 2016 : 18th Annual Conference YUCOMAT 2016 : programme and the book of abstracts; September 5-10, Herceg Novi
T1  - Influence of mechanical activation on the MgO-Al2O3-SiO2 system with TeO2
SP  - 75
EP  - 75
UR  - https://hdl.handle.net/21.15107/rcub_vinar_7552
ER  - 

@conference{
author = "Đorđević, Nataša and Obradović, Nina and Filipović, Suzana and Kosanović, Darko and Marković, Smilja and Mitrić, Miodrag and Pavlović, Vladimir B.",
year = "2016",
abstract = "Cordierite 2MgO+2Al2O3+5SiO2 is frequently used ceramic material, that is commonly used as a carrier of electrical components due to its low dielectric constant (~ 5), and low temperature thermal expansion coefficient (20•10-7 ºC-1). In order to accelerate the process of sintering, 5.00 mass% TeO2 was added to the starting mixtures. System was tested in two parallel mixtures, one with no added additives, and the other one with TeO2. The mechanical activation of the both mixtures was performed in a high-energy ball mill in time intervals from 0 to 40 min with ball to powder mass ratio 1:40. The particle size analysis (PSA) was employed in order to determine the changes in the particle size of the mechanically treated powders. The phase composition of the starting powders as well as microstructures was analyzed by the means of X-ray diffraction method and SEM.",
publisher = "Belgrade : Materials Research Society of Serbia",
journal = "YUCOMAT 2016 : 18th Annual Conference YUCOMAT 2016 : programme and the book of abstracts; September 5-10, Herceg Novi",
title = "Influence of mechanical activation on the MgO-Al2O3-SiO2 system with TeO2",
pages = "75-75",
url = "https://hdl.handle.net/21.15107/rcub_vinar_7552"
}

Đorđević, N., Obradović, N., Filipović, S., Kosanović, D., Marković, S., Mitrić, M.,& Pavlović, V. B.. (2016). Influence of mechanical activation on the MgO-Al2O3-SiO2 system with TeO2. in YUCOMAT 2016 : 18th Annual Conference YUCOMAT 2016 : programme and the book of abstracts; September 5-10, Herceg Novi
Belgrade : Materials Research Society of Serbia., 75-75.
https://hdl.handle.net/21.15107/rcub_vinar_7552

Đorđević N, Obradović N, Filipović S, Kosanović D, Marković S, Mitrić M, Pavlović VB. Influence of mechanical activation on the MgO-Al2O3-SiO2 system with TeO2. in YUCOMAT 2016 : 18th Annual Conference YUCOMAT 2016 : programme and the book of abstracts; September 5-10, Herceg Novi. 2016;:75-75.
https://hdl.handle.net/21.15107/rcub_vinar_7552 .

Đorđević, Nataša, Obradović, Nina, Filipović, Suzana, Kosanović, Darko, Marković, Smilja, Mitrić, Miodrag, Pavlović, Vladimir B., "Influence of mechanical activation on the MgO-Al2O3-SiO2 system with TeO2" in YUCOMAT 2016 : 18th Annual Conference YUCOMAT 2016 : programme and the book of abstracts; September 5-10, Herceg Novi (2016):75-75,
https://hdl.handle.net/21.15107/rcub_vinar_7552 .

TY  - JOUR
AU  - Obradović, Nina
AU  - Đorđević, Nataša
AU  - Filipović, Suzana
AU  - Marković, Smilja
AU  - Kosanović, Darko
AU  - Mitrić, Miodrag
AU  - Pavlović, Vladimir B.
PY  - 2016
UR  - https://vinar.vin.bg.ac.rs/handle/123456789/999
AB  - Since cordierite, 2MgO center dot 2Al(2)O(3)center dot 5SiO(2) (MAS), is a very useful high-temperature ceramic material, it is important to decrease its sintering temperature. In order to accelerate the process of sintering, 5.00 mass% MoO3 was added to the starting mixtures. The mechanical activation of the starting mixtures was performed in a high-energy ball mill in time intervals from 0 to 160 min. After the activation, starting mixtures were sintered at 1300 A degrees C for 2 h. In order to determine the impact of mechanical activation on particle size distribution and powders morphology, the mechanically treated powders were characterized by a laser light-scattering particle size analyzer and scanning electron microscopy. The phase composition of the starting mixtures and sintered samples was analyzed by the X-ray diffraction method. In order to determine temperature intervals of chemical reactions and phase transitions, differential thermal analyses (DTA) and thermo-gravimetric analysis were used. Kissingers equation was employed to calculate apparent activation energies of various processes that occur within the system during heating. Based on the obtained DTA results, it was established that mechanical activation along with MoO3 additive has influence on sintering temperature which was decreased for more than 100 A degrees C, comparing to the literature data.
PB  - Springer
T2  - Journal of Thermal Analysis and Calorimetry
T1  - Reaction kinetics of mechanically activated cordierite-based ceramics studied via DTA
VL  - 124
IS  - 2
SP  - 667
EP  - 673
DO  - 10.1007/s10973-015-5132-9
ER  - 

@article{
author = "Obradović, Nina and Đorđević, Nataša and Filipović, Suzana and Marković, Smilja and Kosanović, Darko and Mitrić, Miodrag and Pavlović, Vladimir B.",
year = "2016",
abstract = "Since cordierite, 2MgO center dot 2Al(2)O(3)center dot 5SiO(2) (MAS), is a very useful high-temperature ceramic material, it is important to decrease its sintering temperature. In order to accelerate the process of sintering, 5.00 mass% MoO3 was added to the starting mixtures. The mechanical activation of the starting mixtures was performed in a high-energy ball mill in time intervals from 0 to 160 min. After the activation, starting mixtures were sintered at 1300 A degrees C for 2 h. In order to determine the impact of mechanical activation on particle size distribution and powders morphology, the mechanically treated powders were characterized by a laser light-scattering particle size analyzer and scanning electron microscopy. The phase composition of the starting mixtures and sintered samples was analyzed by the X-ray diffraction method. In order to determine temperature intervals of chemical reactions and phase transitions, differential thermal analyses (DTA) and thermo-gravimetric analysis were used. Kissingers equation was employed to calculate apparent activation energies of various processes that occur within the system during heating. Based on the obtained DTA results, it was established that mechanical activation along with MoO3 additive has influence on sintering temperature which was decreased for more than 100 A degrees C, comparing to the literature data.",
publisher = "Springer",
journal = "Journal of Thermal Analysis and Calorimetry",
title = "Reaction kinetics of mechanically activated cordierite-based ceramics studied via DTA",
volume = "124",
number = "2",
pages = "667-673",
doi = "10.1007/s10973-015-5132-9"
}

Obradović, N., Đorđević, N., Filipović, S., Marković, S., Kosanović, D., Mitrić, M.,& Pavlović, V. B.. (2016). Reaction kinetics of mechanically activated cordierite-based ceramics studied via DTA. in Journal of Thermal Analysis and Calorimetry
Springer., 124(2), 667-673.
https://doi.org/10.1007/s10973-015-5132-9

Obradović N, Đorđević N, Filipović S, Marković S, Kosanović D, Mitrić M, Pavlović VB. Reaction kinetics of mechanically activated cordierite-based ceramics studied via DTA. in Journal of Thermal Analysis and Calorimetry. 2016;124(2):667-673.
doi:10.1007/s10973-015-5132-9 .

Obradović, Nina, Đorđević, Nataša, Filipović, Suzana, Marković, Smilja, Kosanović, Darko, Mitrić, Miodrag, Pavlović, Vladimir B., "Reaction kinetics of mechanically activated cordierite-based ceramics studied via DTA" in Journal of Thermal Analysis and Calorimetry, 124, no. 2 (2016):667-673,
https://doi.org/10.1007/s10973-015-5132-9 . .

TY  - JOUR
AU  - Filipović, Suzana
AU  - Obradović, Nina
AU  - Pavlović, Vladimir B.
AU  - Mitrić, Miodrag
AU  - Đorđević, Antonije R.
AU  - Kachlik, M.
AU  - Maca, Karel
PY  - 2016
UR  - https://vinar.vin.bg.ac.rs/handle/123456789/1037
AB  - The aim of this study is to explore the influence of the processing route on the structural and physical properties of bulk MgTiO3 ceramics. Commercially available MgO and TiO2 powders were mechanically activated in a planetary ball mill. Green bodies were formed by an isostatic pressure of 300 MPa. The sintering of these samples was done either by the Two-Step Sintering (TSS) approach or by conventional pressureless sintering followed by Hot Isostatic Pressing (post-HIPing). The first set of compacts was sintered by TSS in air at 1300 degrees C for 30 min and the next step was performed at 1200 degrees C for 20 h. The density of the obtained samples after the two-step sintering reached almost 90% of the theoretical density (%TD). The second set of compacts was sintered at 1400 degrees C for 30 min in air. The samples without open porosity were post-sintered by the HIP at 1200 degrees C for 2 h in an argon atmosphere at a pressure of 200 MPa. The density significantly increased up to 96%TD. The differences between samples prepared by these two techniques were also analyzed by XRD and SEM. The lattice vibration spectra were obtained using Raman spectroscopy and they indicate a high degree of lattice disorder, as well as high values of the oxygen vacancy concentration. Electrical characteristic were established in the frequency range from 10 kHz to 10 GHz. The choice of the processing route had considerable influence on structural and physical properties of MgTiO3 ceramics. (C) 2016 Elsevier Ltd and Techna Group S.r.l. All rights reserved.
PB  - Elsevier
T2  - Ceramics International
T1  - Effect of consolidation parameters on structural, microstructural and electrical properties of magnesium titanate ceramics
VL  - 42
IS  - 8
SP  - 9887
EP  - 9898
DO  - 10.1016/j.ceramint.2016.03.088
ER  - 

@article{
author = "Filipović, Suzana and Obradović, Nina and Pavlović, Vladimir B. and Mitrić, Miodrag and Đorđević, Antonije R. and Kachlik, M. and Maca, Karel",
year = "2016",
abstract = "The aim of this study is to explore the influence of the processing route on the structural and physical properties of bulk MgTiO3 ceramics. Commercially available MgO and TiO2 powders were mechanically activated in a planetary ball mill. Green bodies were formed by an isostatic pressure of 300 MPa. The sintering of these samples was done either by the Two-Step Sintering (TSS) approach or by conventional pressureless sintering followed by Hot Isostatic Pressing (post-HIPing). The first set of compacts was sintered by TSS in air at 1300 degrees C for 30 min and the next step was performed at 1200 degrees C for 20 h. The density of the obtained samples after the two-step sintering reached almost 90% of the theoretical density (%TD). The second set of compacts was sintered at 1400 degrees C for 30 min in air. The samples without open porosity were post-sintered by the HIP at 1200 degrees C for 2 h in an argon atmosphere at a pressure of 200 MPa. The density significantly increased up to 96%TD. The differences between samples prepared by these two techniques were also analyzed by XRD and SEM. The lattice vibration spectra were obtained using Raman spectroscopy and they indicate a high degree of lattice disorder, as well as high values of the oxygen vacancy concentration. Electrical characteristic were established in the frequency range from 10 kHz to 10 GHz. The choice of the processing route had considerable influence on structural and physical properties of MgTiO3 ceramics. (C) 2016 Elsevier Ltd and Techna Group S.r.l. All rights reserved.",
publisher = "Elsevier",
journal = "Ceramics International",
title = "Effect of consolidation parameters on structural, microstructural and electrical properties of magnesium titanate ceramics",
volume = "42",
number = "8",
pages = "9887-9898",
doi = "10.1016/j.ceramint.2016.03.088"
}

Filipović, S., Obradović, N., Pavlović, V. B., Mitrić, M., Đorđević, A. R., Kachlik, M.,& Maca, K.. (2016). Effect of consolidation parameters on structural, microstructural and electrical properties of magnesium titanate ceramics. in Ceramics International
Elsevier., 42(8), 9887-9898.
https://doi.org/10.1016/j.ceramint.2016.03.088

Filipović S, Obradović N, Pavlović VB, Mitrić M, Đorđević AR, Kachlik M, Maca K. Effect of consolidation parameters on structural, microstructural and electrical properties of magnesium titanate ceramics. in Ceramics International. 2016;42(8):9887-9898.
doi:10.1016/j.ceramint.2016.03.088 .

Filipović, Suzana, Obradović, Nina, Pavlović, Vladimir B., Mitrić, Miodrag, Đorđević, Antonije R., Kachlik, M., Maca, Karel, "Effect of consolidation parameters on structural, microstructural and electrical properties of magnesium titanate ceramics" in Ceramics International, 42, no. 8 (2016):9887-9898,
https://doi.org/10.1016/j.ceramint.2016.03.088 . .

TY  - CONF
AU  - Obradović, Nina
AU  - Đorđević, Nataša
AU  - Kosanović, Darko
AU  - Filipović, Suzana
AU  - Marković, Smilja
AU  - Mitrić, Miodrag
AU  - Pavlović, Vladimir B.
PY  - 2015
UR  - http://dais.sanu.ac.rs/123456789/761
UR  - https://vinar.vin.bg.ac.rs/handle/123456789/7525
AB  - Cordierite, 2MgO•2Ah03•5Si02 (MAS), is a very attractive high-temperature ceramic material. In order to accelerate the process of sintering, 5.00 mass% Mo03 was added to the starting mixtures. The mechanical activation of the starting mixtures was performed in a high energy ball mill in time intervals from 0 to 160 minutes. In following, starting mixtures were sintered at 1300 °C for 2h. In order to determine the changes in the particle size distribution, the mechanically treated powders were characterized by a laser light-scattering particle size analyzer. The phase composition of the starting mixtures and sintered samples was analyzed by the X-ray diffraction method. Differential thermal analyses (DTA) and thermo-gravimetric (TG) analysis were used in order to determine characteristic temperatures. Kissinger's equation was employed to calculate apparent activation energies of various processes that occur within the system while heating. Based on the obtained DTA results, it was established that mechanical activation along with MoO3 additive, has influence on sintering temperature which was decreased for about 150 °C.
PB  - Ljubljana : Central and Eastern European Committee for Thermal Analysis and Calorimetry
C3  - 3rd Central and Eastern European Conference on Thermal Analysis and Calorimetry 25-28 August 2015, Ljubljana, Slovenia: Book of Abstracts
T1  - Reaction kinetics of mechanically activated cordierite based ceramics studied via DTA
SP  - 195
EP  - 195
UR  - https://hdl.handle.net/21.15107/rcub_vinar_7525
ER  - 

@conference{
author = "Obradović, Nina and Đorđević, Nataša and Kosanović, Darko and Filipović, Suzana and Marković, Smilja and Mitrić, Miodrag and Pavlović, Vladimir B.",
year = "2015",
abstract = "Cordierite, 2MgO•2Ah03•5Si02 (MAS), is a very attractive high-temperature ceramic material. In order to accelerate the process of sintering, 5.00 mass% Mo03 was added to the starting mixtures. The mechanical activation of the starting mixtures was performed in a high energy ball mill in time intervals from 0 to 160 minutes. In following, starting mixtures were sintered at 1300 °C for 2h. In order to determine the changes in the particle size distribution, the mechanically treated powders were characterized by a laser light-scattering particle size analyzer. The phase composition of the starting mixtures and sintered samples was analyzed by the X-ray diffraction method. Differential thermal analyses (DTA) and thermo-gravimetric (TG) analysis were used in order to determine characteristic temperatures. Kissinger's equation was employed to calculate apparent activation energies of various processes that occur within the system while heating. Based on the obtained DTA results, it was established that mechanical activation along with MoO3 additive, has influence on sintering temperature which was decreased for about 150 °C.",
publisher = "Ljubljana : Central and Eastern European Committee for Thermal Analysis and Calorimetry",
journal = "3rd Central and Eastern European Conference on Thermal Analysis and Calorimetry 25-28 August 2015, Ljubljana, Slovenia: Book of Abstracts",
title = "Reaction kinetics of mechanically activated cordierite based ceramics studied via DTA",
pages = "195-195",
url = "https://hdl.handle.net/21.15107/rcub_vinar_7525"
}

Obradović, N., Đorđević, N., Kosanović, D., Filipović, S., Marković, S., Mitrić, M.,& Pavlović, V. B.. (2015). Reaction kinetics of mechanically activated cordierite based ceramics studied via DTA. in 3rd Central and Eastern European Conference on Thermal Analysis and Calorimetry 25-28 August 2015, Ljubljana, Slovenia: Book of Abstracts
Ljubljana : Central and Eastern European Committee for Thermal Analysis and Calorimetry., 195-195.
https://hdl.handle.net/21.15107/rcub_vinar_7525

Obradović N, Đorđević N, Kosanović D, Filipović S, Marković S, Mitrić M, Pavlović VB. Reaction kinetics of mechanically activated cordierite based ceramics studied via DTA. in 3rd Central and Eastern European Conference on Thermal Analysis and Calorimetry 25-28 August 2015, Ljubljana, Slovenia: Book of Abstracts. 2015;:195-195.
https://hdl.handle.net/21.15107/rcub_vinar_7525 .

Obradović, Nina, Đorđević, Nataša, Kosanović, Darko, Filipović, Suzana, Marković, Smilja, Mitrić, Miodrag, Pavlović, Vladimir B., "Reaction kinetics of mechanically activated cordierite based ceramics studied via DTA" in 3rd Central and Eastern European Conference on Thermal Analysis and Calorimetry 25-28 August 2015, Ljubljana, Slovenia: Book of Abstracts (2015):195-195,
https://hdl.handle.net/21.15107/rcub_vinar_7525 .

TY  - CONF
AU  - Filipović, Suzana
AU  - Obradović, Nina
AU  - Pavlović, Vladimir B.
AU  - Kosanović, Darko
AU  - Mitrić, Miodrag
AU  - Paunović, Vesna
AU  - Pouchly, V.
AU  - Kachlik, Martin
AU  - Maca, Karel
PY  - 2015
UR  - https://vinar.vin.bg.ac.rs/handle/123456789/7526
AB  - Mechanically activated powders (0, 10, 40, 80 and 160 minutes) were formed by isostatic pressure 300 MPa to cylindrical green bodies (φ 12 mm). First set of samples was sintered at 1300°C for 30 min in air (heating rate 10 °C/min, cooling rate 5 oC/min). These samples were re-sintered at 1200 oC for 20 h in air (heating rate 20 °C/min, cooling rate 10 oC/min). Samples reached almost 90 % TD. The second set of samples was sintered at 1400 °C for 30 in air (heating rate 10 oC/min, cooling rate 5 °C/min). Relative densities increased up to 93 % TD. The samples of absence of open porosity (MTO-10, 40, 80 and 160) were post-sintered by pressure assisted technique Hot Isostatic Pressing (HIP) at 1200 °C for 2 h in argon atmosphere with pressure 200 MPa. The samples increased densities up to 96 % TD for sample MT-160. Electrical measurements were performed in the microwave field of frequency.
PB  - Belgrade : Serbian Ceramic Society
C3  - Advanced Ceramics and Application : 4th Serbian Ceramic Society Conference : program and the book of abstracts; September 21-23, 2015; Belgrade
T1  - The effect of Hot Isostatic Pressing on the MT sample densities
SP  - 55
EP  - 55
UR  - https://hdl.handle.net/21.15107/rcub_vinar_7526
ER  - 

@conference{
author = "Filipović, Suzana and Obradović, Nina and Pavlović, Vladimir B. and Kosanović, Darko and Mitrić, Miodrag and Paunović, Vesna and Pouchly, V. and Kachlik, Martin and Maca, Karel",
year = "2015",
abstract = "Mechanically activated powders (0, 10, 40, 80 and 160 minutes) were formed by isostatic pressure 300 MPa to cylindrical green bodies (φ 12 mm). First set of samples was sintered at 1300°C for 30 min in air (heating rate 10 °C/min, cooling rate 5 oC/min). These samples were re-sintered at 1200 oC for 20 h in air (heating rate 20 °C/min, cooling rate 10 oC/min). Samples reached almost 90 % TD. The second set of samples was sintered at 1400 °C for 30 in air (heating rate 10 oC/min, cooling rate 5 °C/min). Relative densities increased up to 93 % TD. The samples of absence of open porosity (MTO-10, 40, 80 and 160) were post-sintered by pressure assisted technique Hot Isostatic Pressing (HIP) at 1200 °C for 2 h in argon atmosphere with pressure 200 MPa. The samples increased densities up to 96 % TD for sample MT-160. Electrical measurements were performed in the microwave field of frequency.",
publisher = "Belgrade : Serbian Ceramic Society",
journal = "Advanced Ceramics and Application : 4th Serbian Ceramic Society Conference : program and the book of abstracts; September 21-23, 2015; Belgrade",
title = "The effect of Hot Isostatic Pressing on the MT sample densities",
pages = "55-55",
url = "https://hdl.handle.net/21.15107/rcub_vinar_7526"
}

Filipović, S., Obradović, N., Pavlović, V. B., Kosanović, D., Mitrić, M., Paunović, V., Pouchly, V., Kachlik, M.,& Maca, K.. (2015). The effect of Hot Isostatic Pressing on the MT sample densities. in Advanced Ceramics and Application : 4th Serbian Ceramic Society Conference : program and the book of abstracts; September 21-23, 2015; Belgrade
Belgrade : Serbian Ceramic Society., 55-55.
https://hdl.handle.net/21.15107/rcub_vinar_7526

Filipović S, Obradović N, Pavlović VB, Kosanović D, Mitrić M, Paunović V, Pouchly V, Kachlik M, Maca K. The effect of Hot Isostatic Pressing on the MT sample densities. in Advanced Ceramics and Application : 4th Serbian Ceramic Society Conference : program and the book of abstracts; September 21-23, 2015; Belgrade. 2015;:55-55.
https://hdl.handle.net/21.15107/rcub_vinar_7526 .

Filipović, Suzana, Obradović, Nina, Pavlović, Vladimir B., Kosanović, Darko, Mitrić, Miodrag, Paunović, Vesna, Pouchly, V., Kachlik, Martin, Maca, Karel, "The effect of Hot Isostatic Pressing on the MT sample densities" in Advanced Ceramics and Application : 4th Serbian Ceramic Society Conference : program and the book of abstracts; September 21-23, 2015; Belgrade (2015):55-55,
https://hdl.handle.net/21.15107/rcub_vinar_7526 .

TY  - CONF
AU  - Vujančević, Jelena
AU  - Bjelajac, Anđelika
AU  - Obradović, Nina
AU  - Pavlović, Vera P.
AU  - Mitrić, Miodrag
AU  - Janaćković, Đorđe T.
AU  - Rašić, Goran
AU  - Vlahović, Branislav
AU  - Pavlović, Vladimir B.
PY  - 2015
UR  - https://vinar.vin.bg.ac.rs/handle/123456789/7527
AB  - The influence of electrochemical conditions and the heat treatment on the crystal structure and the microstructure evolution of TiO2 based nanotubes synthesized by the self-ordering anodization process is investigated in this work. The electrochemical anodization was performed at room temperature, for 30 minutes under 15, 20 and 25 V, with stirring. The as-anodized Ti foils were annealed in air at 450, 600, 650 and 700 °C for 30 minutes. The structure and the lattice dynamics of the samples has been studied by using XRD and Raman spectroscopy methods. The microstructure development of the 1-D TiO2 nanostructures has been analyzed by FESEM.
PB  - Belgrade : Serbian Ceramic Society
C3  - Advanced Ceramics and Application : 4th Serbian Ceramic Society Conference : program and the book of abstracts; September 21-23, 2015; Belgrade
T1  - Influence of Synthesis Parameters on Structure of 1-D TiO2 nanostructures
SP  - 81
EP  - 81
UR  - https://hdl.handle.net/21.15107/rcub_vinar_7527
ER  - 

@conference{
author = "Vujančević, Jelena and Bjelajac, Anđelika and Obradović, Nina and Pavlović, Vera P. and Mitrić, Miodrag and Janaćković, Đorđe T. and Rašić, Goran and Vlahović, Branislav and Pavlović, Vladimir B.",
year = "2015",
abstract = "The influence of electrochemical conditions and the heat treatment on the crystal structure and the microstructure evolution of TiO2 based nanotubes synthesized by the self-ordering anodization process is investigated in this work. The electrochemical anodization was performed at room temperature, for 30 minutes under 15, 20 and 25 V, with stirring. The as-anodized Ti foils were annealed in air at 450, 600, 650 and 700 °C for 30 minutes. The structure and the lattice dynamics of the samples has been studied by using XRD and Raman spectroscopy methods. The microstructure development of the 1-D TiO2 nanostructures has been analyzed by FESEM.",
publisher = "Belgrade : Serbian Ceramic Society",
journal = "Advanced Ceramics and Application : 4th Serbian Ceramic Society Conference : program and the book of abstracts; September 21-23, 2015; Belgrade",
title = "Influence of Synthesis Parameters on Structure of 1-D TiO2 nanostructures",
pages = "81-81",
url = "https://hdl.handle.net/21.15107/rcub_vinar_7527"
}

Vujančević, J., Bjelajac, A., Obradović, N., Pavlović, V. P., Mitrić, M., Janaćković, Đ. T., Rašić, G., Vlahović, B.,& Pavlović, V. B.. (2015). Influence of Synthesis Parameters on Structure of 1-D TiO2 nanostructures. in Advanced Ceramics and Application : 4th Serbian Ceramic Society Conference : program and the book of abstracts; September 21-23, 2015; Belgrade
Belgrade : Serbian Ceramic Society., 81-81.
https://hdl.handle.net/21.15107/rcub_vinar_7527

Vujančević J, Bjelajac A, Obradović N, Pavlović VP, Mitrić M, Janaćković ĐT, Rašić G, Vlahović B, Pavlović VB. Influence of Synthesis Parameters on Structure of 1-D TiO2 nanostructures. in Advanced Ceramics and Application : 4th Serbian Ceramic Society Conference : program and the book of abstracts; September 21-23, 2015; Belgrade. 2015;:81-81.
https://hdl.handle.net/21.15107/rcub_vinar_7527 .

Vujančević, Jelena, Bjelajac, Anđelika, Obradović, Nina, Pavlović, Vera P., Mitrić, Miodrag, Janaćković, Đorđe T., Rašić, Goran, Vlahović, Branislav, Pavlović, Vladimir B., "Influence of Synthesis Parameters on Structure of 1-D TiO2 nanostructures" in Advanced Ceramics and Application : 4th Serbian Ceramic Society Conference : program and the book of abstracts; September 21-23, 2015; Belgrade (2015):81-81,
https://hdl.handle.net/21.15107/rcub_vinar_7527 .

TY  - CONF
AU  - Obradović, Nina
AU  - Đorđević, Nataša
AU  - Marković, Smilja
AU  - Marković, Marija
AU  - Mitrić, Miodrag
PY  - 2015
UR  - https://vinar.vin.bg.ac.rs/handle/123456789/7528
AB  - Fire protection coatings on steel constructions for outdoor conditions on the basis of organic solutions have been analyzed. The first layer of coating is corrosion protection, alkyd paint „PROTHERM STEEL PRIMEPOX“ manufactorer „ITALVIS PROTECT“ Italy. The second layer of coating is an expanding coat for outdoor conditions „PROTHERM STEEL (EXT)“ solvent-bazed, „AMONNFIRE“ Italy. The third layer is final colors for metal „AMOTHERM STEEL TOP PU SB“ „AMONNFIRE“ Italy. XRD, DTA/TG and FTIR methods were used for sample characterization. It was found that primary and outer layer had very good adhesion. The second layer, for fire protection possesses 2.5 mass % humidity, which resulted in decrease of adhesion. XRD and FTIR analysis showed that those materials are adequate materials for fire protection up to 1000°C. Principles of fire protection are based on chemical reaction that are taking place in the temperature range 400-700°C.
PB  - Belgrade : Serbian Ceramic Society
C3  - Advanced Ceramics and Application : 2nd Serbian Ceramic Society Conference : program and the book of abstracts; September 30 - October 1, 2013; Belgrade
T1  - Correlation between crystal structure and thermal stability of fire protection coating
SP  - 86
EP  - 86
UR  - https://hdl.handle.net/21.15107/rcub_vinar_7528
ER  - 

@conference{
author = "Obradović, Nina and Đorđević, Nataša and Marković, Smilja and Marković, Marija and Mitrić, Miodrag",
year = "2015",
abstract = "Fire protection coatings on steel constructions for outdoor conditions on the basis of organic solutions have been analyzed. The first layer of coating is corrosion protection, alkyd paint „PROTHERM STEEL PRIMEPOX“ manufactorer „ITALVIS PROTECT“ Italy. The second layer of coating is an expanding coat for outdoor conditions „PROTHERM STEEL (EXT)“ solvent-bazed, „AMONNFIRE“ Italy. The third layer is final colors for metal „AMOTHERM STEEL TOP PU SB“ „AMONNFIRE“ Italy. XRD, DTA/TG and FTIR methods were used for sample characterization. It was found that primary and outer layer had very good adhesion. The second layer, for fire protection possesses 2.5 mass % humidity, which resulted in decrease of adhesion. XRD and FTIR analysis showed that those materials are adequate materials for fire protection up to 1000°C. Principles of fire protection are based on chemical reaction that are taking place in the temperature range 400-700°C.",
publisher = "Belgrade : Serbian Ceramic Society",
journal = "Advanced Ceramics and Application : 2nd Serbian Ceramic Society Conference : program and the book of abstracts; September 30 - October 1, 2013; Belgrade",
title = "Correlation between crystal structure and thermal stability of fire protection coating",
pages = "86-86",
url = "https://hdl.handle.net/21.15107/rcub_vinar_7528"
}

Obradović, N., Đorđević, N., Marković, S., Marković, M.,& Mitrić, M.. (2015). Correlation between crystal structure and thermal stability of fire protection coating. in Advanced Ceramics and Application : 2nd Serbian Ceramic Society Conference : program and the book of abstracts; September 30 - October 1, 2013; Belgrade
Belgrade : Serbian Ceramic Society., 86-86.
https://hdl.handle.net/21.15107/rcub_vinar_7528

Obradović N, Đorđević N, Marković S, Marković M, Mitrić M. Correlation between crystal structure and thermal stability of fire protection coating. in Advanced Ceramics and Application : 2nd Serbian Ceramic Society Conference : program and the book of abstracts; September 30 - October 1, 2013; Belgrade. 2015;:86-86.
https://hdl.handle.net/21.15107/rcub_vinar_7528 .

Obradović, Nina, Đorđević, Nataša, Marković, Smilja, Marković, Marija, Mitrić, Miodrag, "Correlation between crystal structure and thermal stability of fire protection coating" in Advanced Ceramics and Application : 2nd Serbian Ceramic Society Conference : program and the book of abstracts; September 30 - October 1, 2013; Belgrade (2015):86-86,
https://hdl.handle.net/21.15107/rcub_vinar_7528 .

TY  - JOUR
AU  - Peleš, Adriana
AU  - Pavlović, Vera P.
AU  - Filipović, Suzana
AU  - Obradović, Nina
AU  - Mančić, Lidija
AU  - Krstić, Jelena
AU  - Mitrić, Miodrag
AU  - Vlahović, Branislav
AU  - Rašić, Goran
AU  - Kosanović, Darko
AU  - Pavlović, Vladimir B.
PY  - 2015
UR  - https://vinar.vin.bg.ac.rs/handle/123456789/735
AB  - Commercially available ZnO powder was mechanically activated in a planetary ball mill. In order to investigate the specific surface area, pore volume and microstructure of non-activated and mechanically activated ZnO powders the authors performed N-2 physisorption, SEM and TEM. Crystallite size and lattice microstrain were analyzed by X-ray diffraction method. XRD patterns indicate that peak intensities are getting lower and expend with activation time. The reduction in crystallite size and increasing of lattice microstrain with prolonged milling time were determined applying the Rietvelds method. The difference between non-activated and the activated powder has been also observed by X-ray photoelectron spectroscopy (XPS). XPS is used for investigating the chemical bonding of ZnO powder by analyzing the energy of photoelectrons. The lattice vibration spectra were obtained using Raman spectroscopy. In Raman spectra some changes along with atypical resonant scattering were noticed, which were caused by mechanical activation. (C) 2015 Published by Elsevier B.V.
T2  - Journal of Alloys and Compounds
T1  - Structural investigation of mechanically activated ZnO powder
VL  - 648
SP  - 971
EP  - 979
DO  - 10.1016/j.jallcom.2015.06.247
ER  - 

@article{
author = "Peleš, Adriana and Pavlović, Vera P. and Filipović, Suzana and Obradović, Nina and Mančić, Lidija and Krstić, Jelena and Mitrić, Miodrag and Vlahović, Branislav and Rašić, Goran and Kosanović, Darko and Pavlović, Vladimir B.",
year = "2015",
abstract = "Commercially available ZnO powder was mechanically activated in a planetary ball mill. In order to investigate the specific surface area, pore volume and microstructure of non-activated and mechanically activated ZnO powders the authors performed N-2 physisorption, SEM and TEM. Crystallite size and lattice microstrain were analyzed by X-ray diffraction method. XRD patterns indicate that peak intensities are getting lower and expend with activation time. The reduction in crystallite size and increasing of lattice microstrain with prolonged milling time were determined applying the Rietvelds method. The difference between non-activated and the activated powder has been also observed by X-ray photoelectron spectroscopy (XPS). XPS is used for investigating the chemical bonding of ZnO powder by analyzing the energy of photoelectrons. The lattice vibration spectra were obtained using Raman spectroscopy. In Raman spectra some changes along with atypical resonant scattering were noticed, which were caused by mechanical activation. (C) 2015 Published by Elsevier B.V.",
journal = "Journal of Alloys and Compounds",
title = "Structural investigation of mechanically activated ZnO powder",
volume = "648",
pages = "971-979",
doi = "10.1016/j.jallcom.2015.06.247"
}

Peleš, A., Pavlović, V. P., Filipović, S., Obradović, N., Mančić, L., Krstić, J., Mitrić, M., Vlahović, B., Rašić, G., Kosanović, D.,& Pavlović, V. B.. (2015). Structural investigation of mechanically activated ZnO powder. in Journal of Alloys and Compounds, 648, 971-979.
https://doi.org/10.1016/j.jallcom.2015.06.247

Peleš A, Pavlović VP, Filipović S, Obradović N, Mančić L, Krstić J, Mitrić M, Vlahović B, Rašić G, Kosanović D, Pavlović VB. Structural investigation of mechanically activated ZnO powder. in Journal of Alloys and Compounds. 2015;648:971-979.
doi:10.1016/j.jallcom.2015.06.247 .

Peleš, Adriana, Pavlović, Vera P., Filipović, Suzana, Obradović, Nina, Mančić, Lidija, Krstić, Jelena, Mitrić, Miodrag, Vlahović, Branislav, Rašić, Goran, Kosanović, Darko, Pavlović, Vladimir B., "Structural investigation of mechanically activated ZnO powder" in Journal of Alloys and Compounds, 648 (2015):971-979,
https://doi.org/10.1016/j.jallcom.2015.06.247 . .

TY  - JOUR
AU  - Obradović, Nina
AU  - Dordevic, N.
AU  - Peleš, Adriana
AU  - Filipović, Suzana
AU  - Mitrić, Miodrag
AU  - Pavlović, Vladimir B.
PY  - 2015
UR  - https://vinar.vin.bg.ac.rs/handle/123456789/565
AB  - Due to its characteristics, cordierite, 2MgO center dot 2Al(2)O(3)center dot 5SiO(2), is a high-temperature ceramic material of a great scientific interest. Mechanical activation of the starting mixtures containing 5.00 mass% TiO2 was performed in a high-energy ball mill for 10 minutes. The compaction pressure varied from 0.5 to 6tcm(-2) (49-588 MPa). The sintering process was performed at 1350 degrees C for four hours in the air atmosphere. The phase composition of the activated and sintered samples was analyzed using X-ray diffraction. Scanning electron microscopy was used to analyze the microstructure of both compacted and sintered samples. The authors have investigated the influence of compaction pressure on the sintered samples and their electrical properties.
T2  - Science of Sintering
T1  - The Influence of Compaction Pressure on the Density and Electrical Properties of Cordierite-based Ceramics
VL  - 47
IS  - 1
SP  - 15
EP  - 22
DO  - 10.2298/SOS1501015O
ER  - 

@article{
author = "Obradović, Nina and Dordevic, N. and Peleš, Adriana and Filipović, Suzana and Mitrić, Miodrag and Pavlović, Vladimir B.",
year = "2015",
abstract = "Due to its characteristics, cordierite, 2MgO center dot 2Al(2)O(3)center dot 5SiO(2), is a high-temperature ceramic material of a great scientific interest. Mechanical activation of the starting mixtures containing 5.00 mass% TiO2 was performed in a high-energy ball mill for 10 minutes. The compaction pressure varied from 0.5 to 6tcm(-2) (49-588 MPa). The sintering process was performed at 1350 degrees C for four hours in the air atmosphere. The phase composition of the activated and sintered samples was analyzed using X-ray diffraction. Scanning electron microscopy was used to analyze the microstructure of both compacted and sintered samples. The authors have investigated the influence of compaction pressure on the sintered samples and their electrical properties.",
journal = "Science of Sintering",
title = "The Influence of Compaction Pressure on the Density and Electrical Properties of Cordierite-based Ceramics",
volume = "47",
number = "1",
pages = "15-22",
doi = "10.2298/SOS1501015O"
}

Obradović, N., Dordevic, N., Peleš, A., Filipović, S., Mitrić, M.,& Pavlović, V. B.. (2015). The Influence of Compaction Pressure on the Density and Electrical Properties of Cordierite-based Ceramics. in Science of Sintering, 47(1), 15-22.
https://doi.org/10.2298/SOS1501015O

Obradović N, Dordevic N, Peleš A, Filipović S, Mitrić M, Pavlović VB. The Influence of Compaction Pressure on the Density and Electrical Properties of Cordierite-based Ceramics. in Science of Sintering. 2015;47(1):15-22.
doi:10.2298/SOS1501015O .

Obradović, Nina, Dordevic, N., Peleš, Adriana, Filipović, Suzana, Mitrić, Miodrag, Pavlović, Vladimir B., "The Influence of Compaction Pressure on the Density and Electrical Properties of Cordierite-based Ceramics" in Science of Sintering, 47, no. 1 (2015):15-22,
https://doi.org/10.2298/SOS1501015O . .

TY  - CONF
AU  - Đorđević, Nataša
AU  - Obradović, Nina
AU  - Kosanović, Darko
AU  - Marković, Smilja
AU  - Mitrić, Miodrag
PY  - 2014
UR  - http://dais.sanu.ac.rs/123456789/613
UR  - https://vinar.vin.bg.ac.rs/handle/123456789/7491
AB  - Cordierite, 2MgO•2Al2O3•5SiO2 (MAS), is high-temperature ceramic material. Cordierite is commonly used material because of outstanding electrical properties, low temperature expansion coefficient and low dielectric constant. In order to accelerate the process of sintering, 5.00 mass% MoO3 has been added to the starting mixtures. The mechanical activation of the starting mixtures was performed in a high energy ball mill during 0-160 minutes. All starting mixtures were sintered at 1100°C, 1200°C and 1300°C for 2h. The particle size analysis (PSA) was employed in order to determine the changes in the particle size of the mechanically treated powders. The phase composition of the starting powders was analyzed by the X-ray diffraction method. Differential thermal (DTA) and thermogravimetric (TG) analysis were used in order to determine characteristic temperatures within the system during heating. Based on the obtained DTA results, it was established that mechanical activation with additive MoO3, has influence on decreasing sintering temperatures for about 150°C.
PB  - Belgrade : Serbian Ceramic Society
C3  - Advanced Ceramics and Application : 3rd Serbian Ceramic Society Conference : program and the book of abstracts; September 29 - October 1, 2014; Belgrade
T1  - Influence of Mechanical Activation on the Constituents of the MgO-Al2O3-SiO2-MoO3 System
SP  - 119
EP  - 119
UR  - https://hdl.handle.net/21.15107/rcub_vinar_7491
ER  - 

@conference{
author = "Đorđević, Nataša and Obradović, Nina and Kosanović, Darko and Marković, Smilja and Mitrić, Miodrag",
year = "2014",
abstract = "Cordierite, 2MgO•2Al2O3•5SiO2 (MAS), is high-temperature ceramic material. Cordierite is commonly used material because of outstanding electrical properties, low temperature expansion coefficient and low dielectric constant. In order to accelerate the process of sintering, 5.00 mass% MoO3 has been added to the starting mixtures. The mechanical activation of the starting mixtures was performed in a high energy ball mill during 0-160 minutes. All starting mixtures were sintered at 1100°C, 1200°C and 1300°C for 2h. The particle size analysis (PSA) was employed in order to determine the changes in the particle size of the mechanically treated powders. The phase composition of the starting powders was analyzed by the X-ray diffraction method. Differential thermal (DTA) and thermogravimetric (TG) analysis were used in order to determine characteristic temperatures within the system during heating. Based on the obtained DTA results, it was established that mechanical activation with additive MoO3, has influence on decreasing sintering temperatures for about 150°C.",
publisher = "Belgrade : Serbian Ceramic Society",
journal = "Advanced Ceramics and Application : 3rd Serbian Ceramic Society Conference : program and the book of abstracts; September 29 - October 1, 2014; Belgrade",
title = "Influence of Mechanical Activation on the Constituents of the MgO-Al2O3-SiO2-MoO3 System",
pages = "119-119",
url = "https://hdl.handle.net/21.15107/rcub_vinar_7491"
}

Đorđević, N., Obradović, N., Kosanović, D., Marković, S.,& Mitrić, M.. (2014). Influence of Mechanical Activation on the Constituents of the MgO-Al2O3-SiO2-MoO3 System. in Advanced Ceramics and Application : 3rd Serbian Ceramic Society Conference : program and the book of abstracts; September 29 - October 1, 2014; Belgrade
Belgrade : Serbian Ceramic Society., 119-119.
https://hdl.handle.net/21.15107/rcub_vinar_7491

Đorđević N, Obradović N, Kosanović D, Marković S, Mitrić M. Influence of Mechanical Activation on the Constituents of the MgO-Al2O3-SiO2-MoO3 System. in Advanced Ceramics and Application : 3rd Serbian Ceramic Society Conference : program and the book of abstracts; September 29 - October 1, 2014; Belgrade. 2014;:119-119.
https://hdl.handle.net/21.15107/rcub_vinar_7491 .

Đorđević, Nataša, Obradović, Nina, Kosanović, Darko, Marković, Smilja, Mitrić, Miodrag, "Influence of Mechanical Activation on the Constituents of the MgO-Al2O3-SiO2-MoO3 System" in Advanced Ceramics and Application : 3rd Serbian Ceramic Society Conference : program and the book of abstracts; September 29 - October 1, 2014; Belgrade (2014):119-119,
https://hdl.handle.net/21.15107/rcub_vinar_7491 .