Leovac, Vukadin M.

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  • Leovac, Vukadin M. (1)
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Transition metal complexes with thiosemicarbazide-based ligands. Part LVI: Nickel(II) complex with 1,3-diphenylpyrazole-4-carboxaldehyde thiosemicarbazone and unusually deformed coordination geometry

Leovac, Vukadin M.; Novaković, Slađana B.; Bogdanović, Goran A.; Joksović, Milan D.; Szecsenyi, Katalin Meszaros; Češljević, Valerija I.

(2007)

TY  - JOUR
AU  - Leovac, Vukadin M.
AU  - Novaković, Slađana B.
AU  - Bogdanović, Goran A.
AU  - Joksović, Milan D.
AU  - Szecsenyi, Katalin Meszaros
AU  - Češljević, Valerija I.
PY  - 2007
UR  - http://vinar.vin.bg.ac.rs/handle/123456789/3284
AB  - Synthesis of a new nickel(II) complex, [Ni(Ph(2)PzTSC-H)(2)] with 1,3-diphenylpyrazole-4-carboxaldehyde thiosemicarbazone (Ph(2)PzTSC), is described. The compounds have been characterized by elemental and thermal analysis, molar conductivity and spectral (UV-Vis, IR, H-1 NMR, and C-13 NMR) measurements. In the case of complex the magnetic measurement has been also performed. Crystal and molecular structures of both the free ligand and the complex have been determined by single crystal X-ray analysis. It was found that the ligand coordinates in a bidentate NS fashion, in its deprotonated thioenolato form. The cis-square-planar geometry of the complex is significantly distorted tetrahedrally. The Cambridge Structural Database (CSD) study has been performed to obtain geometrical and structural informations on similar nickel(II) complexes in order to compare structural data. (c) 2007 Elsevier Ltd. All rights reserved.
T2  - Polyhedron
T1  - Transition metal complexes with thiosemicarbazide-based ligands. Part LVI: Nickel(II) complex with 1,3-diphenylpyrazole-4-carboxaldehyde thiosemicarbazone and unusually deformed coordination geometry
VL  - 26
IS  - 14
SP  - 3783
EP  - 3792
DO  - 10.1016/j.poly.2007.04.012
ER  - 
@article{
author = "Leovac, Vukadin M. and Novaković, Slađana B. and Bogdanović, Goran A. and Joksović, Milan D. and Szecsenyi, Katalin Meszaros and Češljević, Valerija I.",
year = "2007",
abstract = "Synthesis of a new nickel(II) complex, [Ni(Ph(2)PzTSC-H)(2)] with 1,3-diphenylpyrazole-4-carboxaldehyde thiosemicarbazone (Ph(2)PzTSC), is described. The compounds have been characterized by elemental and thermal analysis, molar conductivity and spectral (UV-Vis, IR, H-1 NMR, and C-13 NMR) measurements. In the case of complex the magnetic measurement has been also performed. Crystal and molecular structures of both the free ligand and the complex have been determined by single crystal X-ray analysis. It was found that the ligand coordinates in a bidentate NS fashion, in its deprotonated thioenolato form. The cis-square-planar geometry of the complex is significantly distorted tetrahedrally. The Cambridge Structural Database (CSD) study has been performed to obtain geometrical and structural informations on similar nickel(II) complexes in order to compare structural data. (c) 2007 Elsevier Ltd. All rights reserved.",
journal = "Polyhedron",
title = "Transition metal complexes with thiosemicarbazide-based ligands. Part LVI: Nickel(II) complex with 1,3-diphenylpyrazole-4-carboxaldehyde thiosemicarbazone and unusually deformed coordination geometry",
volume = "26",
number = "14",
pages = "3783-3792",
doi = "10.1016/j.poly.2007.04.012"
}
Leovac, V. M., Novaković, S. B., Bogdanović, G. A., Joksović, M. D., Szecsenyi, K. M.,& Češljević, V. I.. (2007). Transition metal complexes with thiosemicarbazide-based ligands. Part LVI: Nickel(II) complex with 1,3-diphenylpyrazole-4-carboxaldehyde thiosemicarbazone and unusually deformed coordination geometry. in Polyhedron, 26(14), 3783-3792.
https://doi.org/10.1016/j.poly.2007.04.012
Leovac VM, Novaković SB, Bogdanović GA, Joksović MD, Szecsenyi KM, Češljević VI. Transition metal complexes with thiosemicarbazide-based ligands. Part LVI: Nickel(II) complex with 1,3-diphenylpyrazole-4-carboxaldehyde thiosemicarbazone and unusually deformed coordination geometry. in Polyhedron. 2007;26(14):3783-3792.
doi:10.1016/j.poly.2007.04.012 .
Leovac, Vukadin M., Novaković, Slađana B., Bogdanović, Goran A., Joksović, Milan D., Szecsenyi, Katalin Meszaros, Češljević, Valerija I., "Transition metal complexes with thiosemicarbazide-based ligands. Part LVI: Nickel(II) complex with 1,3-diphenylpyrazole-4-carboxaldehyde thiosemicarbazone and unusually deformed coordination geometry" in Polyhedron, 26, no. 14 (2007):3783-3792,
https://doi.org/10.1016/j.poly.2007.04.012 . .
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