Petrović, Đ.

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Development and validation of a SPE-HPLC-DAD method for the determination of selected pesticides in water samples

Kumrić, Ksenija; Vujasin, Radojka; Egerić, Marija; Petrović, Đ.; Stanković, Katarina; Devečerski, Aleksandar; Matović, Ljiljana

(Society of Physical Chemists of Serbia, 2021)

TY  - CONF
AU  - Kumrić, Ksenija
AU  - Vujasin, Radojka
AU  - Egerić, Marija
AU  - Petrović, Đ.
AU  - Stanković, Katarina
AU  - Devečerski, Aleksandar
AU  - Matović, Ljiljana
PY  - 2021
UR  - https://vinar.vin.bg.ac.rs/handle/123456789/12077
AB  - An analytical method based on solid-phase extraction (SPE) using coconut shell activated carbon (CSAC) as a low-cost adsorbent and high performance liquid chromatography with diode array detector (HPLC-DAD) was developed and validated for the determination of four varying polarity pesticides in water samples. SPE procedure was optimized and under the optimized conditions the proposed method was validated. The method exhibited good linearity, satisfactory precision (1.4 – 5.1%), high enrichment factor, good recovery and low limits of detection (0.025 – 0.039 g/dm3 ). Optimized method was used to determine selected pesticides in tap water samples. The recoveries ranged from 58.2% to 105.3%, with low relative standard deviations. The obtained results indicated that the proposed SPE-HPLC-DAD method could be efficiently used for the determination of the selected pesticides in environmental water samples at trace levels.
PB  - Society of Physical Chemists of Serbia
C3  - Physical chemistry 2021 : 15th international conference on fundamental and applied aspects of physical chemistry
T1  - Development and validation of a SPE-HPLC-DAD method for the determination of selected pesticides in water samples
VL  - II
SP  - 584
EP  - 587
UR  - https://hdl.handle.net/21.15107/rcub_vinar_12077
ER  - 
@conference{
author = "Kumrić, Ksenija and Vujasin, Radojka and Egerić, Marija and Petrović, Đ. and Stanković, Katarina and Devečerski, Aleksandar and Matović, Ljiljana",
year = "2021",
abstract = "An analytical method based on solid-phase extraction (SPE) using coconut shell activated carbon (CSAC) as a low-cost adsorbent and high performance liquid chromatography with diode array detector (HPLC-DAD) was developed and validated for the determination of four varying polarity pesticides in water samples. SPE procedure was optimized and under the optimized conditions the proposed method was validated. The method exhibited good linearity, satisfactory precision (1.4 – 5.1%), high enrichment factor, good recovery and low limits of detection (0.025 – 0.039 g/dm3 ). Optimized method was used to determine selected pesticides in tap water samples. The recoveries ranged from 58.2% to 105.3%, with low relative standard deviations. The obtained results indicated that the proposed SPE-HPLC-DAD method could be efficiently used for the determination of the selected pesticides in environmental water samples at trace levels.",
publisher = "Society of Physical Chemists of Serbia",
journal = "Physical chemistry 2021 : 15th international conference on fundamental and applied aspects of physical chemistry",
title = "Development and validation of a SPE-HPLC-DAD method for the determination of selected pesticides in water samples",
volume = "II",
pages = "584-587",
url = "https://hdl.handle.net/21.15107/rcub_vinar_12077"
}
Kumrić, K., Vujasin, R., Egerić, M., Petrović, Đ., Stanković, K., Devečerski, A.,& Matović, L.. (2021). Development and validation of a SPE-HPLC-DAD method for the determination of selected pesticides in water samples. in Physical chemistry 2021 : 15th international conference on fundamental and applied aspects of physical chemistry
Society of Physical Chemists of Serbia., II, 584-587.
https://hdl.handle.net/21.15107/rcub_vinar_12077
Kumrić K, Vujasin R, Egerić M, Petrović Đ, Stanković K, Devečerski A, Matović L. Development and validation of a SPE-HPLC-DAD method for the determination of selected pesticides in water samples. in Physical chemistry 2021 : 15th international conference on fundamental and applied aspects of physical chemistry. 2021;II:584-587.
https://hdl.handle.net/21.15107/rcub_vinar_12077 .
Kumrić, Ksenija, Vujasin, Radojka, Egerić, Marija, Petrović, Đ., Stanković, Katarina, Devečerski, Aleksandar, Matović, Ljiljana, "Development and validation of a SPE-HPLC-DAD method for the determination of selected pesticides in water samples" in Physical chemistry 2021 : 15th international conference on fundamental and applied aspects of physical chemistry, II (2021):584-587,
https://hdl.handle.net/21.15107/rcub_vinar_12077 .