Montone, Amelia

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9fe4f01c-705d-4244-ba79-8576088bc8d9
  • Montone, Amelia (6)
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Author's Bibliography

Nanostructured materials for solid-state hydrogen storage: A review of the achievement of COST Action MP1103

Callini, Elsa; Aguey-Zinsou, Kondo-Francois; Ahuja, Rajeev; Ramon Ares, Jose; Bals, Sara; Biliškov, Nikola; Chakraborty, Sudip; Charalambopoulou, Georgia; Chaudhary, Anna-Lisa; Cuevas, Fermin; Dam, Bernard; de Jongh, Petra; Dornheim, Martin; Filinchuk, Yaroslav; Grbović-Novaković, Jasmina; Hirscher, Michael; Jensen, Torben R.; Jensen, Peter Bjerre; Novaković, Nikola; Lai, Qiwen; Leardini, Fabrice; Gattia, Daniele Mirabile; Pasquini, Luca; Steriotis, Theodore; Turner, Stuart; Vegge, Tejs; Zuttel, Andreas; Montone, Amelia

(2016)

TY  - JOUR
AU  - Callini, Elsa
AU  - Aguey-Zinsou, Kondo-Francois
AU  - Ahuja, Rajeev
AU  - Ramon Ares, Jose
AU  - Bals, Sara
AU  - Biliškov, Nikola
AU  - Chakraborty, Sudip
AU  - Charalambopoulou, Georgia
AU  - Chaudhary, Anna-Lisa
AU  - Cuevas, Fermin
AU  - Dam, Bernard
AU  - de Jongh, Petra
AU  - Dornheim, Martin
AU  - Filinchuk, Yaroslav
AU  - Grbović-Novaković, Jasmina
AU  - Hirscher, Michael
AU  - Jensen, Torben R.
AU  - Jensen, Peter Bjerre
AU  - Novaković, Nikola
AU  - Lai, Qiwen
AU  - Leardini, Fabrice
AU  - Gattia, Daniele Mirabile
AU  - Pasquini, Luca
AU  - Steriotis, Theodore
AU  - Turner, Stuart
AU  - Vegge, Tejs
AU  - Zuttel, Andreas
AU  - Montone, Amelia
PY  - 2016
UR  - https://vinar.vin.bg.ac.rs/handle/123456789/7109
AB  - In the framework of the European Cooperation in Science and Technology (COST) Action MP1103 Nanostructured Materials for Solid-State Hydrogen Storage were synthesized, characterized and modeled. This Action dealt with the state of the art of energy storage and set up a competitive and coordinated network capable to define new and unexplored ways for Solid State Hydrogen Storage by innovative and interdisciplinary research within the European Research Area. An important number of new compounds have been synthesized: metal hydrides, complex hydrides, metal halide ammines and amidoboranes. Tuning the structure from bulk to thin film, nanoparticles and nanoconfined composites improved the hydrogen sorption properties and opened the perspective to new technological applications. Direct imaging of the hydrogenation reactions and in situ measurements under operando conditions have been carried out in these studies. Computational screening methods allowed the prediction of suitable compounds for hydrogen storage and the modeling of the hydrogen sorption reactions on mono-, bi-, and three-dimensional systems. This manuscript presents a review of the main achievements of this Action. (C) 2016 Hydrogen Energy Publications LLC. Published by Elsevier Ltd. All rights reserved.
T2  - International Journal of Hydrogen Energy
T1  - Nanostructured materials for solid-state hydrogen storage: A review of the achievement of COST Action MP1103
VL  - 41
IS  - 32
SP  - 14404
EP  - 14428
DO  - 10.1016/j.ijhydene.2016.04.025
ER  - 
@article{
author = "Callini, Elsa and Aguey-Zinsou, Kondo-Francois and Ahuja, Rajeev and Ramon Ares, Jose and Bals, Sara and Biliškov, Nikola and Chakraborty, Sudip and Charalambopoulou, Georgia and Chaudhary, Anna-Lisa and Cuevas, Fermin and Dam, Bernard and de Jongh, Petra and Dornheim, Martin and Filinchuk, Yaroslav and Grbović-Novaković, Jasmina and Hirscher, Michael and Jensen, Torben R. and Jensen, Peter Bjerre and Novaković, Nikola and Lai, Qiwen and Leardini, Fabrice and Gattia, Daniele Mirabile and Pasquini, Luca and Steriotis, Theodore and Turner, Stuart and Vegge, Tejs and Zuttel, Andreas and Montone, Amelia",
year = "2016",
abstract = "In the framework of the European Cooperation in Science and Technology (COST) Action MP1103 Nanostructured Materials for Solid-State Hydrogen Storage were synthesized, characterized and modeled. This Action dealt with the state of the art of energy storage and set up a competitive and coordinated network capable to define new and unexplored ways for Solid State Hydrogen Storage by innovative and interdisciplinary research within the European Research Area. An important number of new compounds have been synthesized: metal hydrides, complex hydrides, metal halide ammines and amidoboranes. Tuning the structure from bulk to thin film, nanoparticles and nanoconfined composites improved the hydrogen sorption properties and opened the perspective to new technological applications. Direct imaging of the hydrogenation reactions and in situ measurements under operando conditions have been carried out in these studies. Computational screening methods allowed the prediction of suitable compounds for hydrogen storage and the modeling of the hydrogen sorption reactions on mono-, bi-, and three-dimensional systems. This manuscript presents a review of the main achievements of this Action. (C) 2016 Hydrogen Energy Publications LLC. Published by Elsevier Ltd. All rights reserved.",
journal = "International Journal of Hydrogen Energy",
title = "Nanostructured materials for solid-state hydrogen storage: A review of the achievement of COST Action MP1103",
volume = "41",
number = "32",
pages = "14404-14428",
doi = "10.1016/j.ijhydene.2016.04.025"
}
Callini, E., Aguey-Zinsou, K., Ahuja, R., Ramon Ares, J., Bals, S., Biliškov, N., Chakraborty, S., Charalambopoulou, G., Chaudhary, A., Cuevas, F., Dam, B., de Jongh, P., Dornheim, M., Filinchuk, Y., Grbović-Novaković, J., Hirscher, M., Jensen, T. R., Jensen, P. B., Novaković, N., Lai, Q., Leardini, F., Gattia, D. M., Pasquini, L., Steriotis, T., Turner, S., Vegge, T., Zuttel, A.,& Montone, A.. (2016). Nanostructured materials for solid-state hydrogen storage: A review of the achievement of COST Action MP1103. in International Journal of Hydrogen Energy, 41(32), 14404-14428.
https://doi.org/10.1016/j.ijhydene.2016.04.025
Callini E, Aguey-Zinsou K, Ahuja R, Ramon Ares J, Bals S, Biliškov N, Chakraborty S, Charalambopoulou G, Chaudhary A, Cuevas F, Dam B, de Jongh P, Dornheim M, Filinchuk Y, Grbović-Novaković J, Hirscher M, Jensen TR, Jensen PB, Novaković N, Lai Q, Leardini F, Gattia DM, Pasquini L, Steriotis T, Turner S, Vegge T, Zuttel A, Montone A. Nanostructured materials for solid-state hydrogen storage: A review of the achievement of COST Action MP1103. in International Journal of Hydrogen Energy. 2016;41(32):14404-14428.
doi:10.1016/j.ijhydene.2016.04.025 .
Callini, Elsa, Aguey-Zinsou, Kondo-Francois, Ahuja, Rajeev, Ramon Ares, Jose, Bals, Sara, Biliškov, Nikola, Chakraborty, Sudip, Charalambopoulou, Georgia, Chaudhary, Anna-Lisa, Cuevas, Fermin, Dam, Bernard, de Jongh, Petra, Dornheim, Martin, Filinchuk, Yaroslav, Grbović-Novaković, Jasmina, Hirscher, Michael, Jensen, Torben R., Jensen, Peter Bjerre, Novaković, Nikola, Lai, Qiwen, Leardini, Fabrice, Gattia, Daniele Mirabile, Pasquini, Luca, Steriotis, Theodore, Turner, Stuart, Vegge, Tejs, Zuttel, Andreas, Montone, Amelia, "Nanostructured materials for solid-state hydrogen storage: A review of the achievement of COST Action MP1103" in International Journal of Hydrogen Energy, 41, no. 32 (2016):14404-14428,
https://doi.org/10.1016/j.ijhydene.2016.04.025 . .
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Ex situ integration of iron oxide nanoparticles onto exfoliated expanded graphite flakes in aqueous suspension

Jović, Nataša G.; Calatayud, Maria Pilar; Sanz, Beatriz; Montone, Amelia; Goya, Gerardo F.

(2014)

TY  - JOUR
AU  - Jović, Nataša G.
AU  - Calatayud, Maria Pilar
AU  - Sanz, Beatriz
AU  - Montone, Amelia
AU  - Goya, Gerardo F.
PY  - 2014
UR  - https://vinar.vin.bg.ac.rs/handle/123456789/137
AB  - Hybrid structures composed of exfoliated expanded graphite (EG) and iron oxide nanocrystals were produced by an ex situ process. The iron oxide nanoparticles coated with meso-2,3-dimercaptosuccinic acid (DMSA), or poly(acrylic acid) (PAA) were integrated onto the exfoliated EG flakes by mixing their aqueous suspensions at room temperature under the support of 1-ethyl-3-(3-dimethylaminopropyl)carbodiimide (EDC) and N-hydroxysuccinnimide (NHS). EG flakes both naked and functionalized with branched polyethylenimine (PEI) were employed. Complete integration of the two constituents was achieved and stability was maintained for more than 12 months. No preferential spatial distribution of anchoring sites for attachment of iron oxide nanoparticles was observed, regardless of whether the EG flakes were used naked or functionalized with PEI molecules. The structural and physicochemical characteristics of the exfoliated expanded graphite and its hybrid nano-structures were investigated by SEM, TEM, FTIR and Raman techniques.
T2  - Journal of the Serbian Chemical Society
T1  - Ex situ integration of iron oxide nanoparticles onto exfoliated expanded graphite flakes in aqueous suspension
VL  - 79
IS  - 9
SP  - 1155
EP  - 1167
DO  - 10.2298/JSC131121019J
ER  - 
@article{
author = "Jović, Nataša G. and Calatayud, Maria Pilar and Sanz, Beatriz and Montone, Amelia and Goya, Gerardo F.",
year = "2014",
abstract = "Hybrid structures composed of exfoliated expanded graphite (EG) and iron oxide nanocrystals were produced by an ex situ process. The iron oxide nanoparticles coated with meso-2,3-dimercaptosuccinic acid (DMSA), or poly(acrylic acid) (PAA) were integrated onto the exfoliated EG flakes by mixing their aqueous suspensions at room temperature under the support of 1-ethyl-3-(3-dimethylaminopropyl)carbodiimide (EDC) and N-hydroxysuccinnimide (NHS). EG flakes both naked and functionalized with branched polyethylenimine (PEI) were employed. Complete integration of the two constituents was achieved and stability was maintained for more than 12 months. No preferential spatial distribution of anchoring sites for attachment of iron oxide nanoparticles was observed, regardless of whether the EG flakes were used naked or functionalized with PEI molecules. The structural and physicochemical characteristics of the exfoliated expanded graphite and its hybrid nano-structures were investigated by SEM, TEM, FTIR and Raman techniques.",
journal = "Journal of the Serbian Chemical Society",
title = "Ex situ integration of iron oxide nanoparticles onto exfoliated expanded graphite flakes in aqueous suspension",
volume = "79",
number = "9",
pages = "1155-1167",
doi = "10.2298/JSC131121019J"
}
Jović, N. G., Calatayud, M. P., Sanz, B., Montone, A.,& Goya, G. F.. (2014). Ex situ integration of iron oxide nanoparticles onto exfoliated expanded graphite flakes in aqueous suspension. in Journal of the Serbian Chemical Society, 79(9), 1155-1167.
https://doi.org/10.2298/JSC131121019J
Jović NG, Calatayud MP, Sanz B, Montone A, Goya GF. Ex situ integration of iron oxide nanoparticles onto exfoliated expanded graphite flakes in aqueous suspension. in Journal of the Serbian Chemical Society. 2014;79(9):1155-1167.
doi:10.2298/JSC131121019J .
Jović, Nataša G., Calatayud, Maria Pilar, Sanz, Beatriz, Montone, Amelia, Goya, Gerardo F., "Ex situ integration of iron oxide nanoparticles onto exfoliated expanded graphite flakes in aqueous suspension" in Journal of the Serbian Chemical Society, 79, no. 9 (2014):1155-1167,
https://doi.org/10.2298/JSC131121019J . .
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Hydrogen sorption properties of MgH2/NaBH4 composites

Kurko, Sandra V.; Aurora, Annalisa; Gattia, Daniele Mirabile; Contini, Vittoria; Montone, Amelia; Rašković-Lovre, Željka; Grbović-Novaković, Jasmina

(2013)

TY  - JOUR
AU  - Kurko, Sandra V.
AU  - Aurora, Annalisa
AU  - Gattia, Daniele Mirabile
AU  - Contini, Vittoria
AU  - Montone, Amelia
AU  - Rašković-Lovre, Željka
AU  - Grbović-Novaković, Jasmina
PY  - 2013
UR  - https://vinar.vin.bg.ac.rs/handle/123456789/5689
AB  - The hydrogen sorption properties of magnesium hydride-sodium borohydride composites prepared by means of high-energy ball milling under Ar atmosphere were investigated. Mutual influence of milling time and the content of NaBH4 were studied. Microstructural and morphological analyses were carried out using X-ray Diffraction (XRD), laser scattering measurements and Scanning Electron Microscopy (SEM), while kinetic analysis and cycling were performed in a Sieverts volumetric apparatus. It has been shown that low content of NaBH4 and short milling time are beneficial for hydrogen sorption kinetics. Copyright (C) 2013, Hydrogen Energy Publications, LLC. Published by Elsevier Ltd. All rights reserved.
T2  - International Journal of Hydrogen Energy
T1  - Hydrogen sorption properties of MgH2/NaBH4 composites
VL  - 38
IS  - 27
SP  - 12140
EP  - 12145
DO  - 10.1016/j.ijhydene.2013.04.075
ER  - 
@article{
author = "Kurko, Sandra V. and Aurora, Annalisa and Gattia, Daniele Mirabile and Contini, Vittoria and Montone, Amelia and Rašković-Lovre, Željka and Grbović-Novaković, Jasmina",
year = "2013",
abstract = "The hydrogen sorption properties of magnesium hydride-sodium borohydride composites prepared by means of high-energy ball milling under Ar atmosphere were investigated. Mutual influence of milling time and the content of NaBH4 were studied. Microstructural and morphological analyses were carried out using X-ray Diffraction (XRD), laser scattering measurements and Scanning Electron Microscopy (SEM), while kinetic analysis and cycling were performed in a Sieverts volumetric apparatus. It has been shown that low content of NaBH4 and short milling time are beneficial for hydrogen sorption kinetics. Copyright (C) 2013, Hydrogen Energy Publications, LLC. Published by Elsevier Ltd. All rights reserved.",
journal = "International Journal of Hydrogen Energy",
title = "Hydrogen sorption properties of MgH2/NaBH4 composites",
volume = "38",
number = "27",
pages = "12140-12145",
doi = "10.1016/j.ijhydene.2013.04.075"
}
Kurko, S. V., Aurora, A., Gattia, D. M., Contini, V., Montone, A., Rašković-Lovre, Ž.,& Grbović-Novaković, J.. (2013). Hydrogen sorption properties of MgH2/NaBH4 composites. in International Journal of Hydrogen Energy, 38(27), 12140-12145.
https://doi.org/10.1016/j.ijhydene.2013.04.075
Kurko SV, Aurora A, Gattia DM, Contini V, Montone A, Rašković-Lovre Ž, Grbović-Novaković J. Hydrogen sorption properties of MgH2/NaBH4 composites. in International Journal of Hydrogen Energy. 2013;38(27):12140-12145.
doi:10.1016/j.ijhydene.2013.04.075 .
Kurko, Sandra V., Aurora, Annalisa, Gattia, Daniele Mirabile, Contini, Vittoria, Montone, Amelia, Rašković-Lovre, Željka, Grbović-Novaković, Jasmina, "Hydrogen sorption properties of MgH2/NaBH4 composites" in International Journal of Hydrogen Energy, 38, no. 27 (2013):12140-12145,
https://doi.org/10.1016/j.ijhydene.2013.04.075 . .
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Structural and Optical Characterization of Flower-Like Rutile Nanostructures Doped with Fe3+

Abazović, Nadica; Čomor, Mirjana; Zec, Slavica; Nedeljković, Jovan; Piscopiello, Emanuela; Montone, Amelia; Antisari, Marco Vittori

(2009)

TY  - JOUR
AU  - Abazović, Nadica
AU  - Čomor, Mirjana
AU  - Zec, Slavica
AU  - Nedeljković, Jovan
AU  - Piscopiello, Emanuela
AU  - Montone, Amelia
AU  - Antisari, Marco Vittori
PY  - 2009
UR  - https://vinar.vin.bg.ac.rs/handle/123456789/3672
AB  - Flower-like agglomerates with sizes of 200-400 nm of pure and Fe3+-doped TiO2 with rutile crystalline structure were synthesized by the coprecipitation method. The morphology of the agglomerates was determined by electron microscopy (TEM and HRTEM). TiO2 agglomerates consist of nanorods with clearly visible crystalline faces, parallel to the axis of elongation whose direction was along the [101] direction of pure TiO2 and the [111] direction of doped TiO2. Furthermore, nanorods consist of chains of spherical particles, most likely interconnected through the so-called oriented attachment or grain-rotation-induced grain coalescence (GRIGC) process. UV/Vis reflection measurements revealed that the absorption of pure TiO2 was significantly shifted from UV toward the visible spectral region upon the incorporation of Fe3+ into the TiO2 host.
T2  - Journal of the American Ceramic Society
T1  - Structural and Optical Characterization of Flower-Like Rutile Nanostructures Doped with Fe3+
VL  - 92
IS  - 4
SP  - 894
EP  - 896
DO  - 10.1111/j.1551-2916.2009.02962.x
ER  - 
@article{
author = "Abazović, Nadica and Čomor, Mirjana and Zec, Slavica and Nedeljković, Jovan and Piscopiello, Emanuela and Montone, Amelia and Antisari, Marco Vittori",
year = "2009",
abstract = "Flower-like agglomerates with sizes of 200-400 nm of pure and Fe3+-doped TiO2 with rutile crystalline structure were synthesized by the coprecipitation method. The morphology of the agglomerates was determined by electron microscopy (TEM and HRTEM). TiO2 agglomerates consist of nanorods with clearly visible crystalline faces, parallel to the axis of elongation whose direction was along the [101] direction of pure TiO2 and the [111] direction of doped TiO2. Furthermore, nanorods consist of chains of spherical particles, most likely interconnected through the so-called oriented attachment or grain-rotation-induced grain coalescence (GRIGC) process. UV/Vis reflection measurements revealed that the absorption of pure TiO2 was significantly shifted from UV toward the visible spectral region upon the incorporation of Fe3+ into the TiO2 host.",
journal = "Journal of the American Ceramic Society",
title = "Structural and Optical Characterization of Flower-Like Rutile Nanostructures Doped with Fe3+",
volume = "92",
number = "4",
pages = "894-896",
doi = "10.1111/j.1551-2916.2009.02962.x"
}
Abazović, N., Čomor, M., Zec, S., Nedeljković, J., Piscopiello, E., Montone, A.,& Antisari, M. V.. (2009). Structural and Optical Characterization of Flower-Like Rutile Nanostructures Doped with Fe3+. in Journal of the American Ceramic Society, 92(4), 894-896.
https://doi.org/10.1111/j.1551-2916.2009.02962.x
Abazović N, Čomor M, Zec S, Nedeljković J, Piscopiello E, Montone A, Antisari MV. Structural and Optical Characterization of Flower-Like Rutile Nanostructures Doped with Fe3+. in Journal of the American Ceramic Society. 2009;92(4):894-896.
doi:10.1111/j.1551-2916.2009.02962.x .
Abazović, Nadica, Čomor, Mirjana, Zec, Slavica, Nedeljković, Jovan, Piscopiello, Emanuela, Montone, Amelia, Antisari, Marco Vittori, "Structural and Optical Characterization of Flower-Like Rutile Nanostructures Doped with Fe3+" in Journal of the American Ceramic Society, 92, no. 4 (2009):894-896,
https://doi.org/10.1111/j.1551-2916.2009.02962.x . .
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TiO2 doped with nitrogen: Synthesis and characterization

Abazović, Nadica; Montone, Amelia; Mirenghi, Luciana; Janković, Ivana A.; Čomor, Mirjana

(2008)

TY  - JOUR
AU  - Abazović, Nadica
AU  - Montone, Amelia
AU  - Mirenghi, Luciana
AU  - Janković, Ivana A.
AU  - Čomor, Mirjana
PY  - 2008
UR  - https://vinar.vin.bg.ac.rs/handle/123456789/6726
AB  - In this study, nitrogen-doped titanium dioxide (TiO2) powders were synthesized in two ways: by heating of titanium hydroxide with urea and by direct hydrolysis of titanium tetraisopropoxicle (TTIP) with ammonium hydroxide. The samples were characterized by structural (XRD), analytical (XPS), optical (UV/Vis absorption/reflection and Raman spectroscopy) and morphological (SEM, TEM) techniques. The characterization suggested that the doped materials have anatase crystalline form without any detectable peaks that correspond to dopants. The absorption threshold of titanium dioxide was moved in the visible range of optical spectrum from 3.2 eV to 2.20 eV. Particle sizes of synthesized powders were obtained from XRD measurements and from TEM data ranging from 6-20 nm. XPS and Raman spectroscopy were used for detection of nitrogen in doped samples.
T2  - Journal of Nanoscience and Nanotechnology
T1  - TiO2 doped with nitrogen: Synthesis and characterization
VL  - 8
IS  - 2
SP  - 613
EP  - 618
DO  - 10.1166/jnn.2008.A226
ER  - 
@article{
author = "Abazović, Nadica and Montone, Amelia and Mirenghi, Luciana and Janković, Ivana A. and Čomor, Mirjana",
year = "2008",
abstract = "In this study, nitrogen-doped titanium dioxide (TiO2) powders were synthesized in two ways: by heating of titanium hydroxide with urea and by direct hydrolysis of titanium tetraisopropoxicle (TTIP) with ammonium hydroxide. The samples were characterized by structural (XRD), analytical (XPS), optical (UV/Vis absorption/reflection and Raman spectroscopy) and morphological (SEM, TEM) techniques. The characterization suggested that the doped materials have anatase crystalline form without any detectable peaks that correspond to dopants. The absorption threshold of titanium dioxide was moved in the visible range of optical spectrum from 3.2 eV to 2.20 eV. Particle sizes of synthesized powders were obtained from XRD measurements and from TEM data ranging from 6-20 nm. XPS and Raman spectroscopy were used for detection of nitrogen in doped samples.",
journal = "Journal of Nanoscience and Nanotechnology",
title = "TiO2 doped with nitrogen: Synthesis and characterization",
volume = "8",
number = "2",
pages = "613-618",
doi = "10.1166/jnn.2008.A226"
}
Abazović, N., Montone, A., Mirenghi, L., Janković, I. A.,& Čomor, M.. (2008). TiO2 doped with nitrogen: Synthesis and characterization. in Journal of Nanoscience and Nanotechnology, 8(2), 613-618.
https://doi.org/10.1166/jnn.2008.A226
Abazović N, Montone A, Mirenghi L, Janković IA, Čomor M. TiO2 doped with nitrogen: Synthesis and characterization. in Journal of Nanoscience and Nanotechnology. 2008;8(2):613-618.
doi:10.1166/jnn.2008.A226 .
Abazović, Nadica, Montone, Amelia, Mirenghi, Luciana, Janković, Ivana A., Čomor, Mirjana, "TiO2 doped with nitrogen: Synthesis and characterization" in Journal of Nanoscience and Nanotechnology, 8, no. 2 (2008):613-618,
https://doi.org/10.1166/jnn.2008.A226 . .
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Combustion Synthesis and Characterization of CeO2 Nanopowder

Šećerov, Bojana Lj.; Andrić, Željka; Abazović, Nadica; Krsmanović, Radenka; Mitrić, Miodrag; Montone, Amelia; Dramićanin, Miroslav

(2008)

TY  - JOUR
AU  - Šećerov, Bojana Lj.
AU  - Andrić, Željka
AU  - Abazović, Nadica
AU  - Krsmanović, Radenka
AU  - Mitrić, Miodrag
AU  - Montone, Amelia
AU  - Dramićanin, Miroslav
PY  - 2008
UR  - https://vinar.vin.bg.ac.rs/handle/123456789/3545
AB  - Modified combustion procedure, named as polymer complex solution method (PCS), was used for synthesis of CeO2 nanopowder. As fuel was employed polyethylene glycol (PEG) with average molecular weight 200. Post-synthesis thermal treatments were done at 800 degrees C for 2 hours. X-ray powder diffraction, electron microscopy (SEM and TEM), laser light scattering, infrared spectroscopy, UV-VIS diffuse reflectance spectroscopy and luminescence spectroscopy were used as characterization methods. The objectives were to investigate the structure and morphology of the synthesized powder, in particular the aggregation and particle size distribution, and its luminescence properties. Photoluminescent properties of CeO2 nanopowder were determined from its emission and excitation spectra. In the excitation spectra two lines were present: one at 322 nm and other at 356 nm. Two lines were also visible in the emission spectra, one at 427 nm and other at 492 nm. Violet emission placed at 427 nm and excitation at 356 nm corresponded to D-5(1) - GT F-4(1) transition of cerium trivalent ion. A UV-VIS diffuse reflectance spectrum shows the absorption edge at 375 nm. The observed spectral blue shift revealed the presence of fine crystallites which escape XRD detection. The presented results demonstrate that this simple preparation technique provides well crystallized nanoparticles of CeO2.
T2  - Acta Chimica Slovenica
T1  - Combustion Synthesis and Characterization of CeO2 Nanopowder
VL  - 55
IS  - 3
SP  - 486
EP  - 491
UR  - https://hdl.handle.net/21.15107/rcub_vinar_3545
ER  - 
@article{
author = "Šećerov, Bojana Lj. and Andrić, Željka and Abazović, Nadica and Krsmanović, Radenka and Mitrić, Miodrag and Montone, Amelia and Dramićanin, Miroslav",
year = "2008",
abstract = "Modified combustion procedure, named as polymer complex solution method (PCS), was used for synthesis of CeO2 nanopowder. As fuel was employed polyethylene glycol (PEG) with average molecular weight 200. Post-synthesis thermal treatments were done at 800 degrees C for 2 hours. X-ray powder diffraction, electron microscopy (SEM and TEM), laser light scattering, infrared spectroscopy, UV-VIS diffuse reflectance spectroscopy and luminescence spectroscopy were used as characterization methods. The objectives were to investigate the structure and morphology of the synthesized powder, in particular the aggregation and particle size distribution, and its luminescence properties. Photoluminescent properties of CeO2 nanopowder were determined from its emission and excitation spectra. In the excitation spectra two lines were present: one at 322 nm and other at 356 nm. Two lines were also visible in the emission spectra, one at 427 nm and other at 492 nm. Violet emission placed at 427 nm and excitation at 356 nm corresponded to D-5(1) - GT F-4(1) transition of cerium trivalent ion. A UV-VIS diffuse reflectance spectrum shows the absorption edge at 375 nm. The observed spectral blue shift revealed the presence of fine crystallites which escape XRD detection. The presented results demonstrate that this simple preparation technique provides well crystallized nanoparticles of CeO2.",
journal = "Acta Chimica Slovenica",
title = "Combustion Synthesis and Characterization of CeO2 Nanopowder",
volume = "55",
number = "3",
pages = "486-491",
url = "https://hdl.handle.net/21.15107/rcub_vinar_3545"
}
Šećerov, B. Lj., Andrić, Ž., Abazović, N., Krsmanović, R., Mitrić, M., Montone, A.,& Dramićanin, M.. (2008). Combustion Synthesis and Characterization of CeO2 Nanopowder. in Acta Chimica Slovenica, 55(3), 486-491.
https://hdl.handle.net/21.15107/rcub_vinar_3545
Šećerov BL, Andrić Ž, Abazović N, Krsmanović R, Mitrić M, Montone A, Dramićanin M. Combustion Synthesis and Characterization of CeO2 Nanopowder. in Acta Chimica Slovenica. 2008;55(3):486-491.
https://hdl.handle.net/21.15107/rcub_vinar_3545 .
Šećerov, Bojana Lj., Andrić, Željka, Abazović, Nadica, Krsmanović, Radenka, Mitrić, Miodrag, Montone, Amelia, Dramićanin, Miroslav, "Combustion Synthesis and Characterization of CeO2 Nanopowder" in Acta Chimica Slovenica, 55, no. 3 (2008):486-491,
https://hdl.handle.net/21.15107/rcub_vinar_3545 .
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