Filipović, Suzana

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Authority KeyName Variants
orcid::0000-0001-6383-8327
  • Filipović, Suzana (45)
Projects
Directed synthesis, structure and properties of multifunctional materials Ministry of Education, Science and Technological Development, Republic of Serbia, Grant no. 451-03-68/2020-14/200175 (Institute of Technical Sciences of SASA, Belgrade)
Ministry of Education, Science and Technological Development, Republic of Serbia, Grant no. 451-03-68/2020-14/200017 (University of Belgrade, Institute of Nuclear Sciences 'Vinča', Belgrade-Vinča) Ministry of Education, Science and Technological Development, Republic of Serbia, Grant no. 451-03-68/2020-14/200116 (University of Belgrade, Faculty of Agriculture)
Investigation of the relation in triad: Synthesis structure-properties for functional materials Synthesis, processing and applications of nanostructured multifunctional materials with defined properties
Serbian Academy of Sciences and Arts [F-7/II] Grant agency of the Czech Republic [15-06390S], Ministry of Education, Youth and Sports of the Czech Republic [LQ1601]
Ministry of Education, Science and Technological Development, Republic of Serbia, Grant no. 451-03-68/2020-14/200026 (University of Belgrade, Institute of Chemistry, Technology and Metallurgy - IChTM) Ministry of Education, Science and Technological Development, Republic of Serbia, Grant no. 451-03-68/2020-14/200103 (University of Belgrade, Faculty of Electrical Engineering)
Ministry of Education, Science and Technological Development, Republic of Serbia, Grant no. 451-03-68/2020-14/200105 (University of Belgrade, Faculty of Mechanical Engineering) Ministry of Education, Science and Technological Development, Republic of Serbia, Grant no. 451-03-68/2020-14/200135 (University of Belgrade, Faculty of Technology and Metallurgy)
Ministry of Education, Science and Technological Development, Republic of Serbia, Grant no. 451-03-68/2020-14/200162 (University of Belgrade, Faculty of Physics) Ministry of Education, Science and Technological Development, Republic of Serbia, Grant no. 451-03-68/2020-14/200288 (Innovation Center of the Faculty of Chemistry)
Zero- to Three-Dimensional Nanostructures for Application in Electronics and Renewable Energy Sources: Synthesis, Characterization and Processing Ministry for Science of the Republic of Serbia [142011 G], Serbian Academy of Sciences and Arts [F-7/II]
Ministry for Science of the Republic of Serbia [G 142011], Serbian Academy of Sciences and Arts [F-198] Ministry of Science and Technology of the Republic of Serbia [142011G], Serbian Academy of Sciences and Arts
Ministry of Science of Republic of Serbia [142011 G], Serbian Academy of Sciences and Arts NASA [NNX09AV07A]
National Science Foundation grants HRD-1345219 and DMR-1523617. NSF CREST [HRD-0833184]
NSF CREST [HRD-0833184], NASA [NNX09AV07A], Serbian Academy of Science and Arts [F/198] NSF-PREM [1523617]
NSF PREM award DMR 11523617 Serbian Academy of Science and Arts [F-198]
Serbian Academy of Science and Arts [F/198], European Regional Development Fund through a project CEITEC [CZ.1.05/1.1.00/02.0068] Serbian Academy of Sciences and Arts [F133]
Serbian Academy of Sciences and Arts https://doi.org/10.13039/501100018992 : F133 Supported by the Department of Energy/National Nuclear Security Administration NA0003979 award.

Author's Bibliography

Effect of the filler morphology on the crystallization behavior and dielectric properties of the polyvinylidene fluoride‐based composite

Filipović, Suzana; Obradović, Nina; Corlett, Cole; Fahrenholtz, William G.; Rosenschon, Martin; Füglein, Ekkehard; Dojčilović, Radovan; Tošić, Dragana; Petrović, Jovana; Đorđević, Antonije; Vlahović, Branislav; Pavlović, Vladimir B.

(2023)

TY  - JOUR
AU  - Filipović, Suzana
AU  - Obradović, Nina
AU  - Corlett, Cole
AU  - Fahrenholtz, William G.
AU  - Rosenschon, Martin
AU  - Füglein, Ekkehard
AU  - Dojčilović, Radovan
AU  - Tošić, Dragana
AU  - Petrović, Jovana
AU  - Đorđević, Antonije
AU  - Vlahović, Branislav
AU  - Pavlović, Vladimir B.
PY  - 2023
UR  - https://vinar.vin.bg.ac.rs/handle/123456789/12400
AB  - Ceramic/polymer composites can be chemically stable, mechanically strong, and flexible, which make them candidates for electric devices, such as pressure or temperature sensors, energy storage or harvesting devices, actuators, and so forth. Depending on the application, various electrical properties are of importance. Polymers usually have low dielectric permittivity, but increased dielectric permittivity can be achieved by the addition of the ceramic fillers with high dielectric constant. With the aim to enhance dielectric properties of the composite without loss of flexibility, 5 wt% of BaTiO3-Fe2O3 powder was added into a polyvinylidene fluoride matrix. The powder was prepared by different synthesis conditions to produce core/shell structures. The effect of the phase composition and morphology of the BaTiO3-Fe2O3 core/shell filler on the structure and lattice dynamics of the polymer composites was investigated. Based on the results of the thermal analysis, various parameters of ceramic/polymer composites were determined. Differences in the phase composition and morphology of the filler have an influence on the formation of various polyvinylidene fluoride allomorphs and the degree of crystallinity. Furthermore, the dielectric performances of pure polyvinylidene fluoride and the polymer/ceramic composites were measured.
T2  - Journal of Applied Polymer Science
T1  - Effect of the filler morphology on the crystallization behavior and dielectric properties of the polyvinylidene fluoride‐based composite
DO  - 10.1002/app.55040
ER  - 
@article{
author = "Filipović, Suzana and Obradović, Nina and Corlett, Cole and Fahrenholtz, William G. and Rosenschon, Martin and Füglein, Ekkehard and Dojčilović, Radovan and Tošić, Dragana and Petrović, Jovana and Đorđević, Antonije and Vlahović, Branislav and Pavlović, Vladimir B.",
year = "2023",
abstract = "Ceramic/polymer composites can be chemically stable, mechanically strong, and flexible, which make them candidates for electric devices, such as pressure or temperature sensors, energy storage or harvesting devices, actuators, and so forth. Depending on the application, various electrical properties are of importance. Polymers usually have low dielectric permittivity, but increased dielectric permittivity can be achieved by the addition of the ceramic fillers with high dielectric constant. With the aim to enhance dielectric properties of the composite without loss of flexibility, 5 wt% of BaTiO3-Fe2O3 powder was added into a polyvinylidene fluoride matrix. The powder was prepared by different synthesis conditions to produce core/shell structures. The effect of the phase composition and morphology of the BaTiO3-Fe2O3 core/shell filler on the structure and lattice dynamics of the polymer composites was investigated. Based on the results of the thermal analysis, various parameters of ceramic/polymer composites were determined. Differences in the phase composition and morphology of the filler have an influence on the formation of various polyvinylidene fluoride allomorphs and the degree of crystallinity. Furthermore, the dielectric performances of pure polyvinylidene fluoride and the polymer/ceramic composites were measured.",
journal = "Journal of Applied Polymer Science",
title = "Effect of the filler morphology on the crystallization behavior and dielectric properties of the polyvinylidene fluoride‐based composite",
doi = "10.1002/app.55040"
}
Filipović, S., Obradović, N., Corlett, C., Fahrenholtz, W. G., Rosenschon, M., Füglein, E., Dojčilović, R., Tošić, D., Petrović, J., Đorđević, A., Vlahović, B.,& Pavlović, V. B.. (2023). Effect of the filler morphology on the crystallization behavior and dielectric properties of the polyvinylidene fluoride‐based composite. in Journal of Applied Polymer Science.
https://doi.org/10.1002/app.55040
Filipović S, Obradović N, Corlett C, Fahrenholtz WG, Rosenschon M, Füglein E, Dojčilović R, Tošić D, Petrović J, Đorđević A, Vlahović B, Pavlović VB. Effect of the filler morphology on the crystallization behavior and dielectric properties of the polyvinylidene fluoride‐based composite. in Journal of Applied Polymer Science. 2023;.
doi:10.1002/app.55040 .
Filipović, Suzana, Obradović, Nina, Corlett, Cole, Fahrenholtz, William G., Rosenschon, Martin, Füglein, Ekkehard, Dojčilović, Radovan, Tošić, Dragana, Petrović, Jovana, Đorđević, Antonije, Vlahović, Branislav, Pavlović, Vladimir B., "Effect of the filler morphology on the crystallization behavior and dielectric properties of the polyvinylidene fluoride‐based composite" in Journal of Applied Polymer Science (2023),
https://doi.org/10.1002/app.55040 . .

Dielectric and Structural Properties of the Hybrid Material Polyvinylidene Fluoride-Bacterial Nanocellulose-Based Composite

Janićijević, Aleksandra; Filipović, Suzana; Sknepnek, Aleksandra; Vlahović, Branislav; Đorđević, Nenad; Kovacević, Danijela; Mirković, Miljana; Petronijević, Ivan; Zivković, Predrag; Rogan, Jelena; Pavlović, Vladimir B.

(2023)

TY  - JOUR
AU  - Janićijević, Aleksandra
AU  - Filipović, Suzana
AU  - Sknepnek, Aleksandra
AU  - Vlahović, Branislav
AU  - Đorđević, Nenad
AU  - Kovacević, Danijela
AU  - Mirković, Miljana
AU  - Petronijević, Ivan
AU  - Zivković, Predrag
AU  - Rogan, Jelena
AU  - Pavlović, Vladimir B.
PY  - 2023
UR  - https://vinar.vin.bg.ac.rs/handle/123456789/11872
AB  - In the search for environmentally friendly materials with a wide range of properties, polymer composites have emerged as a promising alternative due to their multifunctional properties. This study focuses on the synthesis of composite materials consisting of four components: bacterial nanocellulose (BNC) modified with magnetic Fe3O4 , and a mixture of BaTiO3 (BT) and polyvinylidene fluoride (PVDF). The BT powder was mechanically activated prior to mixing with PVDF. The influence of BT mechanical activation and BNC with magnetic particles on the PVDF matrix was investigated. The obtained composite films’ structural characteristics, morphology, and dielectric properties are presented. This research provides insights into the relationship between mechanical activation of the filler and structural and dielectric properties in the PVDF/BT/BNC/Fe3O4 system, creating the way for the development of materials with a wide range of diverse properties that support the concept of green technologies.
T2  - Polymers
T1  - Dielectric and Structural Properties of the Hybrid Material Polyvinylidene Fluoride-Bacterial Nanocellulose-Based Composite
VL  - 15
IS  - 20
SP  - 4080
DO  - 10.3390/polym15204080
ER  - 
@article{
author = "Janićijević, Aleksandra and Filipović, Suzana and Sknepnek, Aleksandra and Vlahović, Branislav and Đorđević, Nenad and Kovacević, Danijela and Mirković, Miljana and Petronijević, Ivan and Zivković, Predrag and Rogan, Jelena and Pavlović, Vladimir B.",
year = "2023",
abstract = "In the search for environmentally friendly materials with a wide range of properties, polymer composites have emerged as a promising alternative due to their multifunctional properties. This study focuses on the synthesis of composite materials consisting of four components: bacterial nanocellulose (BNC) modified with magnetic Fe3O4 , and a mixture of BaTiO3 (BT) and polyvinylidene fluoride (PVDF). The BT powder was mechanically activated prior to mixing with PVDF. The influence of BT mechanical activation and BNC with magnetic particles on the PVDF matrix was investigated. The obtained composite films’ structural characteristics, morphology, and dielectric properties are presented. This research provides insights into the relationship between mechanical activation of the filler and structural and dielectric properties in the PVDF/BT/BNC/Fe3O4 system, creating the way for the development of materials with a wide range of diverse properties that support the concept of green technologies.",
journal = "Polymers",
title = "Dielectric and Structural Properties of the Hybrid Material Polyvinylidene Fluoride-Bacterial Nanocellulose-Based Composite",
volume = "15",
number = "20",
pages = "4080",
doi = "10.3390/polym15204080"
}
Janićijević, A., Filipović, S., Sknepnek, A., Vlahović, B., Đorđević, N., Kovacević, D., Mirković, M., Petronijević, I., Zivković, P., Rogan, J.,& Pavlović, V. B.. (2023). Dielectric and Structural Properties of the Hybrid Material Polyvinylidene Fluoride-Bacterial Nanocellulose-Based Composite. in Polymers, 15(20), 4080.
https://doi.org/10.3390/polym15204080
Janićijević A, Filipović S, Sknepnek A, Vlahović B, Đorđević N, Kovacević D, Mirković M, Petronijević I, Zivković P, Rogan J, Pavlović VB. Dielectric and Structural Properties of the Hybrid Material Polyvinylidene Fluoride-Bacterial Nanocellulose-Based Composite. in Polymers. 2023;15(20):4080.
doi:10.3390/polym15204080 .
Janićijević, Aleksandra, Filipović, Suzana, Sknepnek, Aleksandra, Vlahović, Branislav, Đorđević, Nenad, Kovacević, Danijela, Mirković, Miljana, Petronijević, Ivan, Zivković, Predrag, Rogan, Jelena, Pavlović, Vladimir B., "Dielectric and Structural Properties of the Hybrid Material Polyvinylidene Fluoride-Bacterial Nanocellulose-Based Composite" in Polymers, 15, no. 20 (2023):4080,
https://doi.org/10.3390/polym15204080 . .

Hydroxyapatite/TiO2 Nanomaterial with Defined Microstructural and Good Antimicrobial Properties

Mirković, Miljana M.; Filipović, Suzana; Kalijadis, Ana; Mašković, Pavle; Mašković, Jelena; Vlahović, Branislav; Pavlović, Vladimir B.

(2022)

TY  - JOUR
AU  - Mirković, Miljana M.
AU  - Filipović, Suzana
AU  - Kalijadis, Ana
AU  - Mašković, Pavle
AU  - Mašković, Jelena
AU  - Vlahović, Branislav
AU  - Pavlović, Vladimir B.
PY  - 2022
UR  - https://vinar.vin.bg.ac.rs/handle/123456789/10270
AB  - Due to the growing number of people infected with the new coronavirus globally, which weakens immunity, there has been an increase in bacterial infections. Hence, knowledge about simple and low-cost synthesis methods of materials with good structural and antimicrobial properties is of great importance. A material obtained through the combination of a nanoscale hydroxyapatite material (with good biocompatibility) and titanium dioxide (with good degradation properties of organic molecules) can absorb and decompose bacteria. In this investigation, three different synthesis routes used to prepare hydroxyapatite/titanium dioxide nanomaterials are examined. The morphology and semiquantitative chemical composition are characterized by scanning electron microscopy with energy dispersive X-ray analysis (SEM-EDX). The obtained materials’ phase and structural characterization are determined using the X-ray powder diffraction method (XRD). The crystallite sizes of the obtained materials are in the range of 8 nm to 15 nm. Based on XRD peak positions, the hexagonal hydroxyapatite phases are formed in all samples along with TiO2 anatase and rutile phases. According to SEM and TEM analyses, the morphology of the prepared samples differs depending on the synthesis route. The EDX analysis confirmed the presence of Ti, Ca, P, and O in the obtained materials. The IR spectroscopy verified the vibration bands characteristic for HAp and titanium. The investigated materials show excellent antimicrobial and photocatalytic properties.
T2  - Antibiotics
T1  - Hydroxyapatite/TiO2 Nanomaterial with Defined Microstructural and Good Antimicrobial Properties
VL  - 11
IS  - 5
SP  - 592
DO  - 10.3390/antibiotics11050592
ER  - 
@article{
author = "Mirković, Miljana M. and Filipović, Suzana and Kalijadis, Ana and Mašković, Pavle and Mašković, Jelena and Vlahović, Branislav and Pavlović, Vladimir B.",
year = "2022",
abstract = "Due to the growing number of people infected with the new coronavirus globally, which weakens immunity, there has been an increase in bacterial infections. Hence, knowledge about simple and low-cost synthesis methods of materials with good structural and antimicrobial properties is of great importance. A material obtained through the combination of a nanoscale hydroxyapatite material (with good biocompatibility) and titanium dioxide (with good degradation properties of organic molecules) can absorb and decompose bacteria. In this investigation, three different synthesis routes used to prepare hydroxyapatite/titanium dioxide nanomaterials are examined. The morphology and semiquantitative chemical composition are characterized by scanning electron microscopy with energy dispersive X-ray analysis (SEM-EDX). The obtained materials’ phase and structural characterization are determined using the X-ray powder diffraction method (XRD). The crystallite sizes of the obtained materials are in the range of 8 nm to 15 nm. Based on XRD peak positions, the hexagonal hydroxyapatite phases are formed in all samples along with TiO2 anatase and rutile phases. According to SEM and TEM analyses, the morphology of the prepared samples differs depending on the synthesis route. The EDX analysis confirmed the presence of Ti, Ca, P, and O in the obtained materials. The IR spectroscopy verified the vibration bands characteristic for HAp and titanium. The investigated materials show excellent antimicrobial and photocatalytic properties.",
journal = "Antibiotics",
title = "Hydroxyapatite/TiO2 Nanomaterial with Defined Microstructural and Good Antimicrobial Properties",
volume = "11",
number = "5",
pages = "592",
doi = "10.3390/antibiotics11050592"
}
Mirković, M. M., Filipović, S., Kalijadis, A., Mašković, P., Mašković, J., Vlahović, B.,& Pavlović, V. B.. (2022). Hydroxyapatite/TiO2 Nanomaterial with Defined Microstructural and Good Antimicrobial Properties. in Antibiotics, 11(5), 592.
https://doi.org/10.3390/antibiotics11050592
Mirković MM, Filipović S, Kalijadis A, Mašković P, Mašković J, Vlahović B, Pavlović VB. Hydroxyapatite/TiO2 Nanomaterial with Defined Microstructural and Good Antimicrobial Properties. in Antibiotics. 2022;11(5):592.
doi:10.3390/antibiotics11050592 .
Mirković, Miljana M., Filipović, Suzana, Kalijadis, Ana, Mašković, Pavle, Mašković, Jelena, Vlahović, Branislav, Pavlović, Vladimir B., "Hydroxyapatite/TiO2 Nanomaterial with Defined Microstructural and Good Antimicrobial Properties" in Antibiotics, 11, no. 5 (2022):592,
https://doi.org/10.3390/antibiotics11050592 . .
10
9

Structural Characterization of Nanocellulose/Fe3O4 Hybrid Nanomaterials

Janićijević, Aleksandra; Pavlović, Vera P.; Kovačević, Danijela; Perić, Marko; Vlahović, Branislav; Pavlović, Vladimir B.; Filipović, Suzana

(2022)

TY  - JOUR
AU  - Janićijević, Aleksandra
AU  - Pavlović, Vera P.
AU  - Kovačević, Danijela
AU  - Perić, Marko
AU  - Vlahović, Branislav
AU  - Pavlović, Vladimir B.
AU  - Filipović, Suzana
PY  - 2022
UR  - https://vinar.vin.bg.ac.rs/handle/123456789/10269
AB  - The rise of innovation in the electrical industry is driven by the controlled design of new materials. The hybrid materials based on magnetite/nanocellulose are highly interesting due to their various applications in medicine, ecology, catalysis and electronics. In this study, the structure and morphology of nanocellulose/magnetite hybrid nanomaterials were investigated. The effect of nanocellulose loading on the crystal structure of synthesized composites was investigated by XRD and FTIR methods. The presented study reveals that the interaction between the cellulose and magnetic nanoparticles depends on the nanocellulose content. Further, a transition from cellulose II to cellulose I allomorph is observed. SEM and EDS are employed to determine the variation in morphology with changes in component concentrations. By the calculation of magnetic interactions between adjacent Fe3+ and Fe2+ ions within composites, it is determined that ferromagnetic coupling predominates.
T2  - Polymers
T1  - Structural Characterization of Nanocellulose/Fe3O4 Hybrid Nanomaterials
VL  - 14
IS  - 9
SP  - 1819
DO  - 10.3390/polym14091819
ER  - 
@article{
author = "Janićijević, Aleksandra and Pavlović, Vera P. and Kovačević, Danijela and Perić, Marko and Vlahović, Branislav and Pavlović, Vladimir B. and Filipović, Suzana",
year = "2022",
abstract = "The rise of innovation in the electrical industry is driven by the controlled design of new materials. The hybrid materials based on magnetite/nanocellulose are highly interesting due to their various applications in medicine, ecology, catalysis and electronics. In this study, the structure and morphology of nanocellulose/magnetite hybrid nanomaterials were investigated. The effect of nanocellulose loading on the crystal structure of synthesized composites was investigated by XRD and FTIR methods. The presented study reveals that the interaction between the cellulose and magnetic nanoparticles depends on the nanocellulose content. Further, a transition from cellulose II to cellulose I allomorph is observed. SEM and EDS are employed to determine the variation in morphology with changes in component concentrations. By the calculation of magnetic interactions between adjacent Fe3+ and Fe2+ ions within composites, it is determined that ferromagnetic coupling predominates.",
journal = "Polymers",
title = "Structural Characterization of Nanocellulose/Fe3O4 Hybrid Nanomaterials",
volume = "14",
number = "9",
pages = "1819",
doi = "10.3390/polym14091819"
}
Janićijević, A., Pavlović, V. P., Kovačević, D., Perić, M., Vlahović, B., Pavlović, V. B.,& Filipović, S.. (2022). Structural Characterization of Nanocellulose/Fe3O4 Hybrid Nanomaterials. in Polymers, 14(9), 1819.
https://doi.org/10.3390/polym14091819
Janićijević A, Pavlović VP, Kovačević D, Perić M, Vlahović B, Pavlović VB, Filipović S. Structural Characterization of Nanocellulose/Fe3O4 Hybrid Nanomaterials. in Polymers. 2022;14(9):1819.
doi:10.3390/polym14091819 .
Janićijević, Aleksandra, Pavlović, Vera P., Kovačević, Danijela, Perić, Marko, Vlahović, Branislav, Pavlović, Vladimir B., Filipović, Suzana, "Structural Characterization of Nanocellulose/Fe3O4 Hybrid Nanomaterials" in Polymers, 14, no. 9 (2022):1819,
https://doi.org/10.3390/polym14091819 . .
7
4

Effect of high energy ball milling on sintering of MgO-TiO2 system

Filipović, Suzana; Obradović, Nina; Fahrenholtz, William G.; Smith, Steven; Mirković, M.; Peleš, Adriana; Tadić, Nenad; Đorđević, Antonije

(Belgrade : Serbian Ceramic Society, 2022)

TY  - CONF
AU  - Filipović, Suzana
AU  - Obradović, Nina
AU  - Fahrenholtz, William G.
AU  - Smith, Steven
AU  - Mirković, M.
AU  - Peleš, Adriana
AU  - Tadić, Nenad
AU  - Đorđević, Antonije
PY  - 2022
UR  - https://vinar.vin.bg.ac.rs/handle/123456789/10825
AB  - Perovskite ceramic material based on MgTiO3 is used in various types of electronic devices owing to its dielectric properties, high dielectric constant, and low losses. These features can be tailored by setting preparation conditions. Densification of magnesium titanate by Spark Plasma Sintering (SPS) was the aim of this work. First, the mechanical activation in the highenergy ball mill was applied on the powder of MgO-TiO2 mixed in mole ratio 1:1. Prepared powder mixtures, activated for different times, were SPS sintered, at 1200 o C with a heating rate of 100o C/min. After reaching the desired temperature, a uniaxial pressure of 50 MPa was applied, and dwelled at this condition for 5 min, followed by cooling to room temperature at 5o C/min. The starting powders, activated mixtures, and sintered ceramics bodies were investigated by X-ray diffraction, scanning electron microscopy (SEM), and energy dispersive spectroscopy (EDS). The presence of the MgTi2O5 phase was noticed for the nonmilled ceramics. In the samples obtained from milled powders, MgTi2O5 was detected in EDS spectra in a lower amount, below the threshold of the XRD method. Dielectric measurements were performed at a wide range of frequencies and temperatures. The highest value of the hardness was obtained from powder milled for 15 min before SPS.
PB  - Belgrade : Serbian Ceramic Society
C3  - Advanced Ceramics and Application : 10th Serbian Ceramic Society Conference : program and the book of abstracts; September 26-27, 2022; Belgrade
T1  - Effect of high energy ball milling on sintering of MgO-TiO2 system
SP  - 88
UR  - https://hdl.handle.net/21.15107/rcub_vinar_10825
ER  - 
@conference{
author = "Filipović, Suzana and Obradović, Nina and Fahrenholtz, William G. and Smith, Steven and Mirković, M. and Peleš, Adriana and Tadić, Nenad and Đorđević, Antonije",
year = "2022",
abstract = "Perovskite ceramic material based on MgTiO3 is used in various types of electronic devices owing to its dielectric properties, high dielectric constant, and low losses. These features can be tailored by setting preparation conditions. Densification of magnesium titanate by Spark Plasma Sintering (SPS) was the aim of this work. First, the mechanical activation in the highenergy ball mill was applied on the powder of MgO-TiO2 mixed in mole ratio 1:1. Prepared powder mixtures, activated for different times, were SPS sintered, at 1200 o C with a heating rate of 100o C/min. After reaching the desired temperature, a uniaxial pressure of 50 MPa was applied, and dwelled at this condition for 5 min, followed by cooling to room temperature at 5o C/min. The starting powders, activated mixtures, and sintered ceramics bodies were investigated by X-ray diffraction, scanning electron microscopy (SEM), and energy dispersive spectroscopy (EDS). The presence of the MgTi2O5 phase was noticed for the nonmilled ceramics. In the samples obtained from milled powders, MgTi2O5 was detected in EDS spectra in a lower amount, below the threshold of the XRD method. Dielectric measurements were performed at a wide range of frequencies and temperatures. The highest value of the hardness was obtained from powder milled for 15 min before SPS.",
publisher = "Belgrade : Serbian Ceramic Society",
journal = "Advanced Ceramics and Application : 10th Serbian Ceramic Society Conference : program and the book of abstracts; September 26-27, 2022; Belgrade",
title = "Effect of high energy ball milling on sintering of MgO-TiO2 system",
pages = "88",
url = "https://hdl.handle.net/21.15107/rcub_vinar_10825"
}
Filipović, S., Obradović, N., Fahrenholtz, W. G., Smith, S., Mirković, M., Peleš, A., Tadić, N.,& Đorđević, A.. (2022). Effect of high energy ball milling on sintering of MgO-TiO2 system. in Advanced Ceramics and Application : 10th Serbian Ceramic Society Conference : program and the book of abstracts; September 26-27, 2022; Belgrade
Belgrade : Serbian Ceramic Society., 88.
https://hdl.handle.net/21.15107/rcub_vinar_10825
Filipović S, Obradović N, Fahrenholtz WG, Smith S, Mirković M, Peleš A, Tadić N, Đorđević A. Effect of high energy ball milling on sintering of MgO-TiO2 system. in Advanced Ceramics and Application : 10th Serbian Ceramic Society Conference : program and the book of abstracts; September 26-27, 2022; Belgrade. 2022;:88.
https://hdl.handle.net/21.15107/rcub_vinar_10825 .
Filipović, Suzana, Obradović, Nina, Fahrenholtz, William G., Smith, Steven, Mirković, M., Peleš, Adriana, Tadić, Nenad, Đorđević, Antonije, "Effect of high energy ball milling on sintering of MgO-TiO2 system" in Advanced Ceramics and Application : 10th Serbian Ceramic Society Conference : program and the book of abstracts; September 26-27, 2022; Belgrade (2022):88,
https://hdl.handle.net/21.15107/rcub_vinar_10825 .

Multiferroic heterostructure BaTiO3/ε-Fe2O3 composite obtained by in situ reaction

Filipović, Suzana; Obradović, Nina; Anđelković, Ljubica; Olćan, Dragan; Petrović, Jovana S.; Mirković, Miljana M.; Pavlović, Vladimir B.; Jeremić, Dejan; Vlahović, Branislav; Đorđević, Antonije

(2021)

TY  - JOUR
AU  - Filipović, Suzana
AU  - Obradović, Nina
AU  - Anđelković, Ljubica
AU  - Olćan, Dragan
AU  - Petrović, Jovana S.
AU  - Mirković, Miljana M.
AU  - Pavlović, Vladimir B.
AU  - Jeremić, Dejan
AU  - Vlahović, Branislav
AU  - Đorđević, Antonije
PY  - 2021
UR  - https://vinar.vin.bg.ac.rs/handle/123456789/9410
AB  - Solid-state reaction between BaTiO3and Fe2O3was used to produce a multiferroic heterostructure composite. Commercial BaTiO3and Fe(NO3)3•9H2O were suspended in ethanol for 30 minutes in an ultrasound bath. The prepared mixture was thermally processed at 300°C for 6 h. Sintering at 1300 °C for 1 h resulted in a mixture of different phases, BaTiO3, BaFe12O19and Ba12Ti28Fe15O84, which were confirmed by x-ray powder diffraction. A dense microstructure with a small volume fraction of closed porosity was indicated by the scanning electron microscopy, while a homogeneous distribution of Fe ions over BaTiO3phase was visible from energy dispersive spectroscopy mapping. Doping of BaTiO3with Fe2O3resulted in formation of magnetic hexaferrite phases, as confirmed by dielectric measurements that showed a broadened maximum of the permittivity measured as a function of temperature. © 2021 Authors. Published by association for ETRAN Society.
T2  - Science of Sintering
T1  - Multiferroic heterostructure BaTiO3/ε-Fe2O3 composite obtained by in situ reaction
VL  - 53
IS  - 1
SP  - 1
EP  - 8
DO  - 10.2298/SOS2101001F
ER  - 
@article{
author = "Filipović, Suzana and Obradović, Nina and Anđelković, Ljubica and Olćan, Dragan and Petrović, Jovana S. and Mirković, Miljana M. and Pavlović, Vladimir B. and Jeremić, Dejan and Vlahović, Branislav and Đorđević, Antonije",
year = "2021",
abstract = "Solid-state reaction between BaTiO3and Fe2O3was used to produce a multiferroic heterostructure composite. Commercial BaTiO3and Fe(NO3)3•9H2O were suspended in ethanol for 30 minutes in an ultrasound bath. The prepared mixture was thermally processed at 300°C for 6 h. Sintering at 1300 °C for 1 h resulted in a mixture of different phases, BaTiO3, BaFe12O19and Ba12Ti28Fe15O84, which were confirmed by x-ray powder diffraction. A dense microstructure with a small volume fraction of closed porosity was indicated by the scanning electron microscopy, while a homogeneous distribution of Fe ions over BaTiO3phase was visible from energy dispersive spectroscopy mapping. Doping of BaTiO3with Fe2O3resulted in formation of magnetic hexaferrite phases, as confirmed by dielectric measurements that showed a broadened maximum of the permittivity measured as a function of temperature. © 2021 Authors. Published by association for ETRAN Society.",
journal = "Science of Sintering",
title = "Multiferroic heterostructure BaTiO3/ε-Fe2O3 composite obtained by in situ reaction",
volume = "53",
number = "1",
pages = "1-8",
doi = "10.2298/SOS2101001F"
}
Filipović, S., Obradović, N., Anđelković, L., Olćan, D., Petrović, J. S., Mirković, M. M., Pavlović, V. B., Jeremić, D., Vlahović, B.,& Đorđević, A.. (2021). Multiferroic heterostructure BaTiO3/ε-Fe2O3 composite obtained by in situ reaction. in Science of Sintering, 53(1), 1-8.
https://doi.org/10.2298/SOS2101001F
Filipović S, Obradović N, Anđelković L, Olćan D, Petrović JS, Mirković MM, Pavlović VB, Jeremić D, Vlahović B, Đorđević A. Multiferroic heterostructure BaTiO3/ε-Fe2O3 composite obtained by in situ reaction. in Science of Sintering. 2021;53(1):1-8.
doi:10.2298/SOS2101001F .
Filipović, Suzana, Obradović, Nina, Anđelković, Ljubica, Olćan, Dragan, Petrović, Jovana S., Mirković, Miljana M., Pavlović, Vladimir B., Jeremić, Dejan, Vlahović, Branislav, Đorđević, Antonije, "Multiferroic heterostructure BaTiO3/ε-Fe2O3 composite obtained by in situ reaction" in Science of Sintering, 53, no. 1 (2021):1-8,
https://doi.org/10.2298/SOS2101001F . .
2
1
4

Effect of prolonged precipitation on morphology and crystal struture of the bacterial nanocelulose/Fe3O4 composite

Janićijević, Aleksandra; Pavlović, Vladimir B.; Sknepnek, A.; Mirković, Miljana M.; Kovačević, D.; Đorđević, Nataša; Filipović, Suzana

(Belgrade : Serbian Ceramic Society, 2021)

TY  - CONF
AU  - Janićijević, Aleksandra
AU  - Pavlović, Vladimir B.
AU  - Sknepnek, A.
AU  - Mirković, Miljana M.
AU  - Kovačević, D.
AU  - Đorđević, Nataša
AU  - Filipović, Suzana
PY  - 2021
UR  - https://vinar.vin.bg.ac.rs/handle/123456789/10792
AB  - Cellulose is a biopolymer with a wide range of properties like biocompatibility, hydrophilicity, porosity, good mechanical properties, biodegradability and non-toxicity. The properties and application of cellulose based materials are related to the source of the cellulose production. Despite the fact that the plant cellulose is playing a leading role in obtaining cellulose fibers, it has been found that ecologically and economically, a better source for obtaining cellulose is by fermenting a particular strain of bacteria. Although bacterial nano cellulose (BCN) based materials can be used in numerous industries, from the paper and food industries to biomedicine, their application in electronics is limited because bacterial cellulose does not have conductive and ferromagnetic properties. Having this in mind in this research, the results of the development of nanocomposite materials based on BCN modified with Fe3O4 has been presented. The differences in the interaction of Fe3O4 nanoparticles and BCN obtained by varying precipitation parameters were investigated and the effect of reaction time was followed by SEM-EDS, XRD, and FTIR analysis. It has been found that this type of modifications of the initial BCN, enables development of new composite materials with superior properties, which can be used in various fields of electronics.
PB  - Belgrade : Serbian Ceramic Society
C3  - Advanced Ceramics and Application : 9th Serbian Ceramic Society Conference : program and the book of abstracts; September 20-21, 2021; Belgrade
T1  - Effect of prolonged precipitation on morphology and crystal struture of the bacterial nanocelulose/Fe3O4 composite
SP  - 55
EP  - 56
UR  - https://hdl.handle.net/21.15107/rcub_vinar_10792
ER  - 
@conference{
author = "Janićijević, Aleksandra and Pavlović, Vladimir B. and Sknepnek, A. and Mirković, Miljana M. and Kovačević, D. and Đorđević, Nataša and Filipović, Suzana",
year = "2021",
abstract = "Cellulose is a biopolymer with a wide range of properties like biocompatibility, hydrophilicity, porosity, good mechanical properties, biodegradability and non-toxicity. The properties and application of cellulose based materials are related to the source of the cellulose production. Despite the fact that the plant cellulose is playing a leading role in obtaining cellulose fibers, it has been found that ecologically and economically, a better source for obtaining cellulose is by fermenting a particular strain of bacteria. Although bacterial nano cellulose (BCN) based materials can be used in numerous industries, from the paper and food industries to biomedicine, their application in electronics is limited because bacterial cellulose does not have conductive and ferromagnetic properties. Having this in mind in this research, the results of the development of nanocomposite materials based on BCN modified with Fe3O4 has been presented. The differences in the interaction of Fe3O4 nanoparticles and BCN obtained by varying precipitation parameters were investigated and the effect of reaction time was followed by SEM-EDS, XRD, and FTIR analysis. It has been found that this type of modifications of the initial BCN, enables development of new composite materials with superior properties, which can be used in various fields of electronics.",
publisher = "Belgrade : Serbian Ceramic Society",
journal = "Advanced Ceramics and Application : 9th Serbian Ceramic Society Conference : program and the book of abstracts; September 20-21, 2021; Belgrade",
title = "Effect of prolonged precipitation on morphology and crystal struture of the bacterial nanocelulose/Fe3O4 composite",
pages = "55-56",
url = "https://hdl.handle.net/21.15107/rcub_vinar_10792"
}
Janićijević, A., Pavlović, V. B., Sknepnek, A., Mirković, M. M., Kovačević, D., Đorđević, N.,& Filipović, S.. (2021). Effect of prolonged precipitation on morphology and crystal struture of the bacterial nanocelulose/Fe3O4 composite. in Advanced Ceramics and Application : 9th Serbian Ceramic Society Conference : program and the book of abstracts; September 20-21, 2021; Belgrade
Belgrade : Serbian Ceramic Society., 55-56.
https://hdl.handle.net/21.15107/rcub_vinar_10792
Janićijević A, Pavlović VB, Sknepnek A, Mirković MM, Kovačević D, Đorđević N, Filipović S. Effect of prolonged precipitation on morphology and crystal struture of the bacterial nanocelulose/Fe3O4 composite. in Advanced Ceramics and Application : 9th Serbian Ceramic Society Conference : program and the book of abstracts; September 20-21, 2021; Belgrade. 2021;:55-56.
https://hdl.handle.net/21.15107/rcub_vinar_10792 .
Janićijević, Aleksandra, Pavlović, Vladimir B., Sknepnek, A., Mirković, Miljana M., Kovačević, D., Đorđević, Nataša, Filipović, Suzana, "Effect of prolonged precipitation on morphology and crystal struture of the bacterial nanocelulose/Fe3O4 composite" in Advanced Ceramics and Application : 9th Serbian Ceramic Society Conference : program and the book of abstracts; September 20-21, 2021; Belgrade (2021):55-56,
https://hdl.handle.net/21.15107/rcub_vinar_10792 .

Enhanced dielectric properties of PVDF-based composites with BaTiO3 ceramic decorated with Fe2O3

Filipović, Suzana; Obradović, Nina; Rosenschon, M.; Füglein, E.; Dojčilović, Radovan; Đorđević, Antonije; Petrović, J.; Pavlović, Vladimir B.

(Belgrade : Serbian Ceramic Society, 2021)

TY  - CONF
AU  - Filipović, Suzana
AU  - Obradović, Nina
AU  - Rosenschon, M.
AU  - Füglein, E.
AU  - Dojčilović, Radovan
AU  - Đorđević, Antonije
AU  - Petrović, J.
AU  - Pavlović, Vladimir B.
PY  - 2021
UR  - https://vinar.vin.bg.ac.rs/handle/123456789/10796
AB  - The increase in the utilization of ceramic/polymer composites as components for electric devices is mainly based on their high chemical stability, mechanical strength, and flexibility. The polymers usually have poor dielectric performances. In order to increase the dielectric permittivity, ceramic fillers with high dielectric constant have been used as active fillers, and usually in large amounts, which have a detrimental effect on the mechanical properties of the composite. With the aim to enhance the dielectric properties of the composite without loss of polymer’s flexibility, 5 wt.% of BaTiO3/Fe2O3 core/shell powders, prepared by different synthesis conditions, was added into the PVDF matrix. The effect of the phase composition and morphology of the starting BaTiO3/Fe2O3 core/shell filler on the crystal structure and lattice dynamics was investigated. Based on the results of the thermal analysis, TG/DSC, various parameters of ceramic/polymer composites were determined. We were able to corroborate that differences in the phase composition and morphology of BaTiO3/Fe2O3 core/shell filler have an influence on the formation of various PVDF allomorph modifications, as well as the level of crystallinity. The dielectric performances of the pure PVDF and polymer/ceramic composites were measured. An enhancement in the dielectric permittivity and decrease in the loss tangent were revealed.
PB  - Belgrade : Serbian Ceramic Society
C3  - Advanced Ceramics and Application : 9th Serbian Ceramic Society Conference : program and the book of abstracts; September 20-21, 2021; Belgrade
T1  - Enhanced dielectric properties of PVDF-based composites with BaTiO3 ceramic decorated with Fe2O3
SP  - 58
UR  - https://hdl.handle.net/21.15107/rcub_vinar_10796
ER  - 
@conference{
author = "Filipović, Suzana and Obradović, Nina and Rosenschon, M. and Füglein, E. and Dojčilović, Radovan and Đorđević, Antonije and Petrović, J. and Pavlović, Vladimir B.",
year = "2021",
abstract = "The increase in the utilization of ceramic/polymer composites as components for electric devices is mainly based on their high chemical stability, mechanical strength, and flexibility. The polymers usually have poor dielectric performances. In order to increase the dielectric permittivity, ceramic fillers with high dielectric constant have been used as active fillers, and usually in large amounts, which have a detrimental effect on the mechanical properties of the composite. With the aim to enhance the dielectric properties of the composite without loss of polymer’s flexibility, 5 wt.% of BaTiO3/Fe2O3 core/shell powders, prepared by different synthesis conditions, was added into the PVDF matrix. The effect of the phase composition and morphology of the starting BaTiO3/Fe2O3 core/shell filler on the crystal structure and lattice dynamics was investigated. Based on the results of the thermal analysis, TG/DSC, various parameters of ceramic/polymer composites were determined. We were able to corroborate that differences in the phase composition and morphology of BaTiO3/Fe2O3 core/shell filler have an influence on the formation of various PVDF allomorph modifications, as well as the level of crystallinity. The dielectric performances of the pure PVDF and polymer/ceramic composites were measured. An enhancement in the dielectric permittivity and decrease in the loss tangent were revealed.",
publisher = "Belgrade : Serbian Ceramic Society",
journal = "Advanced Ceramics and Application : 9th Serbian Ceramic Society Conference : program and the book of abstracts; September 20-21, 2021; Belgrade",
title = "Enhanced dielectric properties of PVDF-based composites with BaTiO3 ceramic decorated with Fe2O3",
pages = "58",
url = "https://hdl.handle.net/21.15107/rcub_vinar_10796"
}
Filipović, S., Obradović, N., Rosenschon, M., Füglein, E., Dojčilović, R., Đorđević, A., Petrović, J.,& Pavlović, V. B.. (2021). Enhanced dielectric properties of PVDF-based composites with BaTiO3 ceramic decorated with Fe2O3. in Advanced Ceramics and Application : 9th Serbian Ceramic Society Conference : program and the book of abstracts; September 20-21, 2021; Belgrade
Belgrade : Serbian Ceramic Society., 58.
https://hdl.handle.net/21.15107/rcub_vinar_10796
Filipović S, Obradović N, Rosenschon M, Füglein E, Dojčilović R, Đorđević A, Petrović J, Pavlović VB. Enhanced dielectric properties of PVDF-based composites with BaTiO3 ceramic decorated with Fe2O3. in Advanced Ceramics and Application : 9th Serbian Ceramic Society Conference : program and the book of abstracts; September 20-21, 2021; Belgrade. 2021;:58.
https://hdl.handle.net/21.15107/rcub_vinar_10796 .
Filipović, Suzana, Obradović, Nina, Rosenschon, M., Füglein, E., Dojčilović, Radovan, Đorđević, Antonije, Petrović, J., Pavlović, Vladimir B., "Enhanced dielectric properties of PVDF-based composites with BaTiO3 ceramic decorated with Fe2O3" in Advanced Ceramics and Application : 9th Serbian Ceramic Society Conference : program and the book of abstracts; September 20-21, 2021; Belgrade (2021):58,
https://hdl.handle.net/21.15107/rcub_vinar_10796 .

Study of Nanosized Hydroxyapatite Material Annealing at Different Retention Times

Miljković, Miljana; Kljajević, Ljiljana M.; Filipović, Suzana; Pavlović, Vladimir B.; Nenadović, Snežana S.

(2020)

TY  - JOUR
AU  - Miljković, Miljana
AU  - Kljajević, Ljiljana M.
AU  - Filipović, Suzana
AU  - Pavlović, Vladimir B.
AU  - Nenadović, Snežana S.
PY  - 2020
UR  - https://vinar.vin.bg.ac.rs/handle/123456789/8916
AB  - The aim of the study was to investigate the influence of low heating temperatures with two different retention times to optimize the process for obtaining nanosized hydroxyapatite material that can possibly be used in the fields of biology and pharmacy. Nanosized hydroxyapatite was successfully obtained by wet chemical precipitation. The annealing of the material performed at 300 oC with two different retention times i.e. 3 and 6 hours in air atmosphere. Low annealing temperature with extended retention time was selected in terms to reduce energy consumption. FTIR spectroscopy was used to confirm characteristic vibrational bands of hydroxyapatite samples, and presence of carbonate bands of hydroxyapatite annealed for 3h and 6h. X-Ray powder diffraction analysis were used to examine phase composition, determine the size of unit cells and crystallite sizes, and SEMEDS methods were used to obtain particle size and arrangement also grain growth morphology and confirmed the presence of calcium, phosphorous oxygen and carbonate peaks. The results show that different retention time has influence on particle growth as well as unit cell parameters and crystallite sizes changes of hydroxyapatite material.
T2  - Science of Sintering
T1  - Study of Nanosized Hydroxyapatite Material Annealing at Different Retention Times
VL  - 52
IS  - 4
SP  - 405
EP  - 413
DO  - 10.2298/SOS2004405M
ER  - 
@article{
author = "Miljković, Miljana and Kljajević, Ljiljana M. and Filipović, Suzana and Pavlović, Vladimir B. and Nenadović, Snežana S.",
year = "2020",
abstract = "The aim of the study was to investigate the influence of low heating temperatures with two different retention times to optimize the process for obtaining nanosized hydroxyapatite material that can possibly be used in the fields of biology and pharmacy. Nanosized hydroxyapatite was successfully obtained by wet chemical precipitation. The annealing of the material performed at 300 oC with two different retention times i.e. 3 and 6 hours in air atmosphere. Low annealing temperature with extended retention time was selected in terms to reduce energy consumption. FTIR spectroscopy was used to confirm characteristic vibrational bands of hydroxyapatite samples, and presence of carbonate bands of hydroxyapatite annealed for 3h and 6h. X-Ray powder diffraction analysis were used to examine phase composition, determine the size of unit cells and crystallite sizes, and SEMEDS methods were used to obtain particle size and arrangement also grain growth morphology and confirmed the presence of calcium, phosphorous oxygen and carbonate peaks. The results show that different retention time has influence on particle growth as well as unit cell parameters and crystallite sizes changes of hydroxyapatite material.",
journal = "Science of Sintering",
title = "Study of Nanosized Hydroxyapatite Material Annealing at Different Retention Times",
volume = "52",
number = "4",
pages = "405-413",
doi = "10.2298/SOS2004405M"
}
Miljković, M., Kljajević, L. M., Filipović, S., Pavlović, V. B.,& Nenadović, S. S.. (2020). Study of Nanosized Hydroxyapatite Material Annealing at Different Retention Times. in Science of Sintering, 52(4), 405-413.
https://doi.org/10.2298/SOS2004405M
Miljković M, Kljajević LM, Filipović S, Pavlović VB, Nenadović SS. Study of Nanosized Hydroxyapatite Material Annealing at Different Retention Times. in Science of Sintering. 2020;52(4):405-413.
doi:10.2298/SOS2004405M .
Miljković, Miljana, Kljajević, Ljiljana M., Filipović, Suzana, Pavlović, Vladimir B., Nenadović, Snežana S., "Study of Nanosized Hydroxyapatite Material Annealing at Different Retention Times" in Science of Sintering, 52, no. 4 (2020):405-413,
https://doi.org/10.2298/SOS2004405M . .
3
1
3

The effect of ball milling on properties of sintered manganese-doped alumina

Filipović, Suzana; Obradović, Nina; Marković, Smilja; Mitrić, Miodrag; Balać, Igor; Đorđević, Antonije; Pavlović, Vladimir B.

(2019)

TY  - JOUR
AU  - Filipović, Suzana
AU  - Obradović, Nina
AU  - Marković, Smilja
AU  - Mitrić, Miodrag
AU  - Balać, Igor
AU  - Đorđević, Antonije
AU  - Pavlović, Vladimir B.
PY  - 2019
UR  - https://vinar.vin.bg.ac.rs/handle/123456789/8441
AB  - Alumina-based compounds have many technological applications and attract great attention even after decades of investigation, due to their good chemical, electrical, and mechanical properties. A mixture of several alumina modifications (α-, κ-, γ-Al2O3) doped with 1 wt% of Mn2O3 was used for this experiment. The powder was mechanically activated for 60 min in an ethanol medium. After compaction, green bodies were sintered in the temperature range from 1200 to 1400 °C. Microstructures of the obtained specimens were investigated by scanning electron microscopy (SEM) and Energy-dispersive X-ray spectroscopy (EDS). The influence of morphological changes on electrical and mechanical properties was examined in detail. We have developed a test fixture and corresponding software for measurement of the relative dielectric permittivity and the loss tangent of ceramic specimens. This new method overcomes the problems of dimensions and shape of samples, as well as the problem of applying silver paste. The accuracy is around 2% for ε'r and 0.003 for tanδ. We demonstrate that the mechanical activation (MA) has the dominant influence on lowering the characteristic temperatures and microstructure development, which further leads to increased permittivity and tensile strength.
T2  - Advanced Powder Technology
T1  - The effect of ball milling on properties of sintered manganese-doped alumina
VL  - 30
IS  - 11
SP  - 2533
EP  - 2540
DO  - 10.1016/j.apt.2019.07.033
ER  - 
@article{
author = "Filipović, Suzana and Obradović, Nina and Marković, Smilja and Mitrić, Miodrag and Balać, Igor and Đorđević, Antonije and Pavlović, Vladimir B.",
year = "2019",
abstract = "Alumina-based compounds have many technological applications and attract great attention even after decades of investigation, due to their good chemical, electrical, and mechanical properties. A mixture of several alumina modifications (α-, κ-, γ-Al2O3) doped with 1 wt% of Mn2O3 was used for this experiment. The powder was mechanically activated for 60 min in an ethanol medium. After compaction, green bodies were sintered in the temperature range from 1200 to 1400 °C. Microstructures of the obtained specimens were investigated by scanning electron microscopy (SEM) and Energy-dispersive X-ray spectroscopy (EDS). The influence of morphological changes on electrical and mechanical properties was examined in detail. We have developed a test fixture and corresponding software for measurement of the relative dielectric permittivity and the loss tangent of ceramic specimens. This new method overcomes the problems of dimensions and shape of samples, as well as the problem of applying silver paste. The accuracy is around 2% for ε'r and 0.003 for tanδ. We demonstrate that the mechanical activation (MA) has the dominant influence on lowering the characteristic temperatures and microstructure development, which further leads to increased permittivity and tensile strength.",
journal = "Advanced Powder Technology",
title = "The effect of ball milling on properties of sintered manganese-doped alumina",
volume = "30",
number = "11",
pages = "2533-2540",
doi = "10.1016/j.apt.2019.07.033"
}
Filipović, S., Obradović, N., Marković, S., Mitrić, M., Balać, I., Đorđević, A.,& Pavlović, V. B.. (2019). The effect of ball milling on properties of sintered manganese-doped alumina. in Advanced Powder Technology, 30(11), 2533-2540.
https://doi.org/10.1016/j.apt.2019.07.033
Filipović S, Obradović N, Marković S, Mitrić M, Balać I, Đorđević A, Pavlović VB. The effect of ball milling on properties of sintered manganese-doped alumina. in Advanced Powder Technology. 2019;30(11):2533-2540.
doi:10.1016/j.apt.2019.07.033 .
Filipović, Suzana, Obradović, Nina, Marković, Smilja, Mitrić, Miodrag, Balać, Igor, Đorđević, Antonije, Pavlović, Vladimir B., "The effect of ball milling on properties of sintered manganese-doped alumina" in Advanced Powder Technology, 30, no. 11 (2019):2533-2540,
https://doi.org/10.1016/j.apt.2019.07.033 . .
4
3
5

The effect of ball milling on properties of sintered manganese-doped alumina

Filipović, Suzana; Obradović, Nina; Marković, Smilja; Mitrić, Miodrag; Balać, Igor; Đorđević, Antonije; Pavlović, Vladimir B.

(2019)

TY  - JOUR
AU  - Filipović, Suzana
AU  - Obradović, Nina
AU  - Marković, Smilja
AU  - Mitrić, Miodrag
AU  - Balać, Igor
AU  - Đorđević, Antonije
AU  - Pavlović, Vladimir B.
PY  - 2019
UR  - https://vinar.vin.bg.ac.rs/handle/123456789/8442
AB  - Alumina-based compounds have many technological applications and attract great attention even after decades of investigation, due to their good chemical, electrical, and mechanical properties. A mixture of several alumina modifications (α-, κ-, γ-Al2O3) doped with 1 wt% of Mn2O3 was used for this experiment. The powder was mechanically activated for 60 min in an ethanol medium. After compaction, green bodies were sintered in the temperature range from 1200 to 1400 °C. Microstructures of the obtained specimens were investigated by scanning electron microscopy (SEM) and Energy-dispersive X-ray spectroscopy (EDS). The influence of morphological changes on electrical and mechanical properties was examined in detail. We have developed a test fixture and corresponding software for measurement of the relative dielectric permittivity and the loss tangent of ceramic specimens. This new method overcomes the problems of dimensions and shape of samples, as well as the problem of applying silver paste. The accuracy is around 2% for ε'r and 0.003 for tanδ. We demonstrate that the mechanical activation (MA) has the dominant influence on lowering the characteristic temperatures and microstructure development, which further leads to increased permittivity and tensile strength.
T2  - Advanced Powder Technology
T1  - The effect of ball milling on properties of sintered manganese-doped alumina
VL  - 30
IS  - 11
SP  - 2533
EP  - 2540
DO  - 10.1016/j.apt.2019.07.033
ER  - 
@article{
author = "Filipović, Suzana and Obradović, Nina and Marković, Smilja and Mitrić, Miodrag and Balać, Igor and Đorđević, Antonije and Pavlović, Vladimir B.",
year = "2019",
abstract = "Alumina-based compounds have many technological applications and attract great attention even after decades of investigation, due to their good chemical, electrical, and mechanical properties. A mixture of several alumina modifications (α-, κ-, γ-Al2O3) doped with 1 wt% of Mn2O3 was used for this experiment. The powder was mechanically activated for 60 min in an ethanol medium. After compaction, green bodies were sintered in the temperature range from 1200 to 1400 °C. Microstructures of the obtained specimens were investigated by scanning electron microscopy (SEM) and Energy-dispersive X-ray spectroscopy (EDS). The influence of morphological changes on electrical and mechanical properties was examined in detail. We have developed a test fixture and corresponding software for measurement of the relative dielectric permittivity and the loss tangent of ceramic specimens. This new method overcomes the problems of dimensions and shape of samples, as well as the problem of applying silver paste. The accuracy is around 2% for ε'r and 0.003 for tanδ. We demonstrate that the mechanical activation (MA) has the dominant influence on lowering the characteristic temperatures and microstructure development, which further leads to increased permittivity and tensile strength.",
journal = "Advanced Powder Technology",
title = "The effect of ball milling on properties of sintered manganese-doped alumina",
volume = "30",
number = "11",
pages = "2533-2540",
doi = "10.1016/j.apt.2019.07.033"
}
Filipović, S., Obradović, N., Marković, S., Mitrić, M., Balać, I., Đorđević, A.,& Pavlović, V. B.. (2019). The effect of ball milling on properties of sintered manganese-doped alumina. in Advanced Powder Technology, 30(11), 2533-2540.
https://doi.org/10.1016/j.apt.2019.07.033
Filipović S, Obradović N, Marković S, Mitrić M, Balać I, Đorđević A, Pavlović VB. The effect of ball milling on properties of sintered manganese-doped alumina. in Advanced Powder Technology. 2019;30(11):2533-2540.
doi:10.1016/j.apt.2019.07.033 .
Filipović, Suzana, Obradović, Nina, Marković, Smilja, Mitrić, Miodrag, Balać, Igor, Đorđević, Antonije, Pavlović, Vladimir B., "The effect of ball milling on properties of sintered manganese-doped alumina" in Advanced Powder Technology, 30, no. 11 (2019):2533-2540,
https://doi.org/10.1016/j.apt.2019.07.033 . .
4
3
6

Synthesis and characterization of BaTiO3/α-Fe2O3 core/shell structure

Filipović, Suzana; Pavlović, Vera P.; Mitrić, Miodrag; Lević, Steva; Mitrović, Nebojša; Maričić, Aleksa; Vlahović, Branislav; Pavlović, Vladimir B.

(2019)

TY  - JOUR
AU  - Filipović, Suzana
AU  - Pavlović, Vera P.
AU  - Mitrić, Miodrag
AU  - Lević, Steva
AU  - Mitrović, Nebojša
AU  - Maričić, Aleksa
AU  - Vlahović, Branislav
AU  - Pavlović, Vladimir B.
PY  - 2019
UR  - https://doi.org/10.1007/s40145-018-0301-5
UR  - https://vinar.vin.bg.ac.rs/handle/123456789/8103
AB  - Multiferroic materials attracted a lot of attention in recent years because of their significant scientific interest and technological applications. The multiferroic core/shell powders have a better connectivity between the phases, resulting in superior dielectric and magneto electric properties. In this study, the influence of preparation condition on structure and properties of BaTiO3/α-Fe2O3 core/shell composite materials was examined. The five samples were obtained by varying synthesis conditions, such as synthesized method (co-precipitation and sonochemical method) and pH values of solution. XRD and Raman spectroscopy analyses were performed in order to determine phase composition and structural changes within samples. Morphology modifications were examined by SEM and EDS analyses. Finally, effect of structural and microstructural changes on magnetic and electrical properties was detected and explained.
T2  - Journal of Advanced Ceramics
T1  - Synthesis and characterization of BaTiO3/α-Fe2O3 core/shell structure
VL  - 8
IS  - 1
SP  - 133
EP  - 147
DO  - 10.1007/s40145-018-0301-5
ER  - 
@article{
author = "Filipović, Suzana and Pavlović, Vera P. and Mitrić, Miodrag and Lević, Steva and Mitrović, Nebojša and Maričić, Aleksa and Vlahović, Branislav and Pavlović, Vladimir B.",
year = "2019",
abstract = "Multiferroic materials attracted a lot of attention in recent years because of their significant scientific interest and technological applications. The multiferroic core/shell powders have a better connectivity between the phases, resulting in superior dielectric and magneto electric properties. In this study, the influence of preparation condition on structure and properties of BaTiO3/α-Fe2O3 core/shell composite materials was examined. The five samples were obtained by varying synthesis conditions, such as synthesized method (co-precipitation and sonochemical method) and pH values of solution. XRD and Raman spectroscopy analyses were performed in order to determine phase composition and structural changes within samples. Morphology modifications were examined by SEM and EDS analyses. Finally, effect of structural and microstructural changes on magnetic and electrical properties was detected and explained.",
journal = "Journal of Advanced Ceramics",
title = "Synthesis and characterization of BaTiO3/α-Fe2O3 core/shell structure",
volume = "8",
number = "1",
pages = "133-147",
doi = "10.1007/s40145-018-0301-5"
}
Filipović, S., Pavlović, V. P., Mitrić, M., Lević, S., Mitrović, N., Maričić, A., Vlahović, B.,& Pavlović, V. B.. (2019). Synthesis and characterization of BaTiO3/α-Fe2O3 core/shell structure. in Journal of Advanced Ceramics, 8(1), 133-147.
https://doi.org/10.1007/s40145-018-0301-5
Filipović S, Pavlović VP, Mitrić M, Lević S, Mitrović N, Maričić A, Vlahović B, Pavlović VB. Synthesis and characterization of BaTiO3/α-Fe2O3 core/shell structure. in Journal of Advanced Ceramics. 2019;8(1):133-147.
doi:10.1007/s40145-018-0301-5 .
Filipović, Suzana, Pavlović, Vera P., Mitrić, Miodrag, Lević, Steva, Mitrović, Nebojša, Maričić, Aleksa, Vlahović, Branislav, Pavlović, Vladimir B., "Synthesis and characterization of BaTiO3/α-Fe2O3 core/shell structure" in Journal of Advanced Ceramics, 8, no. 1 (2019):133-147,
https://doi.org/10.1007/s40145-018-0301-5 . .
1
9
9
11

Influence of different pore-forming agents on wollastonite microstructures and adsorption capacities

Obradović, Nina; Filipović, Suzana; Marković, Smilja; Mitrić, Miodrag; Rusmirović, Jelena D.; Marinković, Aleksandar D.; Antić, Vesna; Pavlović, Vladimir B.

(2017)

TY  - JOUR
AU  - Obradović, Nina
AU  - Filipović, Suzana
AU  - Marković, Smilja
AU  - Mitrić, Miodrag
AU  - Rusmirović, Jelena D.
AU  - Marinković, Aleksandar D.
AU  - Antić, Vesna
AU  - Pavlović, Vladimir B.
PY  - 2017
UR  - https://vinar.vin.bg.ac.rs/handle/123456789/1558
AB  - In this study, porous macro- and micro-cellular wollastonite-based ceramics was synthesized. A ceramic precursor, methylhydrocyclosiloxane, together with micro-sized CaCO3, was used as a starting material. After 20 min of ultrasound treatment, and calcination at 250 degrees C for 30 min, different pore-forming agents were added to the as-obtained powders. Differential thermal analysis was used to determine characteristic temperatures of processes occurring within powders during heating. Based on the obtained results, the sintering regime was set up. The prepared mixtures were pressed into pallets and sintered at 900 degrees C. During the sintering regime, porous wollastonite-based ceramics was obtained. The phase composition of the sintered samples, as well as the microstructures, were analyzed by using X-ray diffraction and SEM. A two-phase system was detected in all samples, CaSiO3 wollastonite and Ca2SiO4 larnite, and their ratio varied with each pore-forming agent. It was observed that the addition of different pore-forming agents resulted in significantly different microstructures. In a batch test, the influence of pH, the contact time and the initial ion concentration on the adsorption efficiency of As+5, Cr(+6)and phosphate ions on the synthesized adsorbents were studied. Time-dependent adsorption is best described by the pseudo-second-order kinetic model and the Weber-Morris model, which predict intra-particle diffusion as a rate-controlling step of the overall process. High adsorption capacities, 21.93, 23.88, and 27.29 mg g(-1), were obtained for the CaCO3-siloxane-nanocellulose sorbent, and similar/lower capacities were obtained for the CaCO3-siloxane-PMMA and CaCO3-siloxane-cotton wool adsorbents.
T2  - Ceramics International
T1  - Influence of different pore-forming agents on wollastonite microstructures and adsorption capacities
VL  - 43
IS  - 10
SP  - 7461
EP  - 7468
DO  - 10.1016/j.ceramint.2017.03.021
ER  - 
@article{
author = "Obradović, Nina and Filipović, Suzana and Marković, Smilja and Mitrić, Miodrag and Rusmirović, Jelena D. and Marinković, Aleksandar D. and Antić, Vesna and Pavlović, Vladimir B.",
year = "2017",
abstract = "In this study, porous macro- and micro-cellular wollastonite-based ceramics was synthesized. A ceramic precursor, methylhydrocyclosiloxane, together with micro-sized CaCO3, was used as a starting material. After 20 min of ultrasound treatment, and calcination at 250 degrees C for 30 min, different pore-forming agents were added to the as-obtained powders. Differential thermal analysis was used to determine characteristic temperatures of processes occurring within powders during heating. Based on the obtained results, the sintering regime was set up. The prepared mixtures were pressed into pallets and sintered at 900 degrees C. During the sintering regime, porous wollastonite-based ceramics was obtained. The phase composition of the sintered samples, as well as the microstructures, were analyzed by using X-ray diffraction and SEM. A two-phase system was detected in all samples, CaSiO3 wollastonite and Ca2SiO4 larnite, and their ratio varied with each pore-forming agent. It was observed that the addition of different pore-forming agents resulted in significantly different microstructures. In a batch test, the influence of pH, the contact time and the initial ion concentration on the adsorption efficiency of As+5, Cr(+6)and phosphate ions on the synthesized adsorbents were studied. Time-dependent adsorption is best described by the pseudo-second-order kinetic model and the Weber-Morris model, which predict intra-particle diffusion as a rate-controlling step of the overall process. High adsorption capacities, 21.93, 23.88, and 27.29 mg g(-1), were obtained for the CaCO3-siloxane-nanocellulose sorbent, and similar/lower capacities were obtained for the CaCO3-siloxane-PMMA and CaCO3-siloxane-cotton wool adsorbents.",
journal = "Ceramics International",
title = "Influence of different pore-forming agents on wollastonite microstructures and adsorption capacities",
volume = "43",
number = "10",
pages = "7461-7468",
doi = "10.1016/j.ceramint.2017.03.021"
}
Obradović, N., Filipović, S., Marković, S., Mitrić, M., Rusmirović, J. D., Marinković, A. D., Antić, V.,& Pavlović, V. B.. (2017). Influence of different pore-forming agents on wollastonite microstructures and adsorption capacities. in Ceramics International, 43(10), 7461-7468.
https://doi.org/10.1016/j.ceramint.2017.03.021
Obradović N, Filipović S, Marković S, Mitrić M, Rusmirović JD, Marinković AD, Antić V, Pavlović VB. Influence of different pore-forming agents on wollastonite microstructures and adsorption capacities. in Ceramics International. 2017;43(10):7461-7468.
doi:10.1016/j.ceramint.2017.03.021 .
Obradović, Nina, Filipović, Suzana, Marković, Smilja, Mitrić, Miodrag, Rusmirović, Jelena D., Marinković, Aleksandar D., Antić, Vesna, Pavlović, Vladimir B., "Influence of different pore-forming agents on wollastonite microstructures and adsorption capacities" in Ceramics International, 43, no. 10 (2017):7461-7468,
https://doi.org/10.1016/j.ceramint.2017.03.021 . .
20
14
24

Influence of different pore-forming agents on wollastonite microstructures

Obradović, Nina; Filipović, Suzana; Marković, Smilja; Mitrić, Miodrag; Antić, Vesna; Pavlović, Vladimir B.

(Belgrade : Serbian Ceramic Society, 2016)

TY  - CONF
AU  - Obradović, Nina
AU  - Filipović, Suzana
AU  - Marković, Smilja
AU  - Mitrić, Miodrag
AU  - Antić, Vesna
AU  - Pavlović, Vladimir B.
PY  - 2016
UR  - https://vinar.vin.bg.ac.rs/handle/123456789/7548
AB  - In this study, highly porous macro- and micro-cellular wollastonite-based ceramics was synthesized. Ceramic precursor, methylhydrocyclosiloxane, together with micro-sized CaCO3, was used as starting material. After 20 min of ultrasound treatment, and calcination at 250 oC for 30 min, different pore-forming agents were added to the as-obtained powders. Differential thermal analysis was used to determine characteristic temperatures of processes occurring within powders during heating. Based on the obtained results, sintering regime was set up. Prepared mixtures were pressed into pallets and sintered at 900 oC. During the sintering regime, highly porous wollastonite-based ceramics was obtained. The phase composition of the sintered samples as well as microstructures was analyzed by the means of X-ray diffraction method and SEM. Two-phase system was detected in all samples, CaSiO3 wollastonite and Ca2SiO4 larnite, and their ratio varied with each pore-forming agent. It was observed that addition of different pore-forming agent resulted in significantly different microstructures.
PB  - Belgrade : Serbian Ceramic Society
C3  - Advanced Ceramics and Application : 5th Serbian Ceramic Society Conference : program and the book of abstracts; September 21-23, 2016; Belgrade
T1  - Influence of different pore-forming agents on wollastonite microstructures
SP  - 42
UR  - https://hdl.handle.net/21.15107/rcub_vinar_7548
ER  - 
@conference{
author = "Obradović, Nina and Filipović, Suzana and Marković, Smilja and Mitrić, Miodrag and Antić, Vesna and Pavlović, Vladimir B.",
year = "2016",
abstract = "In this study, highly porous macro- and micro-cellular wollastonite-based ceramics was synthesized. Ceramic precursor, methylhydrocyclosiloxane, together with micro-sized CaCO3, was used as starting material. After 20 min of ultrasound treatment, and calcination at 250 oC for 30 min, different pore-forming agents were added to the as-obtained powders. Differential thermal analysis was used to determine characteristic temperatures of processes occurring within powders during heating. Based on the obtained results, sintering regime was set up. Prepared mixtures were pressed into pallets and sintered at 900 oC. During the sintering regime, highly porous wollastonite-based ceramics was obtained. The phase composition of the sintered samples as well as microstructures was analyzed by the means of X-ray diffraction method and SEM. Two-phase system was detected in all samples, CaSiO3 wollastonite and Ca2SiO4 larnite, and their ratio varied with each pore-forming agent. It was observed that addition of different pore-forming agent resulted in significantly different microstructures.",
publisher = "Belgrade : Serbian Ceramic Society",
journal = "Advanced Ceramics and Application : 5th Serbian Ceramic Society Conference : program and the book of abstracts; September 21-23, 2016; Belgrade",
title = "Influence of different pore-forming agents on wollastonite microstructures",
pages = "42",
url = "https://hdl.handle.net/21.15107/rcub_vinar_7548"
}
Obradović, N., Filipović, S., Marković, S., Mitrić, M., Antić, V.,& Pavlović, V. B.. (2016). Influence of different pore-forming agents on wollastonite microstructures. in Advanced Ceramics and Application : 5th Serbian Ceramic Society Conference : program and the book of abstracts; September 21-23, 2016; Belgrade
Belgrade : Serbian Ceramic Society., 42.
https://hdl.handle.net/21.15107/rcub_vinar_7548
Obradović N, Filipović S, Marković S, Mitrić M, Antić V, Pavlović VB. Influence of different pore-forming agents on wollastonite microstructures. in Advanced Ceramics and Application : 5th Serbian Ceramic Society Conference : program and the book of abstracts; September 21-23, 2016; Belgrade. 2016;:42.
https://hdl.handle.net/21.15107/rcub_vinar_7548 .
Obradović, Nina, Filipović, Suzana, Marković, Smilja, Mitrić, Miodrag, Antić, Vesna, Pavlović, Vladimir B., "Influence of different pore-forming agents on wollastonite microstructures" in Advanced Ceramics and Application : 5th Serbian Ceramic Society Conference : program and the book of abstracts; September 21-23, 2016; Belgrade (2016):42,
https://hdl.handle.net/21.15107/rcub_vinar_7548 .

Influence of mechanical activation on the MgO-Al2O3-SiO2 system with TeO2

Đorđević, Nataša; Obradović, Nina; Filipović, Suzana; Kosanović, Darko; Marković, Smilja; Mitrić, Miodrag; Pavlović, Vladimir B.

(Belgrade : Materials Research Society of Serbia, 2016)

TY  - CONF
AU  - Đorđević, Nataša
AU  - Obradović, Nina
AU  - Filipović, Suzana
AU  - Kosanović, Darko
AU  - Marković, Smilja
AU  - Mitrić, Miodrag
AU  - Pavlović, Vladimir B.
PY  - 2016
UR  - https://vinar.vin.bg.ac.rs/handle/123456789/7552
AB  - Cordierite 2MgO+2Al2O3+5SiO2 is frequently used ceramic material, that is commonly used as a carrier of electrical components due to its low dielectric constant (~ 5), and low temperature thermal expansion coefficient (20•10-7 ºC-1). In order to accelerate the process of sintering, 5.00 mass% TeO2 was added to the starting mixtures. System was tested in two parallel mixtures, one with no added additives, and the other one with TeO2. The mechanical activation of the both mixtures was performed in a high-energy ball mill in time intervals from 0 to 40 min with ball to powder mass ratio 1:40. The particle size analysis (PSA) was employed in order to determine the changes in the particle size of the mechanically treated powders. The phase composition of the starting powders as well as microstructures was analyzed by the means of X-ray diffraction method and SEM.
PB  - Belgrade : Materials Research Society of Serbia
C3  - YUCOMAT 2016 : 18th Annual Conference YUCOMAT 2016 : programme and the book of abstracts; September 5-10, Herceg Novi
T1  - Influence of mechanical activation on the MgO-Al2O3-SiO2 system with TeO2
SP  - 75
EP  - 75
UR  - https://hdl.handle.net/21.15107/rcub_vinar_7552
ER  - 
@conference{
author = "Đorđević, Nataša and Obradović, Nina and Filipović, Suzana and Kosanović, Darko and Marković, Smilja and Mitrić, Miodrag and Pavlović, Vladimir B.",
year = "2016",
abstract = "Cordierite 2MgO+2Al2O3+5SiO2 is frequently used ceramic material, that is commonly used as a carrier of electrical components due to its low dielectric constant (~ 5), and low temperature thermal expansion coefficient (20•10-7 ºC-1). In order to accelerate the process of sintering, 5.00 mass% TeO2 was added to the starting mixtures. System was tested in two parallel mixtures, one with no added additives, and the other one with TeO2. The mechanical activation of the both mixtures was performed in a high-energy ball mill in time intervals from 0 to 40 min with ball to powder mass ratio 1:40. The particle size analysis (PSA) was employed in order to determine the changes in the particle size of the mechanically treated powders. The phase composition of the starting powders as well as microstructures was analyzed by the means of X-ray diffraction method and SEM.",
publisher = "Belgrade : Materials Research Society of Serbia",
journal = "YUCOMAT 2016 : 18th Annual Conference YUCOMAT 2016 : programme and the book of abstracts; September 5-10, Herceg Novi",
title = "Influence of mechanical activation on the MgO-Al2O3-SiO2 system with TeO2",
pages = "75-75",
url = "https://hdl.handle.net/21.15107/rcub_vinar_7552"
}
Đorđević, N., Obradović, N., Filipović, S., Kosanović, D., Marković, S., Mitrić, M.,& Pavlović, V. B.. (2016). Influence of mechanical activation on the MgO-Al2O3-SiO2 system with TeO2. in YUCOMAT 2016 : 18th Annual Conference YUCOMAT 2016 : programme and the book of abstracts; September 5-10, Herceg Novi
Belgrade : Materials Research Society of Serbia., 75-75.
https://hdl.handle.net/21.15107/rcub_vinar_7552
Đorđević N, Obradović N, Filipović S, Kosanović D, Marković S, Mitrić M, Pavlović VB. Influence of mechanical activation on the MgO-Al2O3-SiO2 system with TeO2. in YUCOMAT 2016 : 18th Annual Conference YUCOMAT 2016 : programme and the book of abstracts; September 5-10, Herceg Novi. 2016;:75-75.
https://hdl.handle.net/21.15107/rcub_vinar_7552 .
Đorđević, Nataša, Obradović, Nina, Filipović, Suzana, Kosanović, Darko, Marković, Smilja, Mitrić, Miodrag, Pavlović, Vladimir B., "Influence of mechanical activation on the MgO-Al2O3-SiO2 system with TeO2" in YUCOMAT 2016 : 18th Annual Conference YUCOMAT 2016 : programme and the book of abstracts; September 5-10, Herceg Novi (2016):75-75,
https://hdl.handle.net/21.15107/rcub_vinar_7552 .

Reaction kinetics of mechanically activated cordierite-based ceramics studied via DTA

Obradović, Nina; Đorđević, Nataša; Filipović, Suzana; Marković, Smilja; Kosanović, Darko; Mitrić, Miodrag; Pavlović, Vladimir B.

(Springer, 2016)

TY  - JOUR
AU  - Obradović, Nina
AU  - Đorđević, Nataša
AU  - Filipović, Suzana
AU  - Marković, Smilja
AU  - Kosanović, Darko
AU  - Mitrić, Miodrag
AU  - Pavlović, Vladimir B.
PY  - 2016
UR  - https://vinar.vin.bg.ac.rs/handle/123456789/999
AB  - Since cordierite, 2MgO center dot 2Al(2)O(3)center dot 5SiO(2) (MAS), is a very useful high-temperature ceramic material, it is important to decrease its sintering temperature. In order to accelerate the process of sintering, 5.00 mass% MoO3 was added to the starting mixtures. The mechanical activation of the starting mixtures was performed in a high-energy ball mill in time intervals from 0 to 160 min. After the activation, starting mixtures were sintered at 1300 A degrees C for 2 h. In order to determine the impact of mechanical activation on particle size distribution and powders morphology, the mechanically treated powders were characterized by a laser light-scattering particle size analyzer and scanning electron microscopy. The phase composition of the starting mixtures and sintered samples was analyzed by the X-ray diffraction method. In order to determine temperature intervals of chemical reactions and phase transitions, differential thermal analyses (DTA) and thermo-gravimetric analysis were used. Kissingers equation was employed to calculate apparent activation energies of various processes that occur within the system during heating. Based on the obtained DTA results, it was established that mechanical activation along with MoO3 additive has influence on sintering temperature which was decreased for more than 100 A degrees C, comparing to the literature data.
PB  - Springer
T2  - Journal of Thermal Analysis and Calorimetry
T1  - Reaction kinetics of mechanically activated cordierite-based ceramics studied via DTA
VL  - 124
IS  - 2
SP  - 667
EP  - 673
DO  - 10.1007/s10973-015-5132-9
ER  - 
@article{
author = "Obradović, Nina and Đorđević, Nataša and Filipović, Suzana and Marković, Smilja and Kosanović, Darko and Mitrić, Miodrag and Pavlović, Vladimir B.",
year = "2016",
abstract = "Since cordierite, 2MgO center dot 2Al(2)O(3)center dot 5SiO(2) (MAS), is a very useful high-temperature ceramic material, it is important to decrease its sintering temperature. In order to accelerate the process of sintering, 5.00 mass% MoO3 was added to the starting mixtures. The mechanical activation of the starting mixtures was performed in a high-energy ball mill in time intervals from 0 to 160 min. After the activation, starting mixtures were sintered at 1300 A degrees C for 2 h. In order to determine the impact of mechanical activation on particle size distribution and powders morphology, the mechanically treated powders were characterized by a laser light-scattering particle size analyzer and scanning electron microscopy. The phase composition of the starting mixtures and sintered samples was analyzed by the X-ray diffraction method. In order to determine temperature intervals of chemical reactions and phase transitions, differential thermal analyses (DTA) and thermo-gravimetric analysis were used. Kissingers equation was employed to calculate apparent activation energies of various processes that occur within the system during heating. Based on the obtained DTA results, it was established that mechanical activation along with MoO3 additive has influence on sintering temperature which was decreased for more than 100 A degrees C, comparing to the literature data.",
publisher = "Springer",
journal = "Journal of Thermal Analysis and Calorimetry",
title = "Reaction kinetics of mechanically activated cordierite-based ceramics studied via DTA",
volume = "124",
number = "2",
pages = "667-673",
doi = "10.1007/s10973-015-5132-9"
}
Obradović, N., Đorđević, N., Filipović, S., Marković, S., Kosanović, D., Mitrić, M.,& Pavlović, V. B.. (2016). Reaction kinetics of mechanically activated cordierite-based ceramics studied via DTA. in Journal of Thermal Analysis and Calorimetry
Springer., 124(2), 667-673.
https://doi.org/10.1007/s10973-015-5132-9
Obradović N, Đorđević N, Filipović S, Marković S, Kosanović D, Mitrić M, Pavlović VB. Reaction kinetics of mechanically activated cordierite-based ceramics studied via DTA. in Journal of Thermal Analysis and Calorimetry. 2016;124(2):667-673.
doi:10.1007/s10973-015-5132-9 .
Obradović, Nina, Đorđević, Nataša, Filipović, Suzana, Marković, Smilja, Kosanović, Darko, Mitrić, Miodrag, Pavlović, Vladimir B., "Reaction kinetics of mechanically activated cordierite-based ceramics studied via DTA" in Journal of Thermal Analysis and Calorimetry, 124, no. 2 (2016):667-673,
https://doi.org/10.1007/s10973-015-5132-9 . .
7
8
9

Effect of consolidation parameters on structural, microstructural and electrical properties of magnesium titanate ceramics

Filipović, Suzana; Obradović, Nina; Pavlović, Vladimir B.; Mitrić, Miodrag; Đorđević, Antonije R.; Kachlik, M.; Maca, Karel

(Elsevier, 2016)

TY  - JOUR
AU  - Filipović, Suzana
AU  - Obradović, Nina
AU  - Pavlović, Vladimir B.
AU  - Mitrić, Miodrag
AU  - Đorđević, Antonije R.
AU  - Kachlik, M.
AU  - Maca, Karel
PY  - 2016
UR  - https://vinar.vin.bg.ac.rs/handle/123456789/1037
AB  - The aim of this study is to explore the influence of the processing route on the structural and physical properties of bulk MgTiO3 ceramics. Commercially available MgO and TiO2 powders were mechanically activated in a planetary ball mill. Green bodies were formed by an isostatic pressure of 300 MPa. The sintering of these samples was done either by the Two-Step Sintering (TSS) approach or by conventional pressureless sintering followed by Hot Isostatic Pressing (post-HIPing). The first set of compacts was sintered by TSS in air at 1300 degrees C for 30 min and the next step was performed at 1200 degrees C for 20 h. The density of the obtained samples after the two-step sintering reached almost 90% of the theoretical density (%TD). The second set of compacts was sintered at 1400 degrees C for 30 min in air. The samples without open porosity were post-sintered by the HIP at 1200 degrees C for 2 h in an argon atmosphere at a pressure of 200 MPa. The density significantly increased up to 96%TD. The differences between samples prepared by these two techniques were also analyzed by XRD and SEM. The lattice vibration spectra were obtained using Raman spectroscopy and they indicate a high degree of lattice disorder, as well as high values of the oxygen vacancy concentration. Electrical characteristic were established in the frequency range from 10 kHz to 10 GHz. The choice of the processing route had considerable influence on structural and physical properties of MgTiO3 ceramics. (C) 2016 Elsevier Ltd and Techna Group S.r.l. All rights reserved.
PB  - Elsevier
T2  - Ceramics International
T1  - Effect of consolidation parameters on structural, microstructural and electrical properties of magnesium titanate ceramics
VL  - 42
IS  - 8
SP  - 9887
EP  - 9898
DO  - 10.1016/j.ceramint.2016.03.088
ER  - 
@article{
author = "Filipović, Suzana and Obradović, Nina and Pavlović, Vladimir B. and Mitrić, Miodrag and Đorđević, Antonije R. and Kachlik, M. and Maca, Karel",
year = "2016",
abstract = "The aim of this study is to explore the influence of the processing route on the structural and physical properties of bulk MgTiO3 ceramics. Commercially available MgO and TiO2 powders were mechanically activated in a planetary ball mill. Green bodies were formed by an isostatic pressure of 300 MPa. The sintering of these samples was done either by the Two-Step Sintering (TSS) approach or by conventional pressureless sintering followed by Hot Isostatic Pressing (post-HIPing). The first set of compacts was sintered by TSS in air at 1300 degrees C for 30 min and the next step was performed at 1200 degrees C for 20 h. The density of the obtained samples after the two-step sintering reached almost 90% of the theoretical density (%TD). The second set of compacts was sintered at 1400 degrees C for 30 min in air. The samples without open porosity were post-sintered by the HIP at 1200 degrees C for 2 h in an argon atmosphere at a pressure of 200 MPa. The density significantly increased up to 96%TD. The differences between samples prepared by these two techniques were also analyzed by XRD and SEM. The lattice vibration spectra were obtained using Raman spectroscopy and they indicate a high degree of lattice disorder, as well as high values of the oxygen vacancy concentration. Electrical characteristic were established in the frequency range from 10 kHz to 10 GHz. The choice of the processing route had considerable influence on structural and physical properties of MgTiO3 ceramics. (C) 2016 Elsevier Ltd and Techna Group S.r.l. All rights reserved.",
publisher = "Elsevier",
journal = "Ceramics International",
title = "Effect of consolidation parameters on structural, microstructural and electrical properties of magnesium titanate ceramics",
volume = "42",
number = "8",
pages = "9887-9898",
doi = "10.1016/j.ceramint.2016.03.088"
}
Filipović, S., Obradović, N., Pavlović, V. B., Mitrić, M., Đorđević, A. R., Kachlik, M.,& Maca, K.. (2016). Effect of consolidation parameters on structural, microstructural and electrical properties of magnesium titanate ceramics. in Ceramics International
Elsevier., 42(8), 9887-9898.
https://doi.org/10.1016/j.ceramint.2016.03.088
Filipović S, Obradović N, Pavlović VB, Mitrić M, Đorđević AR, Kachlik M, Maca K. Effect of consolidation parameters on structural, microstructural and electrical properties of magnesium titanate ceramics. in Ceramics International. 2016;42(8):9887-9898.
doi:10.1016/j.ceramint.2016.03.088 .
Filipović, Suzana, Obradović, Nina, Pavlović, Vladimir B., Mitrić, Miodrag, Đorđević, Antonije R., Kachlik, M., Maca, Karel, "Effect of consolidation parameters on structural, microstructural and electrical properties of magnesium titanate ceramics" in Ceramics International, 42, no. 8 (2016):9887-9898,
https://doi.org/10.1016/j.ceramint.2016.03.088 . .
15
11
14

Reaction kinetics of mechanically activated cordierite based ceramics studied via DTA

Obradović, Nina; Đorđević, Nataša; Kosanović, Darko; Filipović, Suzana; Marković, Smilja; Mitrić, Miodrag; Pavlović, Vladimir B.

(Ljubljana : Central and Eastern European Committee for Thermal Analysis and Calorimetry, 2015)

TY  - CONF
AU  - Obradović, Nina
AU  - Đorđević, Nataša
AU  - Kosanović, Darko
AU  - Filipović, Suzana
AU  - Marković, Smilja
AU  - Mitrić, Miodrag
AU  - Pavlović, Vladimir B.
PY  - 2015
UR  - http://dais.sanu.ac.rs/123456789/761
UR  - https://vinar.vin.bg.ac.rs/handle/123456789/7525
AB  - Cordierite, 2MgO•2Ah03•5Si02 (MAS), is a very attractive high-temperature ceramic material. In order to accelerate the process of sintering, 5.00 mass% Mo03 was added to the starting mixtures. The mechanical activation of the starting mixtures was performed in a high energy ball mill in time intervals from 0 to 160 minutes. In following, starting mixtures were sintered at 1300 °C for 2h. In order to determine the changes in the particle size distribution, the mechanically treated powders were characterized by a laser light-scattering particle size analyzer. The phase composition of the starting mixtures and sintered samples was analyzed by the X-ray diffraction method. Differential thermal analyses (DTA) and thermo-gravimetric (TG) analysis were used in order to determine characteristic temperatures. Kissinger's equation was employed to calculate apparent activation energies of various processes that occur within the system while heating. Based on the obtained DTA results, it was established that mechanical activation along with MoO3 additive, has influence on sintering temperature which was decreased for about 150 °C.
PB  - Ljubljana : Central and Eastern European Committee for Thermal Analysis and Calorimetry
C3  - 3rd Central and Eastern European Conference on Thermal Analysis and Calorimetry 25-28 August 2015, Ljubljana, Slovenia: Book of Abstracts
T1  - Reaction kinetics of mechanically activated cordierite based ceramics studied via DTA
SP  - 195
EP  - 195
UR  - https://hdl.handle.net/21.15107/rcub_vinar_7525
ER  - 
@conference{
author = "Obradović, Nina and Đorđević, Nataša and Kosanović, Darko and Filipović, Suzana and Marković, Smilja and Mitrić, Miodrag and Pavlović, Vladimir B.",
year = "2015",
abstract = "Cordierite, 2MgO•2Ah03•5Si02 (MAS), is a very attractive high-temperature ceramic material. In order to accelerate the process of sintering, 5.00 mass% Mo03 was added to the starting mixtures. The mechanical activation of the starting mixtures was performed in a high energy ball mill in time intervals from 0 to 160 minutes. In following, starting mixtures were sintered at 1300 °C for 2h. In order to determine the changes in the particle size distribution, the mechanically treated powders were characterized by a laser light-scattering particle size analyzer. The phase composition of the starting mixtures and sintered samples was analyzed by the X-ray diffraction method. Differential thermal analyses (DTA) and thermo-gravimetric (TG) analysis were used in order to determine characteristic temperatures. Kissinger's equation was employed to calculate apparent activation energies of various processes that occur within the system while heating. Based on the obtained DTA results, it was established that mechanical activation along with MoO3 additive, has influence on sintering temperature which was decreased for about 150 °C.",
publisher = "Ljubljana : Central and Eastern European Committee for Thermal Analysis and Calorimetry",
journal = "3rd Central and Eastern European Conference on Thermal Analysis and Calorimetry 25-28 August 2015, Ljubljana, Slovenia: Book of Abstracts",
title = "Reaction kinetics of mechanically activated cordierite based ceramics studied via DTA",
pages = "195-195",
url = "https://hdl.handle.net/21.15107/rcub_vinar_7525"
}
Obradović, N., Đorđević, N., Kosanović, D., Filipović, S., Marković, S., Mitrić, M.,& Pavlović, V. B.. (2015). Reaction kinetics of mechanically activated cordierite based ceramics studied via DTA. in 3rd Central and Eastern European Conference on Thermal Analysis and Calorimetry 25-28 August 2015, Ljubljana, Slovenia: Book of Abstracts
Ljubljana : Central and Eastern European Committee for Thermal Analysis and Calorimetry., 195-195.
https://hdl.handle.net/21.15107/rcub_vinar_7525
Obradović N, Đorđević N, Kosanović D, Filipović S, Marković S, Mitrić M, Pavlović VB. Reaction kinetics of mechanically activated cordierite based ceramics studied via DTA. in 3rd Central and Eastern European Conference on Thermal Analysis and Calorimetry 25-28 August 2015, Ljubljana, Slovenia: Book of Abstracts. 2015;:195-195.
https://hdl.handle.net/21.15107/rcub_vinar_7525 .
Obradović, Nina, Đorđević, Nataša, Kosanović, Darko, Filipović, Suzana, Marković, Smilja, Mitrić, Miodrag, Pavlović, Vladimir B., "Reaction kinetics of mechanically activated cordierite based ceramics studied via DTA" in 3rd Central and Eastern European Conference on Thermal Analysis and Calorimetry 25-28 August 2015, Ljubljana, Slovenia: Book of Abstracts (2015):195-195,
https://hdl.handle.net/21.15107/rcub_vinar_7525 .

The effect of Hot Isostatic Pressing on the MT sample densities

Filipović, Suzana; Obradović, Nina; Pavlović, Vladimir B.; Kosanović, Darko; Mitrić, Miodrag; Paunović, Vesna; Pouchly, V.; Kachlik, Martin; Maca, Karel

(Belgrade : Serbian Ceramic Society, 2015)

TY  - CONF
AU  - Filipović, Suzana
AU  - Obradović, Nina
AU  - Pavlović, Vladimir B.
AU  - Kosanović, Darko
AU  - Mitrić, Miodrag
AU  - Paunović, Vesna
AU  - Pouchly, V.
AU  - Kachlik, Martin
AU  - Maca, Karel
PY  - 2015
UR  - https://vinar.vin.bg.ac.rs/handle/123456789/7526
AB  - Mechanically activated powders (0, 10, 40, 80 and 160 minutes) were formed by isostatic pressure 300 MPa to cylindrical green bodies (φ 12 mm). First set of samples was sintered at 1300°C for 30 min in air (heating rate 10 °C/min, cooling rate 5 oC/min). These samples were re-sintered at 1200 oC for 20 h in air (heating rate 20 °C/min, cooling rate 10 oC/min). Samples reached almost 90 % TD. The second set of samples was sintered at 1400 °C for 30 in air (heating rate 10 oC/min, cooling rate 5 °C/min). Relative densities increased up to 93 % TD. The samples of absence of open porosity (MTO-10, 40, 80 and 160) were post-sintered by pressure assisted technique Hot Isostatic Pressing (HIP) at 1200 °C for 2 h in argon atmosphere with pressure 200 MPa. The samples increased densities up to 96 % TD for sample MT-160. Electrical measurements were performed in the microwave field of frequency.
PB  - Belgrade : Serbian Ceramic Society
C3  - Advanced Ceramics and Application : 4th Serbian Ceramic Society Conference : program and the book of abstracts; September 21-23, 2015; Belgrade
T1  - The effect of Hot Isostatic Pressing on the MT sample densities
SP  - 55
EP  - 55
UR  - https://hdl.handle.net/21.15107/rcub_vinar_7526
ER  - 
@conference{
author = "Filipović, Suzana and Obradović, Nina and Pavlović, Vladimir B. and Kosanović, Darko and Mitrić, Miodrag and Paunović, Vesna and Pouchly, V. and Kachlik, Martin and Maca, Karel",
year = "2015",
abstract = "Mechanically activated powders (0, 10, 40, 80 and 160 minutes) were formed by isostatic pressure 300 MPa to cylindrical green bodies (φ 12 mm). First set of samples was sintered at 1300°C for 30 min in air (heating rate 10 °C/min, cooling rate 5 oC/min). These samples were re-sintered at 1200 oC for 20 h in air (heating rate 20 °C/min, cooling rate 10 oC/min). Samples reached almost 90 % TD. The second set of samples was sintered at 1400 °C for 30 in air (heating rate 10 oC/min, cooling rate 5 °C/min). Relative densities increased up to 93 % TD. The samples of absence of open porosity (MTO-10, 40, 80 and 160) were post-sintered by pressure assisted technique Hot Isostatic Pressing (HIP) at 1200 °C for 2 h in argon atmosphere with pressure 200 MPa. The samples increased densities up to 96 % TD for sample MT-160. Electrical measurements were performed in the microwave field of frequency.",
publisher = "Belgrade : Serbian Ceramic Society",
journal = "Advanced Ceramics and Application : 4th Serbian Ceramic Society Conference : program and the book of abstracts; September 21-23, 2015; Belgrade",
title = "The effect of Hot Isostatic Pressing on the MT sample densities",
pages = "55-55",
url = "https://hdl.handle.net/21.15107/rcub_vinar_7526"
}
Filipović, S., Obradović, N., Pavlović, V. B., Kosanović, D., Mitrić, M., Paunović, V., Pouchly, V., Kachlik, M.,& Maca, K.. (2015). The effect of Hot Isostatic Pressing on the MT sample densities. in Advanced Ceramics and Application : 4th Serbian Ceramic Society Conference : program and the book of abstracts; September 21-23, 2015; Belgrade
Belgrade : Serbian Ceramic Society., 55-55.
https://hdl.handle.net/21.15107/rcub_vinar_7526
Filipović S, Obradović N, Pavlović VB, Kosanović D, Mitrić M, Paunović V, Pouchly V, Kachlik M, Maca K. The effect of Hot Isostatic Pressing on the MT sample densities. in Advanced Ceramics and Application : 4th Serbian Ceramic Society Conference : program and the book of abstracts; September 21-23, 2015; Belgrade. 2015;:55-55.
https://hdl.handle.net/21.15107/rcub_vinar_7526 .
Filipović, Suzana, Obradović, Nina, Pavlović, Vladimir B., Kosanović, Darko, Mitrić, Miodrag, Paunović, Vesna, Pouchly, V., Kachlik, Martin, Maca, Karel, "The effect of Hot Isostatic Pressing on the MT sample densities" in Advanced Ceramics and Application : 4th Serbian Ceramic Society Conference : program and the book of abstracts; September 21-23, 2015; Belgrade (2015):55-55,
https://hdl.handle.net/21.15107/rcub_vinar_7526 .

Structural investigation of mechanically activated ZnO powder

Peleš, Adriana; Pavlović, Vera P.; Filipović, Suzana; Obradović, Nina; Mančić, Lidija; Krstić, Jelena; Mitrić, Miodrag; Vlahović, Branislav; Rašić, Goran; Kosanović, Darko; Pavlović, Vladimir B.

(2015)

TY  - JOUR
AU  - Peleš, Adriana
AU  - Pavlović, Vera P.
AU  - Filipović, Suzana
AU  - Obradović, Nina
AU  - Mančić, Lidija
AU  - Krstić, Jelena
AU  - Mitrić, Miodrag
AU  - Vlahović, Branislav
AU  - Rašić, Goran
AU  - Kosanović, Darko
AU  - Pavlović, Vladimir B.
PY  - 2015
UR  - https://vinar.vin.bg.ac.rs/handle/123456789/735
AB  - Commercially available ZnO powder was mechanically activated in a planetary ball mill. In order to investigate the specific surface area, pore volume and microstructure of non-activated and mechanically activated ZnO powders the authors performed N-2 physisorption, SEM and TEM. Crystallite size and lattice microstrain were analyzed by X-ray diffraction method. XRD patterns indicate that peak intensities are getting lower and expend with activation time. The reduction in crystallite size and increasing of lattice microstrain with prolonged milling time were determined applying the Rietvelds method. The difference between non-activated and the activated powder has been also observed by X-ray photoelectron spectroscopy (XPS). XPS is used for investigating the chemical bonding of ZnO powder by analyzing the energy of photoelectrons. The lattice vibration spectra were obtained using Raman spectroscopy. In Raman spectra some changes along with atypical resonant scattering were noticed, which were caused by mechanical activation. (C) 2015 Published by Elsevier B.V.
T2  - Journal of Alloys and Compounds
T1  - Structural investigation of mechanically activated ZnO powder
VL  - 648
SP  - 971
EP  - 979
DO  - 10.1016/j.jallcom.2015.06.247
ER  - 
@article{
author = "Peleš, Adriana and Pavlović, Vera P. and Filipović, Suzana and Obradović, Nina and Mančić, Lidija and Krstić, Jelena and Mitrić, Miodrag and Vlahović, Branislav and Rašić, Goran and Kosanović, Darko and Pavlović, Vladimir B.",
year = "2015",
abstract = "Commercially available ZnO powder was mechanically activated in a planetary ball mill. In order to investigate the specific surface area, pore volume and microstructure of non-activated and mechanically activated ZnO powders the authors performed N-2 physisorption, SEM and TEM. Crystallite size and lattice microstrain were analyzed by X-ray diffraction method. XRD patterns indicate that peak intensities are getting lower and expend with activation time. The reduction in crystallite size and increasing of lattice microstrain with prolonged milling time were determined applying the Rietvelds method. The difference between non-activated and the activated powder has been also observed by X-ray photoelectron spectroscopy (XPS). XPS is used for investigating the chemical bonding of ZnO powder by analyzing the energy of photoelectrons. The lattice vibration spectra were obtained using Raman spectroscopy. In Raman spectra some changes along with atypical resonant scattering were noticed, which were caused by mechanical activation. (C) 2015 Published by Elsevier B.V.",
journal = "Journal of Alloys and Compounds",
title = "Structural investigation of mechanically activated ZnO powder",
volume = "648",
pages = "971-979",
doi = "10.1016/j.jallcom.2015.06.247"
}
Peleš, A., Pavlović, V. P., Filipović, S., Obradović, N., Mančić, L., Krstić, J., Mitrić, M., Vlahović, B., Rašić, G., Kosanović, D.,& Pavlović, V. B.. (2015). Structural investigation of mechanically activated ZnO powder. in Journal of Alloys and Compounds, 648, 971-979.
https://doi.org/10.1016/j.jallcom.2015.06.247
Peleš A, Pavlović VP, Filipović S, Obradović N, Mančić L, Krstić J, Mitrić M, Vlahović B, Rašić G, Kosanović D, Pavlović VB. Structural investigation of mechanically activated ZnO powder. in Journal of Alloys and Compounds. 2015;648:971-979.
doi:10.1016/j.jallcom.2015.06.247 .
Peleš, Adriana, Pavlović, Vera P., Filipović, Suzana, Obradović, Nina, Mančić, Lidija, Krstić, Jelena, Mitrić, Miodrag, Vlahović, Branislav, Rašić, Goran, Kosanović, Darko, Pavlović, Vladimir B., "Structural investigation of mechanically activated ZnO powder" in Journal of Alloys and Compounds, 648 (2015):971-979,
https://doi.org/10.1016/j.jallcom.2015.06.247 . .
12
10
14

The Influence of Compaction Pressure on the Density and Electrical Properties of Cordierite-based Ceramics

Obradović, Nina; Dordevic, N.; Peleš, Adriana; Filipović, Suzana; Mitrić, Miodrag; Pavlović, Vladimir B.

(2015)

TY  - JOUR
AU  - Obradović, Nina
AU  - Dordevic, N.
AU  - Peleš, Adriana
AU  - Filipović, Suzana
AU  - Mitrić, Miodrag
AU  - Pavlović, Vladimir B.
PY  - 2015
UR  - https://vinar.vin.bg.ac.rs/handle/123456789/565
AB  - Due to its characteristics, cordierite, 2MgO center dot 2Al(2)O(3)center dot 5SiO(2), is a high-temperature ceramic material of a great scientific interest. Mechanical activation of the starting mixtures containing 5.00 mass% TiO2 was performed in a high-energy ball mill for 10 minutes. The compaction pressure varied from 0.5 to 6tcm(-2) (49-588 MPa). The sintering process was performed at 1350 degrees C for four hours in the air atmosphere. The phase composition of the activated and sintered samples was analyzed using X-ray diffraction. Scanning electron microscopy was used to analyze the microstructure of both compacted and sintered samples. The authors have investigated the influence of compaction pressure on the sintered samples and their electrical properties.
T2  - Science of Sintering
T1  - The Influence of Compaction Pressure on the Density and Electrical Properties of Cordierite-based Ceramics
VL  - 47
IS  - 1
SP  - 15
EP  - 22
DO  - 10.2298/SOS1501015O
ER  - 
@article{
author = "Obradović, Nina and Dordevic, N. and Peleš, Adriana and Filipović, Suzana and Mitrić, Miodrag and Pavlović, Vladimir B.",
year = "2015",
abstract = "Due to its characteristics, cordierite, 2MgO center dot 2Al(2)O(3)center dot 5SiO(2), is a high-temperature ceramic material of a great scientific interest. Mechanical activation of the starting mixtures containing 5.00 mass% TiO2 was performed in a high-energy ball mill for 10 minutes. The compaction pressure varied from 0.5 to 6tcm(-2) (49-588 MPa). The sintering process was performed at 1350 degrees C for four hours in the air atmosphere. The phase composition of the activated and sintered samples was analyzed using X-ray diffraction. Scanning electron microscopy was used to analyze the microstructure of both compacted and sintered samples. The authors have investigated the influence of compaction pressure on the sintered samples and their electrical properties.",
journal = "Science of Sintering",
title = "The Influence of Compaction Pressure on the Density and Electrical Properties of Cordierite-based Ceramics",
volume = "47",
number = "1",
pages = "15-22",
doi = "10.2298/SOS1501015O"
}
Obradović, N., Dordevic, N., Peleš, A., Filipović, S., Mitrić, M.,& Pavlović, V. B.. (2015). The Influence of Compaction Pressure on the Density and Electrical Properties of Cordierite-based Ceramics. in Science of Sintering, 47(1), 15-22.
https://doi.org/10.2298/SOS1501015O
Obradović N, Dordevic N, Peleš A, Filipović S, Mitrić M, Pavlović VB. The Influence of Compaction Pressure on the Density and Electrical Properties of Cordierite-based Ceramics. in Science of Sintering. 2015;47(1):15-22.
doi:10.2298/SOS1501015O .
Obradović, Nina, Dordevic, N., Peleš, Adriana, Filipović, Suzana, Mitrić, Miodrag, Pavlović, Vladimir B., "The Influence of Compaction Pressure on the Density and Electrical Properties of Cordierite-based Ceramics" in Science of Sintering, 47, no. 1 (2015):15-22,
https://doi.org/10.2298/SOS1501015O . .
5
8
9

Properties of Magnesium Titanate Ceramic Obtained by Two Stage Sintering

Filipović, Suzana; Obradović, Nina; Pavlović, Vladimir B.; Kosanović, Darko; Mitrić, Miodrag; Paunović, Vesna; Pouchly, V.; Kachlik, Martin; Maca, Karel

(Belgrade : Serbian Ceramic Society, 2014)

TY  - CONF
AU  - Filipović, Suzana
AU  - Obradović, Nina
AU  - Pavlović, Vladimir B.
AU  - Kosanović, Darko
AU  - Mitrić, Miodrag
AU  - Paunović, Vesna
AU  - Pouchly, V.
AU  - Kachlik, Martin
AU  - Maca, Karel
PY  - 2014
UR  - http://dais.sanu.ac.rs/123456789/614
UR  - https://vinar.vin.bg.ac.rs/handle/123456789/7492
AB  - The aim of this paper was investigation of structural and electrical properties of magnesium titanate ceramic obtained mechanochemically and subjected to two stage sintering process. Mixtures of MgO and TiO2 were treated in a planetary ball mill for several time intervals ranging from 0 to 160 minutes. Powders prepared in this way were two stage sintered, at 1400 °C in air in the first stage, and then post-sintered by pressure assisted technique Hot Isostatic Pressing (HIP) at 1280 °C in argon atmosphere with a pressure of 200 MPa. X-ray diffraction was performed in order to established phase composition of obtained ceramics. Densities of sintered samples were measured by Archimedes method. The values of density were over 96 % of theoretical one and pure MgTiO3 phase was observed. Morphology of sintered bodies was investigated by SEM, and micrographs indicate the final sintering stage and very dense ceramics. Electrical measurements were performed in the microwave field of frequency.
PB  - Belgrade : Serbian Ceramic Society
C3  - Advanced Ceramics and Application : 3rd Serbian Ceramic Society Conference : program and the book of abstracts; September 29 - October 1, 2014; Belgrade
T1  - Properties of Magnesium Titanate Ceramic Obtained by Two Stage Sintering
SP  - 118
EP  - 118
UR  - https://hdl.handle.net/21.15107/rcub_vinar_7492
ER  - 
@conference{
author = "Filipović, Suzana and Obradović, Nina and Pavlović, Vladimir B. and Kosanović, Darko and Mitrić, Miodrag and Paunović, Vesna and Pouchly, V. and Kachlik, Martin and Maca, Karel",
year = "2014",
abstract = "The aim of this paper was investigation of structural and electrical properties of magnesium titanate ceramic obtained mechanochemically and subjected to two stage sintering process. Mixtures of MgO and TiO2 were treated in a planetary ball mill for several time intervals ranging from 0 to 160 minutes. Powders prepared in this way were two stage sintered, at 1400 °C in air in the first stage, and then post-sintered by pressure assisted technique Hot Isostatic Pressing (HIP) at 1280 °C in argon atmosphere with a pressure of 200 MPa. X-ray diffraction was performed in order to established phase composition of obtained ceramics. Densities of sintered samples were measured by Archimedes method. The values of density were over 96 % of theoretical one and pure MgTiO3 phase was observed. Morphology of sintered bodies was investigated by SEM, and micrographs indicate the final sintering stage and very dense ceramics. Electrical measurements were performed in the microwave field of frequency.",
publisher = "Belgrade : Serbian Ceramic Society",
journal = "Advanced Ceramics and Application : 3rd Serbian Ceramic Society Conference : program and the book of abstracts; September 29 - October 1, 2014; Belgrade",
title = "Properties of Magnesium Titanate Ceramic Obtained by Two Stage Sintering",
pages = "118-118",
url = "https://hdl.handle.net/21.15107/rcub_vinar_7492"
}
Filipović, S., Obradović, N., Pavlović, V. B., Kosanović, D., Mitrić, M., Paunović, V., Pouchly, V., Kachlik, M.,& Maca, K.. (2014). Properties of Magnesium Titanate Ceramic Obtained by Two Stage Sintering. in Advanced Ceramics and Application : 3rd Serbian Ceramic Society Conference : program and the book of abstracts; September 29 - October 1, 2014; Belgrade
Belgrade : Serbian Ceramic Society., 118-118.
https://hdl.handle.net/21.15107/rcub_vinar_7492
Filipović S, Obradović N, Pavlović VB, Kosanović D, Mitrić M, Paunović V, Pouchly V, Kachlik M, Maca K. Properties of Magnesium Titanate Ceramic Obtained by Two Stage Sintering. in Advanced Ceramics and Application : 3rd Serbian Ceramic Society Conference : program and the book of abstracts; September 29 - October 1, 2014; Belgrade. 2014;:118-118.
https://hdl.handle.net/21.15107/rcub_vinar_7492 .
Filipović, Suzana, Obradović, Nina, Pavlović, Vladimir B., Kosanović, Darko, Mitrić, Miodrag, Paunović, Vesna, Pouchly, V., Kachlik, Martin, Maca, Karel, "Properties of Magnesium Titanate Ceramic Obtained by Two Stage Sintering" in Advanced Ceramics and Application : 3rd Serbian Ceramic Society Conference : program and the book of abstracts; September 29 - October 1, 2014; Belgrade (2014):118-118,
https://hdl.handle.net/21.15107/rcub_vinar_7492 .

Mehanohemijska sinteza magnezijum titanata

Filipović, Suzana; Obradović, Nina; Pavlović, Vladimir B.; Peleš, Adriana; Marković, Smilja; Mitrić, Miodrag; Mitrović, Nebojša

(Beograd : Društvo za ETRAN, 2014)

TY  - CONF
AU  - Filipović, Suzana
AU  - Obradović, Nina
AU  - Pavlović, Vladimir B.
AU  - Peleš, Adriana
AU  - Marković, Smilja
AU  - Mitrić, Miodrag
AU  - Mitrović, Nebojša
PY  - 2014
UR  - https://vinar.vin.bg.ac.rs/handle/123456789/7500
AB  - Mehanohemija je proces Kojim se iz čvrstih polaznuih komponentiprocesom mlevenja može dobiti željeni proizvod reakcije. Smeša polaznih oksids MgO i TiO2 je podvrgnuta mehaničkom tretmanu u vremenskim intervalima od 0 do 160 minuta u visokoenergetskom planetarnom mlinu. Morfologija prahova je ispitana SEM analizom i praćenjem raspodele veličina čestica na laserskom analizatoru, dok su promene u faznom sastavu i mikrostrukturnim parametrima ispraćene snimanjem XRD. Radi određivanja karakterističnih temperatura reakcija koje se odigravaju u aktiviranim sistemima snimljeni su termogrami u intervalu od sobne temperature do 1100C. Utvrđeno je da se prvi tragovi magnezijum titanata javljaju već nakon 40 minuta aktivacije, dok je nakon 160 minuta prisutan čist magnezijum titanat.
PB  - Beograd : Društvo za ETRAN
C3  - Zbornik apstrakata i program 58. konferencije ETRAN-a, Vrnjačka Banja, 2-5. jun 2014.
T1  - Mehanohemijska sinteza magnezijum titanata
SP  - 46
EP  - 46
UR  - https://hdl.handle.net/21.15107/rcub_vinar_7500
ER  - 
@conference{
author = "Filipović, Suzana and Obradović, Nina and Pavlović, Vladimir B. and Peleš, Adriana and Marković, Smilja and Mitrić, Miodrag and Mitrović, Nebojša",
year = "2014",
abstract = "Mehanohemija je proces Kojim se iz čvrstih polaznuih komponentiprocesom mlevenja može dobiti željeni proizvod reakcije. Smeša polaznih oksids MgO i TiO2 je podvrgnuta mehaničkom tretmanu u vremenskim intervalima od 0 do 160 minuta u visokoenergetskom planetarnom mlinu. Morfologija prahova je ispitana SEM analizom i praćenjem raspodele veličina čestica na laserskom analizatoru, dok su promene u faznom sastavu i mikrostrukturnim parametrima ispraćene snimanjem XRD. Radi određivanja karakterističnih temperatura reakcija koje se odigravaju u aktiviranim sistemima snimljeni su termogrami u intervalu od sobne temperature do 1100C. Utvrđeno je da se prvi tragovi magnezijum titanata javljaju već nakon 40 minuta aktivacije, dok je nakon 160 minuta prisutan čist magnezijum titanat.",
publisher = "Beograd : Društvo za ETRAN",
journal = "Zbornik apstrakata i program 58. konferencije ETRAN-a, Vrnjačka Banja, 2-5. jun 2014.",
title = "Mehanohemijska sinteza magnezijum titanata",
pages = "46-46",
url = "https://hdl.handle.net/21.15107/rcub_vinar_7500"
}
Filipović, S., Obradović, N., Pavlović, V. B., Peleš, A., Marković, S., Mitrić, M.,& Mitrović, N.. (2014). Mehanohemijska sinteza magnezijum titanata. in Zbornik apstrakata i program 58. konferencije ETRAN-a, Vrnjačka Banja, 2-5. jun 2014.
Beograd : Društvo za ETRAN., 46-46.
https://hdl.handle.net/21.15107/rcub_vinar_7500
Filipović S, Obradović N, Pavlović VB, Peleš A, Marković S, Mitrić M, Mitrović N. Mehanohemijska sinteza magnezijum titanata. in Zbornik apstrakata i program 58. konferencije ETRAN-a, Vrnjačka Banja, 2-5. jun 2014.. 2014;:46-46.
https://hdl.handle.net/21.15107/rcub_vinar_7500 .
Filipović, Suzana, Obradović, Nina, Pavlović, Vladimir B., Peleš, Adriana, Marković, Smilja, Mitrić, Miodrag, Mitrović, Nebojša, "Mehanohemijska sinteza magnezijum titanata" in Zbornik apstrakata i program 58. konferencije ETRAN-a, Vrnjačka Banja, 2-5. jun 2014. (2014):46-46,
https://hdl.handle.net/21.15107/rcub_vinar_7500 .

Properties of Magnesium Titanate Ceramic Obtained by Two Stage Sintering

Filipović, Suzana; Obradović, Nina; Pavlović, Vladimir B.; Kosanović, Darko; Mitrić, Miodrag; Paunović, Vesna; Pouchly, V.; Kachlik, Martin; Maca, Karel

(2014)

TY  - CONF
AU  - Filipović, Suzana
AU  - Obradović, Nina
AU  - Pavlović, Vladimir B.
AU  - Kosanović, Darko
AU  - Mitrić, Miodrag
AU  - Paunović, Vesna
AU  - Pouchly, V.
AU  - Kachlik, Martin
AU  - Maca, Karel
PY  - 2014
UR  - http://dais.sanu.ac.rs/123456789/638
UR  - https://vinar.vin.bg.ac.rs/handle/123456789/7502
AB  - Poster presented at the III Serbian Ceramic Society Conference, 29th September - 1st October, Belgrade, 2014
T1  - Properties of Magnesium Titanate Ceramic Obtained by Two Stage Sintering
UR  - https://hdl.handle.net/21.15107/rcub_vinar_7502
ER  - 
@conference{
author = "Filipović, Suzana and Obradović, Nina and Pavlović, Vladimir B. and Kosanović, Darko and Mitrić, Miodrag and Paunović, Vesna and Pouchly, V. and Kachlik, Martin and Maca, Karel",
year = "2014",
abstract = "Poster presented at the III Serbian Ceramic Society Conference, 29th September - 1st October, Belgrade, 2014",
title = "Properties of Magnesium Titanate Ceramic Obtained by Two Stage Sintering",
url = "https://hdl.handle.net/21.15107/rcub_vinar_7502"
}
Filipović, S., Obradović, N., Pavlović, V. B., Kosanović, D., Mitrić, M., Paunović, V., Pouchly, V., Kachlik, M.,& Maca, K.. (2014). Properties of Magnesium Titanate Ceramic Obtained by Two Stage Sintering. .
https://hdl.handle.net/21.15107/rcub_vinar_7502
Filipović S, Obradović N, Pavlović VB, Kosanović D, Mitrić M, Paunović V, Pouchly V, Kachlik M, Maca K. Properties of Magnesium Titanate Ceramic Obtained by Two Stage Sintering. 2014;.
https://hdl.handle.net/21.15107/rcub_vinar_7502 .
Filipović, Suzana, Obradović, Nina, Pavlović, Vladimir B., Kosanović, Darko, Mitrić, Miodrag, Paunović, Vesna, Pouchly, V., Kachlik, Martin, Maca, Karel, "Properties of Magnesium Titanate Ceramic Obtained by Two Stage Sintering" (2014),
https://hdl.handle.net/21.15107/rcub_vinar_7502 .

Advantages of Combined Sintering Compared to Conventional Sintering of Mechanically Activated Magnesium Titanate

Filipović, Suzana; Obradović, Nina; Pavlović, Vladimir B.; Kosanović, Darko; Mitrić, Miodrag; Mitrovic, N.; Pouchly, V.; Kachlik, M.; Maca, Karel

(2014)

TY  - JOUR
AU  - Filipović, Suzana
AU  - Obradović, Nina
AU  - Pavlović, Vladimir B.
AU  - Kosanović, Darko
AU  - Mitrić, Miodrag
AU  - Mitrovic, N.
AU  - Pouchly, V.
AU  - Kachlik, M.
AU  - Maca, Karel
PY  - 2014
UR  - https://vinar.vin.bg.ac.rs/handle/123456789/373
AB  - In this article, the advantages of combined sintering in comparison with the conventional one, of mechanically activated magnesium titanate ceramic were investigated. The stoichiometric mixtures of MgO and TiO2 were mechano-chemically activated for 0, 10, 40, 80 and 160 minutes by ball milling and then isostatically pressed (CIP) to form green bodies. Conventional sintering was realized by heating up to 1400 degrees C and hold for 30 minutes in air atmosphere. Resulting ceramic samples with closed porosity were post-sintered by pressure assisted technique Hot Isostatic Pressing (HIP) at 1280 degrees C/3h in argon atmosphere with a pressure of 200 MPa. The best results were observed in the case of samples post-sintered by HIP, when single-phase MgTiO3 samples with relative density of 96% were prepared.
T2  - Science of Sintering
T1  - Advantages of Combined Sintering Compared to Conventional Sintering of Mechanically Activated Magnesium Titanate
VL  - 46
IS  - 3
SP  - 283
EP  - 290
DO  - 10.2298/SOS1403283F
ER  - 
@article{
author = "Filipović, Suzana and Obradović, Nina and Pavlović, Vladimir B. and Kosanović, Darko and Mitrić, Miodrag and Mitrovic, N. and Pouchly, V. and Kachlik, M. and Maca, Karel",
year = "2014",
abstract = "In this article, the advantages of combined sintering in comparison with the conventional one, of mechanically activated magnesium titanate ceramic were investigated. The stoichiometric mixtures of MgO and TiO2 were mechano-chemically activated for 0, 10, 40, 80 and 160 minutes by ball milling and then isostatically pressed (CIP) to form green bodies. Conventional sintering was realized by heating up to 1400 degrees C and hold for 30 minutes in air atmosphere. Resulting ceramic samples with closed porosity were post-sintered by pressure assisted technique Hot Isostatic Pressing (HIP) at 1280 degrees C/3h in argon atmosphere with a pressure of 200 MPa. The best results were observed in the case of samples post-sintered by HIP, when single-phase MgTiO3 samples with relative density of 96% were prepared.",
journal = "Science of Sintering",
title = "Advantages of Combined Sintering Compared to Conventional Sintering of Mechanically Activated Magnesium Titanate",
volume = "46",
number = "3",
pages = "283-290",
doi = "10.2298/SOS1403283F"
}
Filipović, S., Obradović, N., Pavlović, V. B., Kosanović, D., Mitrić, M., Mitrovic, N., Pouchly, V., Kachlik, M.,& Maca, K.. (2014). Advantages of Combined Sintering Compared to Conventional Sintering of Mechanically Activated Magnesium Titanate. in Science of Sintering, 46(3), 283-290.
https://doi.org/10.2298/SOS1403283F
Filipović S, Obradović N, Pavlović VB, Kosanović D, Mitrić M, Mitrovic N, Pouchly V, Kachlik M, Maca K. Advantages of Combined Sintering Compared to Conventional Sintering of Mechanically Activated Magnesium Titanate. in Science of Sintering. 2014;46(3):283-290.
doi:10.2298/SOS1403283F .
Filipović, Suzana, Obradović, Nina, Pavlović, Vladimir B., Kosanović, Darko, Mitrić, Miodrag, Mitrovic, N., Pouchly, V., Kachlik, M., Maca, Karel, "Advantages of Combined Sintering Compared to Conventional Sintering of Mechanically Activated Magnesium Titanate" in Science of Sintering, 46, no. 3 (2014):283-290,
https://doi.org/10.2298/SOS1403283F . .
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