TY  - CONF
AU  - Filipović, Suzana
AU  - Obradović, Nina
AU  - Fahrenholtz, William G.
AU  - Smith, Steven
AU  - Mirković, M.
AU  - Peleš, Adriana
AU  - Tadić, Nenad
AU  - Đorđević, Antonije
PY  - 2022
UR  - https://vinar.vin.bg.ac.rs/handle/123456789/10825
AB  - Perovskite ceramic material based on MgTiO3 is used in various types of electronic devices owing to its dielectric properties, high dielectric constant, and low losses. These features can be tailored by setting preparation conditions. Densification of magnesium titanate by Spark Plasma Sintering (SPS) was the aim of this work. First, the mechanical activation in the highenergy ball mill was applied on the powder of MgO-TiO2 mixed in mole ratio 1:1. Prepared powder mixtures, activated for different times, were SPS sintered, at 1200 o C with a heating rate of 100o C/min. After reaching the desired temperature, a uniaxial pressure of 50 MPa was applied, and dwelled at this condition for 5 min, followed by cooling to room temperature at 5o C/min. The starting powders, activated mixtures, and sintered ceramics bodies were investigated by X-ray diffraction, scanning electron microscopy (SEM), and energy dispersive spectroscopy (EDS). The presence of the MgTi2O5 phase was noticed for the nonmilled ceramics. In the samples obtained from milled powders, MgTi2O5 was detected in EDS spectra in a lower amount, below the threshold of the XRD method. Dielectric measurements were performed at a wide range of frequencies and temperatures. The highest value of the hardness was obtained from powder milled for 15 min before SPS.
PB  - Belgrade : Serbian Ceramic Society
C3  - Advanced Ceramics and Application : 10th Serbian Ceramic Society Conference : program and the book of abstracts; September 26-27, 2022; Belgrade
T1  - Effect of high energy ball milling on sintering of MgO-TiO2 system
SP  - 88
UR  - https://hdl.handle.net/21.15107/rcub_vinar_10825
ER  - 

@conference{
author = "Filipović, Suzana and Obradović, Nina and Fahrenholtz, William G. and Smith, Steven and Mirković, M. and Peleš, Adriana and Tadić, Nenad and Đorđević, Antonije",
year = "2022",
abstract = "Perovskite ceramic material based on MgTiO3 is used in various types of electronic devices owing to its dielectric properties, high dielectric constant, and low losses. These features can be tailored by setting preparation conditions. Densification of magnesium titanate by Spark Plasma Sintering (SPS) was the aim of this work. First, the mechanical activation in the highenergy ball mill was applied on the powder of MgO-TiO2 mixed in mole ratio 1:1. Prepared powder mixtures, activated for different times, were SPS sintered, at 1200 o C with a heating rate of 100o C/min. After reaching the desired temperature, a uniaxial pressure of 50 MPa was applied, and dwelled at this condition for 5 min, followed by cooling to room temperature at 5o C/min. The starting powders, activated mixtures, and sintered ceramics bodies were investigated by X-ray diffraction, scanning electron microscopy (SEM), and energy dispersive spectroscopy (EDS). The presence of the MgTi2O5 phase was noticed for the nonmilled ceramics. In the samples obtained from milled powders, MgTi2O5 was detected in EDS spectra in a lower amount, below the threshold of the XRD method. Dielectric measurements were performed at a wide range of frequencies and temperatures. The highest value of the hardness was obtained from powder milled for 15 min before SPS.",
publisher = "Belgrade : Serbian Ceramic Society",
journal = "Advanced Ceramics and Application : 10th Serbian Ceramic Society Conference : program and the book of abstracts; September 26-27, 2022; Belgrade",
title = "Effect of high energy ball milling on sintering of MgO-TiO2 system",
pages = "88",
url = "https://hdl.handle.net/21.15107/rcub_vinar_10825"
}

Filipović, S., Obradović, N., Fahrenholtz, W. G., Smith, S., Mirković, M., Peleš, A., Tadić, N.,& Đorđević, A.. (2022). Effect of high energy ball milling on sintering of MgO-TiO2 system. in Advanced Ceramics and Application : 10th Serbian Ceramic Society Conference : program and the book of abstracts; September 26-27, 2022; Belgrade
Belgrade : Serbian Ceramic Society., 88.
https://hdl.handle.net/21.15107/rcub_vinar_10825

Filipović S, Obradović N, Fahrenholtz WG, Smith S, Mirković M, Peleš A, Tadić N, Đorđević A. Effect of high energy ball milling on sintering of MgO-TiO2 system. in Advanced Ceramics and Application : 10th Serbian Ceramic Society Conference : program and the book of abstracts; September 26-27, 2022; Belgrade. 2022;:88.
https://hdl.handle.net/21.15107/rcub_vinar_10825 .

Filipović, Suzana, Obradović, Nina, Fahrenholtz, William G., Smith, Steven, Mirković, M., Peleš, Adriana, Tadić, Nenad, Đorđević, Antonije, "Effect of high energy ball milling on sintering of MgO-TiO2 system" in Advanced Ceramics and Application : 10th Serbian Ceramic Society Conference : program and the book of abstracts; September 26-27, 2022; Belgrade (2022):88,
https://hdl.handle.net/21.15107/rcub_vinar_10825 .

TY  - JOUR
AU  - Peleš, Adriana
AU  - Aleksić, Obrad S.
AU  - Pavlović, Vera P.
AU  - Đoković, Vladimir
AU  - Dojčilović, Radovan
AU  - Nikolić, Zoran M.
AU  - Marinković, Filip S.
AU  - Mitrić, Miodrag
AU  - Blagojević, Vladimir D.
AU  - Vlahović, Branislav
AU  - Pavlović, Vladimir B.
PY  - 2018
UR  - http://stacks.iop.org/1402-4896/93/i=10/a=105801?key=crossref.54536d8babe95dbc820e50211f592252
UR  - https://vinar.vin.bg.ac.rs/handle/123456789/7898
AB  - The influence of the mechanical activation of ZnO nanoparticle fillers on the structural and electrical properties of the matrix of poly(vinylidenefluoride)-ZnO (PVDF-ZnO) films was investigated. Transmission electron microscopy and scanning electron microscopy analyses showed that mechanical activation in a high energy planetary ball mill reduces the size of ZnO particles. X-ray diffraction and Raman spectroscopy revealed that PVDF crystallized predominantly as the γ-phase. Non-activated ZnO filler reduces the degree of the crystallinity of the matrix and promotes crystallization of α-phase of PVDF in the film, while the fillers activated for 5 and 10 min induce crystallization of β-phase, indicating that mechanical activation of the filler can be used as a general method for fabrication of PVDF composites with increased content of piezoelectric β-phase crystals. Dielectric spectroscopy measurements show that polymer composite with the high content of β-phase (with ZnO filler activated for 5 min) exhibits the highest value of dielectric permittivity in 150-400 K range of temperatures. Kinetic analysis shows combined effects of increased surface area and increased concentration of surface defects on the interactions between polymer chains and activated nanoparticles. © 2018 IOP Publishing Ltd.
T2  - Physica Scripta
T1  - Structural and electrical properties of ferroelectric poly(vinylidene fluoride) and mechanically activated ZnO nanoparticle composite films
VL  - 93
IS  - 10
SP  - 105801
DO  - 10.1088/1402-4896/aad749
ER  - 

@article{
author = "Peleš, Adriana and Aleksić, Obrad S. and Pavlović, Vera P. and Đoković, Vladimir and Dojčilović, Radovan and Nikolić, Zoran M. and Marinković, Filip S. and Mitrić, Miodrag and Blagojević, Vladimir D. and Vlahović, Branislav and Pavlović, Vladimir B.",
year = "2018",
abstract = "The influence of the mechanical activation of ZnO nanoparticle fillers on the structural and electrical properties of the matrix of poly(vinylidenefluoride)-ZnO (PVDF-ZnO) films was investigated. Transmission electron microscopy and scanning electron microscopy analyses showed that mechanical activation in a high energy planetary ball mill reduces the size of ZnO particles. X-ray diffraction and Raman spectroscopy revealed that PVDF crystallized predominantly as the γ-phase. Non-activated ZnO filler reduces the degree of the crystallinity of the matrix and promotes crystallization of α-phase of PVDF in the film, while the fillers activated for 5 and 10 min induce crystallization of β-phase, indicating that mechanical activation of the filler can be used as a general method for fabrication of PVDF composites with increased content of piezoelectric β-phase crystals. Dielectric spectroscopy measurements show that polymer composite with the high content of β-phase (with ZnO filler activated for 5 min) exhibits the highest value of dielectric permittivity in 150-400 K range of temperatures. Kinetic analysis shows combined effects of increased surface area and increased concentration of surface defects on the interactions between polymer chains and activated nanoparticles. © 2018 IOP Publishing Ltd.",
journal = "Physica Scripta",
title = "Structural and electrical properties of ferroelectric poly(vinylidene fluoride) and mechanically activated ZnO nanoparticle composite films",
volume = "93",
number = "10",
pages = "105801",
doi = "10.1088/1402-4896/aad749"
}

Peleš, A., Aleksić, O. S., Pavlović, V. P., Đoković, V., Dojčilović, R., Nikolić, Z. M., Marinković, F. S., Mitrić, M., Blagojević, V. D., Vlahović, B.,& Pavlović, V. B.. (2018). Structural and electrical properties of ferroelectric poly(vinylidene fluoride) and mechanically activated ZnO nanoparticle composite films. in Physica Scripta, 93(10), 105801.
https://doi.org/10.1088/1402-4896/aad749

Peleš A, Aleksić OS, Pavlović VP, Đoković V, Dojčilović R, Nikolić ZM, Marinković FS, Mitrić M, Blagojević VD, Vlahović B, Pavlović VB. Structural and electrical properties of ferroelectric poly(vinylidene fluoride) and mechanically activated ZnO nanoparticle composite films. in Physica Scripta. 2018;93(10):105801.
doi:10.1088/1402-4896/aad749 .

Peleš, Adriana, Aleksić, Obrad S., Pavlović, Vera P., Đoković, Vladimir, Dojčilović, Radovan, Nikolić, Zoran M., Marinković, Filip S., Mitrić, Miodrag, Blagojević, Vladimir D., Vlahović, Branislav, Pavlović, Vladimir B., "Structural and electrical properties of ferroelectric poly(vinylidene fluoride) and mechanically activated ZnO nanoparticle composite films" in Physica Scripta, 93, no. 10 (2018):105801,
https://doi.org/10.1088/1402-4896/aad749 . .

TY  - JOUR
AU  - Peleš, Adriana
AU  - Pavlović, Vera P.
AU  - Filipović, Suzana
AU  - Obradović, Nina
AU  - Mančić, Lidija
AU  - Krstić, Jelena
AU  - Mitrić, Miodrag
AU  - Vlahović, Branislav
AU  - Rašić, Goran
AU  - Kosanović, Darko
AU  - Pavlović, Vladimir B.
PY  - 2015
UR  - https://vinar.vin.bg.ac.rs/handle/123456789/735
AB  - Commercially available ZnO powder was mechanically activated in a planetary ball mill. In order to investigate the specific surface area, pore volume and microstructure of non-activated and mechanically activated ZnO powders the authors performed N-2 physisorption, SEM and TEM. Crystallite size and lattice microstrain were analyzed by X-ray diffraction method. XRD patterns indicate that peak intensities are getting lower and expend with activation time. The reduction in crystallite size and increasing of lattice microstrain with prolonged milling time were determined applying the Rietvelds method. The difference between non-activated and the activated powder has been also observed by X-ray photoelectron spectroscopy (XPS). XPS is used for investigating the chemical bonding of ZnO powder by analyzing the energy of photoelectrons. The lattice vibration spectra were obtained using Raman spectroscopy. In Raman spectra some changes along with atypical resonant scattering were noticed, which were caused by mechanical activation. (C) 2015 Published by Elsevier B.V.
T2  - Journal of Alloys and Compounds
T1  - Structural investigation of mechanically activated ZnO powder
VL  - 648
SP  - 971
EP  - 979
DO  - 10.1016/j.jallcom.2015.06.247
ER  - 

@article{
author = "Peleš, Adriana and Pavlović, Vera P. and Filipović, Suzana and Obradović, Nina and Mančić, Lidija and Krstić, Jelena and Mitrić, Miodrag and Vlahović, Branislav and Rašić, Goran and Kosanović, Darko and Pavlović, Vladimir B.",
year = "2015",
abstract = "Commercially available ZnO powder was mechanically activated in a planetary ball mill. In order to investigate the specific surface area, pore volume and microstructure of non-activated and mechanically activated ZnO powders the authors performed N-2 physisorption, SEM and TEM. Crystallite size and lattice microstrain were analyzed by X-ray diffraction method. XRD patterns indicate that peak intensities are getting lower and expend with activation time. The reduction in crystallite size and increasing of lattice microstrain with prolonged milling time were determined applying the Rietvelds method. The difference between non-activated and the activated powder has been also observed by X-ray photoelectron spectroscopy (XPS). XPS is used for investigating the chemical bonding of ZnO powder by analyzing the energy of photoelectrons. The lattice vibration spectra were obtained using Raman spectroscopy. In Raman spectra some changes along with atypical resonant scattering were noticed, which were caused by mechanical activation. (C) 2015 Published by Elsevier B.V.",
journal = "Journal of Alloys and Compounds",
title = "Structural investigation of mechanically activated ZnO powder",
volume = "648",
pages = "971-979",
doi = "10.1016/j.jallcom.2015.06.247"
}

Peleš, A., Pavlović, V. P., Filipović, S., Obradović, N., Mančić, L., Krstić, J., Mitrić, M., Vlahović, B., Rašić, G., Kosanović, D.,& Pavlović, V. B.. (2015). Structural investigation of mechanically activated ZnO powder. in Journal of Alloys and Compounds, 648, 971-979.
https://doi.org/10.1016/j.jallcom.2015.06.247

Peleš A, Pavlović VP, Filipović S, Obradović N, Mančić L, Krstić J, Mitrić M, Vlahović B, Rašić G, Kosanović D, Pavlović VB. Structural investigation of mechanically activated ZnO powder. in Journal of Alloys and Compounds. 2015;648:971-979.
doi:10.1016/j.jallcom.2015.06.247 .

Peleš, Adriana, Pavlović, Vera P., Filipović, Suzana, Obradović, Nina, Mančić, Lidija, Krstić, Jelena, Mitrić, Miodrag, Vlahović, Branislav, Rašić, Goran, Kosanović, Darko, Pavlović, Vladimir B., "Structural investigation of mechanically activated ZnO powder" in Journal of Alloys and Compounds, 648 (2015):971-979,
https://doi.org/10.1016/j.jallcom.2015.06.247 . .

TY  - JOUR
AU  - Obradović, Nina
AU  - Dordevic, N.
AU  - Peleš, Adriana
AU  - Filipović, Suzana
AU  - Mitrić, Miodrag
AU  - Pavlović, Vladimir B.
PY  - 2015
UR  - https://vinar.vin.bg.ac.rs/handle/123456789/565
AB  - Due to its characteristics, cordierite, 2MgO center dot 2Al(2)O(3)center dot 5SiO(2), is a high-temperature ceramic material of a great scientific interest. Mechanical activation of the starting mixtures containing 5.00 mass% TiO2 was performed in a high-energy ball mill for 10 minutes. The compaction pressure varied from 0.5 to 6tcm(-2) (49-588 MPa). The sintering process was performed at 1350 degrees C for four hours in the air atmosphere. The phase composition of the activated and sintered samples was analyzed using X-ray diffraction. Scanning electron microscopy was used to analyze the microstructure of both compacted and sintered samples. The authors have investigated the influence of compaction pressure on the sintered samples and their electrical properties.
T2  - Science of Sintering
T1  - The Influence of Compaction Pressure on the Density and Electrical Properties of Cordierite-based Ceramics
VL  - 47
IS  - 1
SP  - 15
EP  - 22
DO  - 10.2298/SOS1501015O
ER  - 

@article{
author = "Obradović, Nina and Dordevic, N. and Peleš, Adriana and Filipović, Suzana and Mitrić, Miodrag and Pavlović, Vladimir B.",
year = "2015",
abstract = "Due to its characteristics, cordierite, 2MgO center dot 2Al(2)O(3)center dot 5SiO(2), is a high-temperature ceramic material of a great scientific interest. Mechanical activation of the starting mixtures containing 5.00 mass% TiO2 was performed in a high-energy ball mill for 10 minutes. The compaction pressure varied from 0.5 to 6tcm(-2) (49-588 MPa). The sintering process was performed at 1350 degrees C for four hours in the air atmosphere. The phase composition of the activated and sintered samples was analyzed using X-ray diffraction. Scanning electron microscopy was used to analyze the microstructure of both compacted and sintered samples. The authors have investigated the influence of compaction pressure on the sintered samples and their electrical properties.",
journal = "Science of Sintering",
title = "The Influence of Compaction Pressure on the Density and Electrical Properties of Cordierite-based Ceramics",
volume = "47",
number = "1",
pages = "15-22",
doi = "10.2298/SOS1501015O"
}

Obradović, N., Dordevic, N., Peleš, A., Filipović, S., Mitrić, M.,& Pavlović, V. B.. (2015). The Influence of Compaction Pressure on the Density and Electrical Properties of Cordierite-based Ceramics. in Science of Sintering, 47(1), 15-22.
https://doi.org/10.2298/SOS1501015O

Obradović N, Dordevic N, Peleš A, Filipović S, Mitrić M, Pavlović VB. The Influence of Compaction Pressure on the Density and Electrical Properties of Cordierite-based Ceramics. in Science of Sintering. 2015;47(1):15-22.
doi:10.2298/SOS1501015O .

Obradović, Nina, Dordevic, N., Peleš, Adriana, Filipović, Suzana, Mitrić, Miodrag, Pavlović, Vladimir B., "The Influence of Compaction Pressure on the Density and Electrical Properties of Cordierite-based Ceramics" in Science of Sintering, 47, no. 1 (2015):15-22,
https://doi.org/10.2298/SOS1501015O . .

TY  - CONF
AU  - Filipović, Suzana
AU  - Obradović, Nina
AU  - Pavlović, Vladimir B.
AU  - Peleš, Adriana
AU  - Marković, Smilja
AU  - Mitrić, Miodrag
AU  - Mitrović, Nebojša
PY  - 2014
UR  - https://vinar.vin.bg.ac.rs/handle/123456789/7500
AB  - Mehanohemija je proces Kojim se iz čvrstih polaznuih komponentiprocesom mlevenja može dobiti željeni proizvod reakcije. Smeša polaznih oksids MgO i TiO2 je podvrgnuta mehaničkom tretmanu u vremenskim intervalima od 0 do 160 minuta u visokoenergetskom planetarnom mlinu. Morfologija prahova je ispitana SEM analizom i praćenjem raspodele veličina čestica na laserskom analizatoru, dok su promene u faznom sastavu i mikrostrukturnim parametrima ispraćene snimanjem XRD. Radi određivanja karakterističnih temperatura reakcija koje se odigravaju u aktiviranim sistemima snimljeni su termogrami u intervalu od sobne temperature do 1100C. Utvrđeno je da se prvi tragovi magnezijum titanata javljaju već nakon 40 minuta aktivacije, dok je nakon 160 minuta prisutan čist magnezijum titanat.
PB  - Beograd : Društvo za ETRAN
C3  - Zbornik apstrakata i program 58. konferencije ETRAN-a, Vrnjačka Banja, 2-5. jun 2014.
T1  - Mehanohemijska sinteza magnezijum titanata
SP  - 46
EP  - 46
UR  - https://hdl.handle.net/21.15107/rcub_vinar_7500
ER  - 

@conference{
author = "Filipović, Suzana and Obradović, Nina and Pavlović, Vladimir B. and Peleš, Adriana and Marković, Smilja and Mitrić, Miodrag and Mitrović, Nebojša",
year = "2014",
abstract = "Mehanohemija je proces Kojim se iz čvrstih polaznuih komponentiprocesom mlevenja može dobiti željeni proizvod reakcije. Smeša polaznih oksids MgO i TiO2 je podvrgnuta mehaničkom tretmanu u vremenskim intervalima od 0 do 160 minuta u visokoenergetskom planetarnom mlinu. Morfologija prahova je ispitana SEM analizom i praćenjem raspodele veličina čestica na laserskom analizatoru, dok su promene u faznom sastavu i mikrostrukturnim parametrima ispraćene snimanjem XRD. Radi određivanja karakterističnih temperatura reakcija koje se odigravaju u aktiviranim sistemima snimljeni su termogrami u intervalu od sobne temperature do 1100C. Utvrđeno je da se prvi tragovi magnezijum titanata javljaju već nakon 40 minuta aktivacije, dok je nakon 160 minuta prisutan čist magnezijum titanat.",
publisher = "Beograd : Društvo za ETRAN",
journal = "Zbornik apstrakata i program 58. konferencije ETRAN-a, Vrnjačka Banja, 2-5. jun 2014.",
title = "Mehanohemijska sinteza magnezijum titanata",
pages = "46-46",
url = "https://hdl.handle.net/21.15107/rcub_vinar_7500"
}

Filipović, S., Obradović, N., Pavlović, V. B., Peleš, A., Marković, S., Mitrić, M.,& Mitrović, N.. (2014). Mehanohemijska sinteza magnezijum titanata. in Zbornik apstrakata i program 58. konferencije ETRAN-a, Vrnjačka Banja, 2-5. jun 2014.
Beograd : Društvo za ETRAN., 46-46.
https://hdl.handle.net/21.15107/rcub_vinar_7500

Filipović S, Obradović N, Pavlović VB, Peleš A, Marković S, Mitrić M, Mitrović N. Mehanohemijska sinteza magnezijum titanata. in Zbornik apstrakata i program 58. konferencije ETRAN-a, Vrnjačka Banja, 2-5. jun 2014.. 2014;:46-46.
https://hdl.handle.net/21.15107/rcub_vinar_7500 .

Filipović, Suzana, Obradović, Nina, Pavlović, Vladimir B., Peleš, Adriana, Marković, Smilja, Mitrić, Miodrag, Mitrović, Nebojša, "Mehanohemijska sinteza magnezijum titanata" in Zbornik apstrakata i program 58. konferencije ETRAN-a, Vrnjačka Banja, 2-5. jun 2014. (2014):46-46,
https://hdl.handle.net/21.15107/rcub_vinar_7500 .

TY  - CONF
AU  - Obradović, Nina
AU  - Peleš, Adriana
AU  - Đorđević, N.
AU  - Marković, Smilja
AU  - Mitrić, Miodrag
AU  - Pavlović, Vladimir B.
PY  - 2013
UR  - http://dais.sanu.ac.rs/123456789/402
UR  - https://vinar.vin.bg.ac.rs/handle/123456789/7420
AB  - According to its low temperature thermal expansion coefficient, low dielectric constant, also good mechanical properties, cordierite, 2MgO×2Al2O3×5SiO2, represents a very attractive hightemperature ceramic material. In this study, cordierite was prepared by solid state reaction of the MgO, Al2O3 and SiO2 mixture. One of the components from the mixture, SiO2, was mechanically activated in a high energy ball mill during 5 and 10 minutes. The applied pressure before the sintering process was 2 t/cm2. Sintering process of mixtures containing non-activated and activated SiO2 powder was performed at 1350 oC for 4h in the air atmosphere. The phase composition of starting oxides and sintered samples was analyzed by the X-ray diffraction method. Particle size analysis was performed to investigate the differences between starting components. Scanning electron microscopy was done to analyze the microstructure of both components and sintered samples. This paper investigates the influence of one mechanically activated SiO2 component on the densities of green bodies as well as on the sintered samples, along with electrical properties of cordierite ceramics.
PB  - Belgrade : Materials Research Society of Serbia
C3  - The Fifteenth Annual Conference YUCOMAT 2013: Programme and the Book of Abstracts
T1  - Influence of one activated component on the sintering process of three phase system
SP  - 103
EP  - 103
UR  - https://hdl.handle.net/21.15107/rcub_vinar_7420
ER  - 

@conference{
author = "Obradović, Nina and Peleš, Adriana and Đorđević, N. and Marković, Smilja and Mitrić, Miodrag and Pavlović, Vladimir B.",
year = "2013",
abstract = "According to its low temperature thermal expansion coefficient, low dielectric constant, also good mechanical properties, cordierite, 2MgO×2Al2O3×5SiO2, represents a very attractive hightemperature ceramic material. In this study, cordierite was prepared by solid state reaction of the MgO, Al2O3 and SiO2 mixture. One of the components from the mixture, SiO2, was mechanically activated in a high energy ball mill during 5 and 10 minutes. The applied pressure before the sintering process was 2 t/cm2. Sintering process of mixtures containing non-activated and activated SiO2 powder was performed at 1350 oC for 4h in the air atmosphere. The phase composition of starting oxides and sintered samples was analyzed by the X-ray diffraction method. Particle size analysis was performed to investigate the differences between starting components. Scanning electron microscopy was done to analyze the microstructure of both components and sintered samples. This paper investigates the influence of one mechanically activated SiO2 component on the densities of green bodies as well as on the sintered samples, along with electrical properties of cordierite ceramics.",
publisher = "Belgrade : Materials Research Society of Serbia",
journal = "The Fifteenth Annual Conference YUCOMAT 2013: Programme and the Book of Abstracts",
title = "Influence of one activated component on the sintering process of three phase system",
pages = "103-103",
url = "https://hdl.handle.net/21.15107/rcub_vinar_7420"
}

Obradović, N., Peleš, A., Đorđević, N., Marković, S., Mitrić, M.,& Pavlović, V. B.. (2013). Influence of one activated component on the sintering process of three phase system. in The Fifteenth Annual Conference YUCOMAT 2013: Programme and the Book of Abstracts
Belgrade : Materials Research Society of Serbia., 103-103.
https://hdl.handle.net/21.15107/rcub_vinar_7420

Obradović N, Peleš A, Đorđević N, Marković S, Mitrić M, Pavlović VB. Influence of one activated component on the sintering process of three phase system. in The Fifteenth Annual Conference YUCOMAT 2013: Programme and the Book of Abstracts. 2013;:103-103.
https://hdl.handle.net/21.15107/rcub_vinar_7420 .

Obradović, Nina, Peleš, Adriana, Đorđević, N., Marković, Smilja, Mitrić, Miodrag, Pavlović, Vladimir B., "Influence of one activated component on the sintering process of three phase system" in The Fifteenth Annual Conference YUCOMAT 2013: Programme and the Book of Abstracts (2013):103-103,
https://hdl.handle.net/21.15107/rcub_vinar_7420 .

TY  - CONF
AU  - Živojinović, Jelena
AU  - Kosanović, Darko
AU  - Obradović, Nina
AU  - Peleš, Adriana
AU  - Labus, Nebojša
AU  - Filipović, Suzana
AU  - Pavlović, Vladimir B.
AU  - Mitrić, Miodrag
AU  - Ristić, Momčilo M.
PY  - 2013
UR  - http://dais.sanu.ac.rs/123456789/414
UR  - https://vinar.vin.bg.ac.rs/handle/123456789/7426
AB  - Strontium-titanate powder was mechanically activated in a planetary ball mill for 0, 5, 10, 30, 60, 90 and 120 minutes. Non-isothermal sintering of non-activated and activated SrTiO3 powder samples in the temperature interval from 50 to 1300 0C with three different heating rates (10, 15 and 20 0C/min) was investigated on a dilatometer. X-ray powder diffraction and scanning electron microscopy (SEM) were used to determine the phase composition, lattice microstrains and microstructure morphology of the samples. XRD results showed the presence of new phases: SrCO3 (strontuim-carbonate) and TiO2 (anatase) after 30 minutes of  mechanical activation.
PB  - Belgrade : Serbian Ceramic Society
C3  - Advanced Ceramics and Application : 2nd Serbian Ceramic Society Conference : program and the book of abstracts; September 30 - October 1, 2013; Belgrade
T1  - Dilatometric Analysis of Mechanically Activated SrTiO3 Powder
SP  - 38
EP  - 38
UR  - https://hdl.handle.net/21.15107/rcub_vinar_7426
ER  - 

@conference{
author = "Živojinović, Jelena and Kosanović, Darko and Obradović, Nina and Peleš, Adriana and Labus, Nebojša and Filipović, Suzana and Pavlović, Vladimir B. and Mitrić, Miodrag and Ristić, Momčilo M.",
year = "2013",
abstract = "Strontium-titanate powder was mechanically activated in a planetary ball mill for 0, 5, 10, 30, 60, 90 and 120 minutes. Non-isothermal sintering of non-activated and activated SrTiO3 powder samples in the temperature interval from 50 to 1300 0C with three different heating rates (10, 15 and 20 0C/min) was investigated on a dilatometer. X-ray powder diffraction and scanning electron microscopy (SEM) were used to determine the phase composition, lattice microstrains and microstructure morphology of the samples. XRD results showed the presence of new phases: SrCO3 (strontuim-carbonate) and TiO2 (anatase) after 30 minutes of  mechanical activation.",
publisher = "Belgrade : Serbian Ceramic Society",
journal = "Advanced Ceramics and Application : 2nd Serbian Ceramic Society Conference : program and the book of abstracts; September 30 - October 1, 2013; Belgrade",
title = "Dilatometric Analysis of Mechanically Activated SrTiO3 Powder",
pages = "38-38",
url = "https://hdl.handle.net/21.15107/rcub_vinar_7426"
}

Živojinović, J., Kosanović, D., Obradović, N., Peleš, A., Labus, N., Filipović, S., Pavlović, V. B., Mitrić, M.,& Ristić, M. M.. (2013). Dilatometric Analysis of Mechanically Activated SrTiO3 Powder. in Advanced Ceramics and Application : 2nd Serbian Ceramic Society Conference : program and the book of abstracts; September 30 - October 1, 2013; Belgrade
Belgrade : Serbian Ceramic Society., 38-38.
https://hdl.handle.net/21.15107/rcub_vinar_7426

Živojinović J, Kosanović D, Obradović N, Peleš A, Labus N, Filipović S, Pavlović VB, Mitrić M, Ristić MM. Dilatometric Analysis of Mechanically Activated SrTiO3 Powder. in Advanced Ceramics and Application : 2nd Serbian Ceramic Society Conference : program and the book of abstracts; September 30 - October 1, 2013; Belgrade. 2013;:38-38.
https://hdl.handle.net/21.15107/rcub_vinar_7426 .

Živojinović, Jelena, Kosanović, Darko, Obradović, Nina, Peleš, Adriana, Labus, Nebojša, Filipović, Suzana, Pavlović, Vladimir B., Mitrić, Miodrag, Ristić, Momčilo M., "Dilatometric Analysis of Mechanically Activated SrTiO3 Powder" in Advanced Ceramics and Application : 2nd Serbian Ceramic Society Conference : program and the book of abstracts; September 30 - October 1, 2013; Belgrade (2013):38-38,
https://hdl.handle.net/21.15107/rcub_vinar_7426 .

TY  - CONF
AU  - Obradović, Nina
AU  - Đorđević, Nataša
AU  - Labus, Nebojša
AU  - Peleš, Adriana
AU  - Mitrić, Miodrag
AU  - Pavlović, Vladimir B.
PY  - 2013
UR  - http://dais.sanu.ac.rs/123456789/416
UR  - https://vinar.vin.bg.ac.rs/handle/123456789/7427
AB  - Mechanical activation is widely used and relatively inexpensive procedure for sintering process sample preparation. However, the influence of pressure, which is used for compaction, has not been completely investigated. Cordierite, 2MgO⋅2Al2O3⋅5SiO2, is a very actual hightemperature ceramic material, due to its characteristics. Based on our previous investigation, the mechanical activation of the starting mixtures with 5.00 mass% TiO2 was performed in a high energy ball mill during 10 minutes. Compaction pressure varied from 0.5 to 6t/cm2 (49 MPa - 588 MPa). Sintering process was performed at 1350oC for 4h in air atmosphere. The phase composition of activated and sintered samples was analyzed by the X-ray diffraction method. Scanning electron microscopy was performed to analyze the microstructure of both compacted and sintered sample. Non-isothermal sintering up to 1400oC, with a constant heating rate, was investigated by thermal shrinkage change with dilatometer. In this paper we research green bodies and sintered samples compaction pressure influence electrical properties.
PB  - Belgrade : Serbian Ceramic Society
C3  - Advanced Ceramics and Application : 2nd Serbian Ceramic Society Conference : program and the book of abstracts; September 30 - October 1, 2013; Belgrade
T1  - Density and electrical properties of cordierite based ceramics as function of compaction pressure
SP  - 39
EP  - 39
UR  - https://hdl.handle.net/21.15107/rcub_vinar_7427
ER  - 

@conference{
author = "Obradović, Nina and Đorđević, Nataša and Labus, Nebojša and Peleš, Adriana and Mitrić, Miodrag and Pavlović, Vladimir B.",
year = "2013",
abstract = "Mechanical activation is widely used and relatively inexpensive procedure for sintering process sample preparation. However, the influence of pressure, which is used for compaction, has not been completely investigated. Cordierite, 2MgO⋅2Al2O3⋅5SiO2, is a very actual hightemperature ceramic material, due to its characteristics. Based on our previous investigation, the mechanical activation of the starting mixtures with 5.00 mass% TiO2 was performed in a high energy ball mill during 10 minutes. Compaction pressure varied from 0.5 to 6t/cm2 (49 MPa - 588 MPa). Sintering process was performed at 1350oC for 4h in air atmosphere. The phase composition of activated and sintered samples was analyzed by the X-ray diffraction method. Scanning electron microscopy was performed to analyze the microstructure of both compacted and sintered sample. Non-isothermal sintering up to 1400oC, with a constant heating rate, was investigated by thermal shrinkage change with dilatometer. In this paper we research green bodies and sintered samples compaction pressure influence electrical properties.",
publisher = "Belgrade : Serbian Ceramic Society",
journal = "Advanced Ceramics and Application : 2nd Serbian Ceramic Society Conference : program and the book of abstracts; September 30 - October 1, 2013; Belgrade",
title = "Density and electrical properties of cordierite based ceramics as function of compaction pressure",
pages = "39-39",
url = "https://hdl.handle.net/21.15107/rcub_vinar_7427"
}

Obradović, N., Đorđević, N., Labus, N., Peleš, A., Mitrić, M.,& Pavlović, V. B.. (2013). Density and electrical properties of cordierite based ceramics as function of compaction pressure. in Advanced Ceramics and Application : 2nd Serbian Ceramic Society Conference : program and the book of abstracts; September 30 - October 1, 2013; Belgrade
Belgrade : Serbian Ceramic Society., 39-39.
https://hdl.handle.net/21.15107/rcub_vinar_7427

Obradović N, Đorđević N, Labus N, Peleš A, Mitrić M, Pavlović VB. Density and electrical properties of cordierite based ceramics as function of compaction pressure. in Advanced Ceramics and Application : 2nd Serbian Ceramic Society Conference : program and the book of abstracts; September 30 - October 1, 2013; Belgrade. 2013;:39-39.
https://hdl.handle.net/21.15107/rcub_vinar_7427 .

Obradović, Nina, Đorđević, Nataša, Labus, Nebojša, Peleš, Adriana, Mitrić, Miodrag, Pavlović, Vladimir B., "Density and electrical properties of cordierite based ceramics as function of compaction pressure" in Advanced Ceramics and Application : 2nd Serbian Ceramic Society Conference : program and the book of abstracts; September 30 - October 1, 2013; Belgrade (2013):39-39,
https://hdl.handle.net/21.15107/rcub_vinar_7427 .

TY  - CONF
AU  - Peleš, Adriana
AU  - Pavlović, Vera P.
AU  - Obradović, Nina
AU  - Živojinović, Jelena
AU  - Mitrić, Miodrag
AU  - Pavlović, Vladimir B.
PY  - 2013
UR  - http://dais.sanu.ac.rs/123456789/426
UR  - https://vinar.vin.bg.ac.rs/handle/123456789/7433
AB  - Materials based on ZnO structure have more frequently application as fillers in polymer ceramics nanocompozites. Performances of these materials depends on fillers morphology, surfaces texture and particles size. According to this, in this paper, the authors investigated the influence of mechanical activation of ZnO powder on crystal and micro structure. Commercially available ZnO powder was activated in a planetary ball mill for 2, 5, 10 and 30 minutes. Characterization of such obtained powders was performed using XRD, SEM and Raman spectroscopy. XRD patterns indicated at lowering of peak intensities along with its broadening wich is realted to partical fragmentation and amorphyzation. Micrographs show irregularly shaped particles at the beginning and with prolonged milling time, particles gained uniformed distibution, while after 30 minutes of activation agglomerates started forming. The results we got by investigation of dynamical structure by Raman spectroscopy are in correlation with the other results of structures analysis. Results presented here enable further optimization of, polymer nanocompozite based on ZnO and PVDF, making process.
PB  - Belgrade : Serbian Ceramic Society
C3  - Advanced Ceramics and Application : 2nd Serbian Ceramic Society Conference : program and the book of abstracts; September 30 - October 1, 2013; Belgrade
T1  - Characterization of mechanically activated ZnO powder
SP  - 47
EP  - 47
UR  - https://hdl.handle.net/21.15107/rcub_vinar_7433
ER  - 

@conference{
author = "Peleš, Adriana and Pavlović, Vera P. and Obradović, Nina and Živojinović, Jelena and Mitrić, Miodrag and Pavlović, Vladimir B.",
year = "2013",
abstract = "Materials based on ZnO structure have more frequently application as fillers in polymer ceramics nanocompozites. Performances of these materials depends on fillers morphology, surfaces texture and particles size. According to this, in this paper, the authors investigated the influence of mechanical activation of ZnO powder on crystal and micro structure. Commercially available ZnO powder was activated in a planetary ball mill for 2, 5, 10 and 30 minutes. Characterization of such obtained powders was performed using XRD, SEM and Raman spectroscopy. XRD patterns indicated at lowering of peak intensities along with its broadening wich is realted to partical fragmentation and amorphyzation. Micrographs show irregularly shaped particles at the beginning and with prolonged milling time, particles gained uniformed distibution, while after 30 minutes of activation agglomerates started forming. The results we got by investigation of dynamical structure by Raman spectroscopy are in correlation with the other results of structures analysis. Results presented here enable further optimization of, polymer nanocompozite based on ZnO and PVDF, making process.",
publisher = "Belgrade : Serbian Ceramic Society",
journal = "Advanced Ceramics and Application : 2nd Serbian Ceramic Society Conference : program and the book of abstracts; September 30 - October 1, 2013; Belgrade",
title = "Characterization of mechanically activated ZnO powder",
pages = "47-47",
url = "https://hdl.handle.net/21.15107/rcub_vinar_7433"
}

Peleš, A., Pavlović, V. P., Obradović, N., Živojinović, J., Mitrić, M.,& Pavlović, V. B.. (2013). Characterization of mechanically activated ZnO powder. in Advanced Ceramics and Application : 2nd Serbian Ceramic Society Conference : program and the book of abstracts; September 30 - October 1, 2013; Belgrade
Belgrade : Serbian Ceramic Society., 47-47.
https://hdl.handle.net/21.15107/rcub_vinar_7433

Peleš A, Pavlović VP, Obradović N, Živojinović J, Mitrić M, Pavlović VB. Characterization of mechanically activated ZnO powder. in Advanced Ceramics and Application : 2nd Serbian Ceramic Society Conference : program and the book of abstracts; September 30 - October 1, 2013; Belgrade. 2013;:47-47.
https://hdl.handle.net/21.15107/rcub_vinar_7433 .

Peleš, Adriana, Pavlović, Vera P., Obradović, Nina, Živojinović, Jelena, Mitrić, Miodrag, Pavlović, Vladimir B., "Characterization of mechanically activated ZnO powder" in Advanced Ceramics and Application : 2nd Serbian Ceramic Society Conference : program and the book of abstracts; September 30 - October 1, 2013; Belgrade (2013):47-47,
https://hdl.handle.net/21.15107/rcub_vinar_7433 .

TY  - CONF
AU  - Peleš, Adriana
AU  - Filipović, Suzana
AU  - Pavlović, Vera P.
AU  - Mitrić, Miodrag
AU  - Obradović, Nina
AU  - Pavlović, Vladimir B.
PY  - 2013
UR  - http://dais.sanu.ac.rs/123456789/433
UR  - https://vinar.vin.bg.ac.rs/handle/123456789/7435
AB  - In this paper, the authors investigated the influence of mechanicall activation of ZnO powder on crystal and micro structure. Because of its structure, ZnO could be used like filler in polymer ceramics nanocompozites. Performances of these material depend on filler morphology, surfaces, texture and size particle. According to this, ZnO powder was activated in a planetary ball mill for 2, 5, 10 and 30 minutes. Changes in crystal and micro structure were observed by SEM, XRD, Raman spectroscopy and UV-Vis Reflection. SEM micrographs show increase of agglomerates size with prolonged milling time. XRD patterns indicate that the peak intensities getting lower and expand with activation time. UV-Vis reflection shows that there is a clear difference in the spectra with increasing activation time. The results we got by the investigation of dinamical structure by Raman spectroscopy are in corelation with the other results of structures analysis. Results presented here enable further optimisation of the polymer nanocompozite based on ZnO and PVDF making process.
PB  - Belgrade : Institute of Technical Sciences of SASA
C3  - Program and the Book of Abstracts / Twelfth Young Researchers' Conference Materials Sciences and Engineering December 11-13, 2013, Belgrade, Serbia
T1  - The influence of mechanical activation on the structure of ZnO
SP  - 11
EP  - 11
UR  - https://hdl.handle.net/21.15107/rcub_vinar_7435
ER  - 

@conference{
author = "Peleš, Adriana and Filipović, Suzana and Pavlović, Vera P. and Mitrić, Miodrag and Obradović, Nina and Pavlović, Vladimir B.",
year = "2013",
abstract = "In this paper, the authors investigated the influence of mechanicall activation of ZnO powder on crystal and micro structure. Because of its structure, ZnO could be used like filler in polymer ceramics nanocompozites. Performances of these material depend on filler morphology, surfaces, texture and size particle. According to this, ZnO powder was activated in a planetary ball mill for 2, 5, 10 and 30 minutes. Changes in crystal and micro structure were observed by SEM, XRD, Raman spectroscopy and UV-Vis Reflection. SEM micrographs show increase of agglomerates size with prolonged milling time. XRD patterns indicate that the peak intensities getting lower and expand with activation time. UV-Vis reflection shows that there is a clear difference in the spectra with increasing activation time. The results we got by the investigation of dinamical structure by Raman spectroscopy are in corelation with the other results of structures analysis. Results presented here enable further optimisation of the polymer nanocompozite based on ZnO and PVDF making process.",
publisher = "Belgrade : Institute of Technical Sciences of SASA",
journal = "Program and the Book of Abstracts / Twelfth Young Researchers' Conference Materials Sciences and Engineering December 11-13, 2013, Belgrade, Serbia",
title = "The influence of mechanical activation on the structure of ZnO",
pages = "11-11",
url = "https://hdl.handle.net/21.15107/rcub_vinar_7435"
}

Peleš, A., Filipović, S., Pavlović, V. P., Mitrić, M., Obradović, N.,& Pavlović, V. B.. (2013). The influence of mechanical activation on the structure of ZnO. in Program and the Book of Abstracts / Twelfth Young Researchers' Conference Materials Sciences and Engineering December 11-13, 2013, Belgrade, Serbia
Belgrade : Institute of Technical Sciences of SASA., 11-11.
https://hdl.handle.net/21.15107/rcub_vinar_7435

Peleš A, Filipović S, Pavlović VP, Mitrić M, Obradović N, Pavlović VB. The influence of mechanical activation on the structure of ZnO. in Program and the Book of Abstracts / Twelfth Young Researchers' Conference Materials Sciences and Engineering December 11-13, 2013, Belgrade, Serbia. 2013;:11-11.
https://hdl.handle.net/21.15107/rcub_vinar_7435 .

Peleš, Adriana, Filipović, Suzana, Pavlović, Vera P., Mitrić, Miodrag, Obradović, Nina, Pavlović, Vladimir B., "The influence of mechanical activation on the structure of ZnO" in Program and the Book of Abstracts / Twelfth Young Researchers' Conference Materials Sciences and Engineering December 11-13, 2013, Belgrade, Serbia (2013):11-11,
https://hdl.handle.net/21.15107/rcub_vinar_7435 .

TY  - CONF
AU  - Obradović, Nina
AU  - Đorđević, N.
AU  - Peleš, Adriana
AU  - Mitrić, Miodrag
AU  - Pavlović, Vladimir B.
PY  - 2012
UR  - http://dais.sanu.ac.rs/123456789/525
UR  - https://vinar.vin.bg.ac.rs/handle/123456789/7468
AB  - Mechanical activation is widely used for sample preparation before the sintering process. However, the influence of pressure, which is used for compaction, has not been completely investigated. Cordierite, 2MgO_2Al2O3_5SiO2, is a very attractive high-temperature ceramic material, due to its outstanding electrical characteristics, such as the low temperature expansion coefficient, low dielectric constant and good mechanical properties. Based on our previous investigation, the mechanical activation of the starting mixtures with 5.00 mass% TiO2 was performed in a high energy ball mill during 10 minutes. Compaction pressure varied from 0.5 to 6 t/cm2. Differential thermal analysis (DTA) was used in order to determine characteristic temperatures within the system during heating. Sintering process was performed at 1350 °C for 4 h in air atmosphere. The phase composition of activated and sintered samples was analyzed by the X-ray diffraction method. Scanning electron microscopy was performed to analyze both compacted and sintered sample microstructure. This paper deals with the influence of compaction pressure on the densities of green bodies as well as on the sintered samples, along with electrical properties
PB  - Belgrade : Materials Research Society of Serbia; Institute of Technical Sciences of SASA; Vinča Institute of Nuclear Sciences, University of Belgrade
C3  - Joint Event of the 11th Young Researchers’ Conference: Materials Science and Engineering and the 1st European Early Stage Researches’ Conference on Hydrogen Storage: Program and the Book of Abstracts
T1  - Compaction pressure's influence on density and electrical properties of sintered cordierite-based ceramics
SP  - 61
EP  - 61
UR  - https://hdl.handle.net/21.15107/rcub_vinar_7468
ER  - 

@conference{
author = "Obradović, Nina and Đorđević, N. and Peleš, Adriana and Mitrić, Miodrag and Pavlović, Vladimir B.",
year = "2012",
abstract = "Mechanical activation is widely used for sample preparation before the sintering process. However, the influence of pressure, which is used for compaction, has not been completely investigated. Cordierite, 2MgO_2Al2O3_5SiO2, is a very attractive high-temperature ceramic material, due to its outstanding electrical characteristics, such as the low temperature expansion coefficient, low dielectric constant and good mechanical properties. Based on our previous investigation, the mechanical activation of the starting mixtures with 5.00 mass% TiO2 was performed in a high energy ball mill during 10 minutes. Compaction pressure varied from 0.5 to 6 t/cm2. Differential thermal analysis (DTA) was used in order to determine characteristic temperatures within the system during heating. Sintering process was performed at 1350 °C for 4 h in air atmosphere. The phase composition of activated and sintered samples was analyzed by the X-ray diffraction method. Scanning electron microscopy was performed to analyze both compacted and sintered sample microstructure. This paper deals with the influence of compaction pressure on the densities of green bodies as well as on the sintered samples, along with electrical properties",
publisher = "Belgrade : Materials Research Society of Serbia; Institute of Technical Sciences of SASA; Vinča Institute of Nuclear Sciences, University of Belgrade",
journal = "Joint Event of the 11th Young Researchers’ Conference: Materials Science and Engineering and the 1st European Early Stage Researches’ Conference on Hydrogen Storage: Program and the Book of Abstracts",
title = "Compaction pressure's influence on density and electrical properties of sintered cordierite-based ceramics",
pages = "61-61",
url = "https://hdl.handle.net/21.15107/rcub_vinar_7468"
}

Obradović, N., Đorđević, N., Peleš, A., Mitrić, M.,& Pavlović, V. B.. (2012). Compaction pressure's influence on density and electrical properties of sintered cordierite-based ceramics. in Joint Event of the 11th Young Researchers’ Conference: Materials Science and Engineering and the 1st European Early Stage Researches’ Conference on Hydrogen Storage: Program and the Book of Abstracts
Belgrade : Materials Research Society of Serbia; Institute of Technical Sciences of SASA; Vinča Institute of Nuclear Sciences, University of Belgrade., 61-61.
https://hdl.handle.net/21.15107/rcub_vinar_7468

Obradović N, Đorđević N, Peleš A, Mitrić M, Pavlović VB. Compaction pressure's influence on density and electrical properties of sintered cordierite-based ceramics. in Joint Event of the 11th Young Researchers’ Conference: Materials Science and Engineering and the 1st European Early Stage Researches’ Conference on Hydrogen Storage: Program and the Book of Abstracts. 2012;:61-61.
https://hdl.handle.net/21.15107/rcub_vinar_7468 .

Obradović, Nina, Đorđević, N., Peleš, Adriana, Mitrić, Miodrag, Pavlović, Vladimir B., "Compaction pressure's influence on density and electrical properties of sintered cordierite-based ceramics" in Joint Event of the 11th Young Researchers’ Conference: Materials Science and Engineering and the 1st European Early Stage Researches’ Conference on Hydrogen Storage: Program and the Book of Abstracts (2012):61-61,
https://hdl.handle.net/21.15107/rcub_vinar_7468 .