Bračko, Ines

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  • Bračko, Ines (9)
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Author's Bibliography

Hydrothermal synthesis of ZnO powders with a tailored particle morphology and improved optical characteristics

Stanković, Ana; Stojanović, Zoran S.; Veselinović, Ljiljana M.; Bračko, Ines; Škapin, Srečo Davor; Marković, Smilja; Uskoković, Dragan

(Belgrade : Materials Research Society of Serbia, 2012)

TY  - CONF
AU  - Stanković, Ana
AU  - Stojanović, Zoran S.
AU  - Veselinović, Ljiljana M.
AU  - Bračko, Ines
AU  - Škapin, Srečo Davor
AU  - Marković, Smilja
AU  - Uskoković, Dragan
PY  - 2012
UR  - http://dais.sanu.ac.rs/123456789/435
UR  - https://vinar.vin.bg.ac.rs/handle/123456789/7437
AB  - ZnO represent one of the most important multifunctional materials. Its properties are well known and confirmed in different application areas such as: gas sensors, UV lasers, solar cells, electroluminescent and optoelectronic devices, piezoelectric transducers, hydrogen-storages, rubber industry and plastic processing, cosmetics and pharmacy, and it is also used as an antibacterial agent. In this work, we propose a low-temperature hydrothermal method for the synthesis of phase-pure ZnO powders with a controlled morphology and narrow particle size distribution. This simple and low-cost method allows tailoring of the shape and size of ZnO particles, from micro-rods via hexagonal prism-like to nano-spheres, by choosing the appropriate pH of the reaction solution, tuned by the varying of [Na+]:[Zn2+] molar ratio. The agglomeration of the powders was prevented with the assistance of PVP as a capping agent. The synthesized powders were characterized by XRD, TEM, SEAD and HRTEM methods to examine the phase purity and crystallinity. FE-SEM measurements were used for the morphology characterization, while the results of Raman and UV-Vis DRS measurements were used for the study of optical properties. The relationship between the particle size and morphology and the optical properties is discussed. Diffuse reflectance spectra of ZnO powders with different size and morphology revealed characteristic R curves with the absorption edge near 380 nm, but with obvious difference in the absorption in the visible region. The micro-sized powder ZnO8 revealed the lowest reflectance (∼70%), compared to submicro- (∼80%) and nano-sized (ZnO12 and ZnO13, ∼90%) powders. Thus, the reflectance of the ZnO powders decreases with the increase in the average particle size.
PB  - Belgrade : Materials Research Society of Serbia
C3  - The Fourteenth Annual Conference YUCOMAT 2012: Programme and the Book of Abstracts
T1  - Hydrothermal synthesis of ZnO powders with a tailored particle morphology and improved optical characteristics
SP  - 47
EP  - 47
UR  - https://hdl.handle.net/21.15107/rcub_vinar_7437
ER  - 
@conference{
author = "Stanković, Ana and Stojanović, Zoran S. and Veselinović, Ljiljana M. and Bračko, Ines and Škapin, Srečo Davor and Marković, Smilja and Uskoković, Dragan",
year = "2012",
abstract = "ZnO represent one of the most important multifunctional materials. Its properties are well known and confirmed in different application areas such as: gas sensors, UV lasers, solar cells, electroluminescent and optoelectronic devices, piezoelectric transducers, hydrogen-storages, rubber industry and plastic processing, cosmetics and pharmacy, and it is also used as an antibacterial agent. In this work, we propose a low-temperature hydrothermal method for the synthesis of phase-pure ZnO powders with a controlled morphology and narrow particle size distribution. This simple and low-cost method allows tailoring of the shape and size of ZnO particles, from micro-rods via hexagonal prism-like to nano-spheres, by choosing the appropriate pH of the reaction solution, tuned by the varying of [Na+]:[Zn2+] molar ratio. The agglomeration of the powders was prevented with the assistance of PVP as a capping agent. The synthesized powders were characterized by XRD, TEM, SEAD and HRTEM methods to examine the phase purity and crystallinity. FE-SEM measurements were used for the morphology characterization, while the results of Raman and UV-Vis DRS measurements were used for the study of optical properties. The relationship between the particle size and morphology and the optical properties is discussed. Diffuse reflectance spectra of ZnO powders with different size and morphology revealed characteristic R curves with the absorption edge near 380 nm, but with obvious difference in the absorption in the visible region. The micro-sized powder ZnO8 revealed the lowest reflectance (∼70%), compared to submicro- (∼80%) and nano-sized (ZnO12 and ZnO13, ∼90%) powders. Thus, the reflectance of the ZnO powders decreases with the increase in the average particle size.",
publisher = "Belgrade : Materials Research Society of Serbia",
journal = "The Fourteenth Annual Conference YUCOMAT 2012: Programme and the Book of Abstracts",
title = "Hydrothermal synthesis of ZnO powders with a tailored particle morphology and improved optical characteristics",
pages = "47-47",
url = "https://hdl.handle.net/21.15107/rcub_vinar_7437"
}
Stanković, A., Stojanović, Z. S., Veselinović, L. M., Bračko, I., Škapin, S. D., Marković, S.,& Uskoković, D.. (2012). Hydrothermal synthesis of ZnO powders with a tailored particle morphology and improved optical characteristics. in The Fourteenth Annual Conference YUCOMAT 2012: Programme and the Book of Abstracts
Belgrade : Materials Research Society of Serbia., 47-47.
https://hdl.handle.net/21.15107/rcub_vinar_7437
Stanković A, Stojanović ZS, Veselinović LM, Bračko I, Škapin SD, Marković S, Uskoković D. Hydrothermal synthesis of ZnO powders with a tailored particle morphology and improved optical characteristics. in The Fourteenth Annual Conference YUCOMAT 2012: Programme and the Book of Abstracts. 2012;:47-47.
https://hdl.handle.net/21.15107/rcub_vinar_7437 .
Stanković, Ana, Stojanović, Zoran S., Veselinović, Ljiljana M., Bračko, Ines, Škapin, Srečo Davor, Marković, Smilja, Uskoković, Dragan, "Hydrothermal synthesis of ZnO powders with a tailored particle morphology and improved optical characteristics" in The Fourteenth Annual Conference YUCOMAT 2012: Programme and the Book of Abstracts (2012):47-47,
https://hdl.handle.net/21.15107/rcub_vinar_7437 .

Peculiarities in sintering behavior of Ca-deficient hydroxyapatite nanopowders

Lukić, Miodrag; Veselinović, Ljiljana M.; Stojanović, Zoran S.; Maček Kržmanc, Marjeta; Bračko, Ines; Škapin, Srečo Davor; Marković, Smilja; Uskoković, Dragan

(Elsevier, 2012)

TY  - JOUR
AU  - Lukić, Miodrag
AU  - Veselinović, Ljiljana M.
AU  - Stojanović, Zoran S.
AU  - Maček Kržmanc, Marjeta
AU  - Bračko, Ines
AU  - Škapin, Srečo Davor
AU  - Marković, Smilja
AU  - Uskoković, Dragan
PY  - 2012
UR  - http://dais.sanu.ac.rs/123456789/476
UR  - https://vinar.vin.bg.ac.rs/handle/123456789/7447
AB  - We report unusual sintering behavior of Ca-deficient hydroxyapatite processed with different heating rates; particularly, faster heating resulted in higher densification. We hypothesize that faster heating delays formation of β-tricalcium phosphate which yields to unobstructed densification in intermediate sintering stage, allowing further tailoring of both microstructure and phase composition (hydroxyapatite/tricalcium phosphate).
PB  - Elsevier
T2  - Materials Letters
T1  - Peculiarities in sintering behavior of Ca-deficient hydroxyapatite nanopowders
SP  - 331
EP  - 335
DO  - 10.1016/j.matlet.2011.10.085
ER  - 
@article{
author = "Lukić, Miodrag and Veselinović, Ljiljana M. and Stojanović, Zoran S. and Maček Kržmanc, Marjeta and Bračko, Ines and Škapin, Srečo Davor and Marković, Smilja and Uskoković, Dragan",
year = "2012",
abstract = "We report unusual sintering behavior of Ca-deficient hydroxyapatite processed with different heating rates; particularly, faster heating resulted in higher densification. We hypothesize that faster heating delays formation of β-tricalcium phosphate which yields to unobstructed densification in intermediate sintering stage, allowing further tailoring of both microstructure and phase composition (hydroxyapatite/tricalcium phosphate).",
publisher = "Elsevier",
journal = "Materials Letters",
title = "Peculiarities in sintering behavior of Ca-deficient hydroxyapatite nanopowders",
pages = "331-335",
doi = "10.1016/j.matlet.2011.10.085"
}
Lukić, M., Veselinović, L. M., Stojanović, Z. S., Maček Kržmanc, M., Bračko, I., Škapin, S. D., Marković, S.,& Uskoković, D.. (2012). Peculiarities in sintering behavior of Ca-deficient hydroxyapatite nanopowders. in Materials Letters
Elsevier., 331-335.
https://doi.org/10.1016/j.matlet.2011.10.085
Lukić M, Veselinović LM, Stojanović ZS, Maček Kržmanc M, Bračko I, Škapin SD, Marković S, Uskoković D. Peculiarities in sintering behavior of Ca-deficient hydroxyapatite nanopowders. in Materials Letters. 2012;:331-335.
doi:10.1016/j.matlet.2011.10.085 .
Lukić, Miodrag, Veselinović, Ljiljana M., Stojanović, Zoran S., Maček Kržmanc, Marjeta, Bračko, Ines, Škapin, Srečo Davor, Marković, Smilja, Uskoković, Dragan, "Peculiarities in sintering behavior of Ca-deficient hydroxyapatite nanopowders" in Materials Letters (2012):331-335,
https://doi.org/10.1016/j.matlet.2011.10.085 . .
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ZnO micro and nanocrystals with enhanced visible light absorption

Stanković, Ana; Stojanović, Zoran S.; Veselinović, Ljiljana M.; Škapin, Srečo Davor; Bračko, Ines; Marković, Smilja; Uskoković, Dragan

(Elsevier, 2012)

TY  - JOUR
AU  - Stanković, Ana
AU  - Stojanović, Zoran S.
AU  - Veselinović, Ljiljana M.
AU  - Škapin, Srečo Davor
AU  - Bračko, Ines
AU  - Marković, Smilja
AU  - Uskoković, Dragan
PY  - 2012
UR  - http://dais.sanu.ac.rs/123456789/486
UR  - https://vinar.vin.bg.ac.rs/handle/123456789/7450
AB  - In this paper, we investigate the effect of the particle size and morphology on the optical properties of ZnO. A series of ZnO micro and nanocrystals were synthesized by the hydrothermal processing of zinc acetate dihydrate and sodium hydroxide as the starting materials, and polyvinylpyrrolidone (PVP) as the polymer surfactant. The particle size and morphology were tailored by adjusting the reactant molar ratios [Zn2+]/[OH−], while the reaction temperature and the time remained unchanged. X-ray diffraction (XRD), transmission electron microscopy (TEM), selected area electron diffraction (SAED) and high-resolution TEM (HRTEM) have shown that the micro and nanocrystals have a high crystalline pure wurtzite-type hexagonal structure with nanosized crystallites. The size and morphology of the ZnO micro and nanocrystals were investigated by field emission scanning electron microscopy (FE-SEM), which showed a modification from micro-rods via hexagonal-faceted prismatic morphology to nanospheres, caused by simple adjustment of the reactant molar ratio [Zn2+]/[OH−] from 1:1 to 1:5. The optical properties of the ZnO micro and nanocrystals, as well as their dependence on the particle size and morphology were investigated by Raman and ultraviolet–visible (UV–vis) diffuse reflectance spectroscopy (DRS). The UV–vis spectra showed that the modification of the particle size and morphology from nanospheres to micro-rods resulted in increased absorption, and a slight red-shift of the absorption edge (0.06 eV). Besides, the band gap energy of the synthesized ZnO micro and nanocrystals showed the red shift (∼0.20 eV) compared to bulk ZnO. According to the results of a Raman spectroscopy, the enhanced visible light absorption of the ZnO micro and nanocrystals is related to two phenomena: (1) the existence of lattice defects (oxygen vacancies and zinc interstitials), and (2) the particle surface sensitization by PVP.
PB  - Elsevier
T2  - Materials Science and Engineering: B
T1  - ZnO micro and nanocrystals with enhanced visible light absorption
SP  - 1038
EP  - 1045
DO  - 10.1016/j.mseb.2012.05.013
ER  - 
@article{
author = "Stanković, Ana and Stojanović, Zoran S. and Veselinović, Ljiljana M. and Škapin, Srečo Davor and Bračko, Ines and Marković, Smilja and Uskoković, Dragan",
year = "2012",
abstract = "In this paper, we investigate the effect of the particle size and morphology on the optical properties of ZnO. A series of ZnO micro and nanocrystals were synthesized by the hydrothermal processing of zinc acetate dihydrate and sodium hydroxide as the starting materials, and polyvinylpyrrolidone (PVP) as the polymer surfactant. The particle size and morphology were tailored by adjusting the reactant molar ratios [Zn2+]/[OH−], while the reaction temperature and the time remained unchanged. X-ray diffraction (XRD), transmission electron microscopy (TEM), selected area electron diffraction (SAED) and high-resolution TEM (HRTEM) have shown that the micro and nanocrystals have a high crystalline pure wurtzite-type hexagonal structure with nanosized crystallites. The size and morphology of the ZnO micro and nanocrystals were investigated by field emission scanning electron microscopy (FE-SEM), which showed a modification from micro-rods via hexagonal-faceted prismatic morphology to nanospheres, caused by simple adjustment of the reactant molar ratio [Zn2+]/[OH−] from 1:1 to 1:5. The optical properties of the ZnO micro and nanocrystals, as well as their dependence on the particle size and morphology were investigated by Raman and ultraviolet–visible (UV–vis) diffuse reflectance spectroscopy (DRS). The UV–vis spectra showed that the modification of the particle size and morphology from nanospheres to micro-rods resulted in increased absorption, and a slight red-shift of the absorption edge (0.06 eV). Besides, the band gap energy of the synthesized ZnO micro and nanocrystals showed the red shift (∼0.20 eV) compared to bulk ZnO. According to the results of a Raman spectroscopy, the enhanced visible light absorption of the ZnO micro and nanocrystals is related to two phenomena: (1) the existence of lattice defects (oxygen vacancies and zinc interstitials), and (2) the particle surface sensitization by PVP.",
publisher = "Elsevier",
journal = "Materials Science and Engineering: B",
title = "ZnO micro and nanocrystals with enhanced visible light absorption",
pages = "1038-1045",
doi = "10.1016/j.mseb.2012.05.013"
}
Stanković, A., Stojanović, Z. S., Veselinović, L. M., Škapin, S. D., Bračko, I., Marković, S.,& Uskoković, D.. (2012). ZnO micro and nanocrystals with enhanced visible light absorption. in Materials Science and Engineering: B
Elsevier., 1038-1045.
https://doi.org/10.1016/j.mseb.2012.05.013
Stanković A, Stojanović ZS, Veselinović LM, Škapin SD, Bračko I, Marković S, Uskoković D. ZnO micro and nanocrystals with enhanced visible light absorption. in Materials Science and Engineering: B. 2012;:1038-1045.
doi:10.1016/j.mseb.2012.05.013 .
Stanković, Ana, Stojanović, Zoran S., Veselinović, Ljiljana M., Škapin, Srečo Davor, Bračko, Ines, Marković, Smilja, Uskoković, Dragan, "ZnO micro and nanocrystals with enhanced visible light absorption" in Materials Science and Engineering: B (2012):1038-1045,
https://doi.org/10.1016/j.mseb.2012.05.013 . .
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Hydrothermal synthesis of ZnO powders with a tailored particle morphology and improved optical characteristics

Stanković, Ana; Stojanović, Zoran S.; Veselinović, Ljiljana M.; Bračko, Ines; Škapin, Srečo Davor; Marković, Smilja; Uskoković, Dragan

(2012)

TY  - CONF
AU  - Stanković, Ana
AU  - Stojanović, Zoran S.
AU  - Veselinović, Ljiljana M.
AU  - Bračko, Ines
AU  - Škapin, Srečo Davor
AU  - Marković, Smilja
AU  - Uskoković, Dragan
PY  - 2012
UR  - http://dais.sanu.ac.rs/123456789/145
UR  - https://vinar.vin.bg.ac.rs/handle/123456789/7351
AB  - Poster presented at the 14th Annual Conference of the Materials Research Society of Serbia - YUCOMAT 2012, Herceg Novi, Montenegro, September 3–7, 2012
T1  - Hydrothermal synthesis of ZnO powders with a tailored particle morphology and improved optical characteristics
UR  - https://hdl.handle.net/21.15107/rcub_vinar_7351
ER  - 
@conference{
author = "Stanković, Ana and Stojanović, Zoran S. and Veselinović, Ljiljana M. and Bračko, Ines and Škapin, Srečo Davor and Marković, Smilja and Uskoković, Dragan",
year = "2012",
abstract = "Poster presented at the 14th Annual Conference of the Materials Research Society of Serbia - YUCOMAT 2012, Herceg Novi, Montenegro, September 3–7, 2012",
title = "Hydrothermal synthesis of ZnO powders with a tailored particle morphology and improved optical characteristics",
url = "https://hdl.handle.net/21.15107/rcub_vinar_7351"
}
Stanković, A., Stojanović, Z. S., Veselinović, L. M., Bračko, I., Škapin, S. D., Marković, S.,& Uskoković, D.. (2012). Hydrothermal synthesis of ZnO powders with a tailored particle morphology and improved optical characteristics. .
https://hdl.handle.net/21.15107/rcub_vinar_7351
Stanković A, Stojanović ZS, Veselinović LM, Bračko I, Škapin SD, Marković S, Uskoković D. Hydrothermal synthesis of ZnO powders with a tailored particle morphology and improved optical characteristics. 2012;.
https://hdl.handle.net/21.15107/rcub_vinar_7351 .
Stanković, Ana, Stojanović, Zoran S., Veselinović, Ljiljana M., Bračko, Ines, Škapin, Srečo Davor, Marković, Smilja, Uskoković, Dragan, "Hydrothermal synthesis of ZnO powders with a tailored particle morphology and improved optical characteristics" (2012),
https://hdl.handle.net/21.15107/rcub_vinar_7351 .

Synthesis and characterization of selenium nanoparticles in the presence of bovine serum albumin or poly (L-glutamic acid) for biomedical application

Filipović, Nenad; Stevanović, Magdalena; Škapin, Srečo Davor; Bračko, Ines; Uskoković, Dragan

(Belgrade : Materials Research Society of Serbia; Institute of Technical Sciences of SASA; Vinča Institute of Nuclear Sciences, University of Belgrade, 2012)

TY  - CONF
AU  - Filipović, Nenad
AU  - Stevanović, Magdalena
AU  - Škapin, Srečo Davor
AU  - Bračko, Ines
AU  - Uskoković, Dragan
PY  - 2012
UR  - http://dais.sanu.ac.rs/123456789/502
UR  - https://vinar.vin.bg.ac.rs/handle/123456789/7458
AB  - It is well known that selenium is an essential trace element playing the important roles in mammalian biology. For years, its organic forms and some salts have been used in studying its biological effects, but recently, selenium nanoparticles have gained great attention as a possible material for cancer therapy and prevention. In this study we report the facile and reproducible method for synthesis the nanoselenium by reduction of sodium selenite with an ascorbic acid, in the presence of a two stabilizing agents, bovine serum albumin (BSA) or poly (L-glutamic acid) (PGA). The influence of the sodium selenite/ascorbic acid ratio as well as the types and concentration of two different stabilizers on the wide variety physicochemical characteristics of obtained particles were examined.
PB  - Belgrade : Materials Research Society of Serbia; Institute of Technical Sciences of SASA; Vinča Institute of Nuclear Sciences, University of Belgrade
C3  - Joint Event of the 11th Young Researchers’ Conference: Materials Science and Engineering and the 1st European Early Stage Researches’ Conference on Hydrogen Storage: Program and the Book of Abstracts
T1  - Synthesis and characterization of selenium nanoparticles in the presence of bovine serum albumin or poly (L-glutamic acid) for biomedical application
SP  - 105
EP  - 105
UR  - https://hdl.handle.net/21.15107/rcub_vinar_7458
ER  - 
@conference{
author = "Filipović, Nenad and Stevanović, Magdalena and Škapin, Srečo Davor and Bračko, Ines and Uskoković, Dragan",
year = "2012",
abstract = "It is well known that selenium is an essential trace element playing the important roles in mammalian biology. For years, its organic forms and some salts have been used in studying its biological effects, but recently, selenium nanoparticles have gained great attention as a possible material for cancer therapy and prevention. In this study we report the facile and reproducible method for synthesis the nanoselenium by reduction of sodium selenite with an ascorbic acid, in the presence of a two stabilizing agents, bovine serum albumin (BSA) or poly (L-glutamic acid) (PGA). The influence of the sodium selenite/ascorbic acid ratio as well as the types and concentration of two different stabilizers on the wide variety physicochemical characteristics of obtained particles were examined.",
publisher = "Belgrade : Materials Research Society of Serbia; Institute of Technical Sciences of SASA; Vinča Institute of Nuclear Sciences, University of Belgrade",
journal = "Joint Event of the 11th Young Researchers’ Conference: Materials Science and Engineering and the 1st European Early Stage Researches’ Conference on Hydrogen Storage: Program and the Book of Abstracts",
title = "Synthesis and characterization of selenium nanoparticles in the presence of bovine serum albumin or poly (L-glutamic acid) for biomedical application",
pages = "105-105",
url = "https://hdl.handle.net/21.15107/rcub_vinar_7458"
}
Filipović, N., Stevanović, M., Škapin, S. D., Bračko, I.,& Uskoković, D.. (2012). Synthesis and characterization of selenium nanoparticles in the presence of bovine serum albumin or poly (L-glutamic acid) for biomedical application. in Joint Event of the 11th Young Researchers’ Conference: Materials Science and Engineering and the 1st European Early Stage Researches’ Conference on Hydrogen Storage: Program and the Book of Abstracts
Belgrade : Materials Research Society of Serbia; Institute of Technical Sciences of SASA; Vinča Institute of Nuclear Sciences, University of Belgrade., 105-105.
https://hdl.handle.net/21.15107/rcub_vinar_7458
Filipović N, Stevanović M, Škapin SD, Bračko I, Uskoković D. Synthesis and characterization of selenium nanoparticles in the presence of bovine serum albumin or poly (L-glutamic acid) for biomedical application. in Joint Event of the 11th Young Researchers’ Conference: Materials Science and Engineering and the 1st European Early Stage Researches’ Conference on Hydrogen Storage: Program and the Book of Abstracts. 2012;:105-105.
https://hdl.handle.net/21.15107/rcub_vinar_7458 .
Filipović, Nenad, Stevanović, Magdalena, Škapin, Srečo Davor, Bračko, Ines, Uskoković, Dragan, "Synthesis and characterization of selenium nanoparticles in the presence of bovine serum albumin or poly (L-glutamic acid) for biomedical application" in Joint Event of the 11th Young Researchers’ Conference: Materials Science and Engineering and the 1st European Early Stage Researches’ Conference on Hydrogen Storage: Program and the Book of Abstracts (2012):105-105,
https://hdl.handle.net/21.15107/rcub_vinar_7458 .

Synthetical bone-like and biological hydroxyapatites: a comparative study of crystal structure and morphology

Marković, Smilja; Veselinović, Ljiljana M.; Lukić, Miodrag; Karanović, Ljiljana; Bračko, Ines; Ignjatović, Nenad L.; Uskoković, Dragan

(IOP Publishing, 2011)

TY  - JOUR
AU  - Marković, Smilja
AU  - Veselinović, Ljiljana M.
AU  - Lukić, Miodrag
AU  - Karanović, Ljiljana
AU  - Bračko, Ines
AU  - Ignjatović, Nenad L.
AU  - Uskoković, Dragan
PY  - 2011
UR  - http://dais.sanu.ac.rs/123456789/731
UR  - https://vinar.vin.bg.ac.rs/handle/123456789/7522
AB  - Phase composition, crystal structure and morphology of biological hydroxyapatite (BHAp) extracted from human mandible bone, and carbonated hydroxyapatite (CHAp), synthesized by the chemical precipitation method, were studied by x-ray powder diffraction (XRD), Fourier transform infrared (FTIR) and Raman (R) spectroscopy techniques, combined with transmission electron microscopy (TEM). Structural and microstructural parameters were determined through Rietveld refinement of recorded XRD data, performed using the FullProf computing program, and TEM. Microstructural analysis shows anisotropic extension along the [0 0 l] crystallographic direction (i.e. elongated crystallites shape) of both investigated samples. The average crystallite sizes of 10 and 8 nm were estimated for BHAp and CHAp, respectively. The FTIR and R spectroscopy studies show that carbonate ions substitute both phosphate and hydroxyl ions in the crystal structure of BHAp as well as in CHAp, indicating that both of them are mixed AB-type of CHAp. The thermal behaviour and carbonate content were analysed using thermogravimetric and differential thermal analysis. The carbonate content of about 1 wt.% and phase transition, at near 790 °C, from HAp to β-tricalcium phosphate were determined in both samples. The quality of synthesized CHAp powder, particularly, the particle size distribution and uniformity of morphology, was analysed by a particle size analyser based on laser diffraction and field emission scanning electron microscopy, respectively. These data were used to discuss similarity between natural and synthetic CHAp. Good correlation between the unit cell parameters, average crystallite size, morphology, carbonate content and crystallographic positions of carbonate ions in natural and synthetic HAp samples was found.
PB  - IOP Publishing
T2  - Biomedical Materials
T1  - Synthetical bone-like and biological hydroxyapatites: a comparative study of crystal structure and morphology
EP  - Art. No. 045005
DO  - 10.1088/1748-6041/6/4/045005
ER  - 
@article{
author = "Marković, Smilja and Veselinović, Ljiljana M. and Lukić, Miodrag and Karanović, Ljiljana and Bračko, Ines and Ignjatović, Nenad L. and Uskoković, Dragan",
year = "2011",
abstract = "Phase composition, crystal structure and morphology of biological hydroxyapatite (BHAp) extracted from human mandible bone, and carbonated hydroxyapatite (CHAp), synthesized by the chemical precipitation method, were studied by x-ray powder diffraction (XRD), Fourier transform infrared (FTIR) and Raman (R) spectroscopy techniques, combined with transmission electron microscopy (TEM). Structural and microstructural parameters were determined through Rietveld refinement of recorded XRD data, performed using the FullProf computing program, and TEM. Microstructural analysis shows anisotropic extension along the [0 0 l] crystallographic direction (i.e. elongated crystallites shape) of both investigated samples. The average crystallite sizes of 10 and 8 nm were estimated for BHAp and CHAp, respectively. The FTIR and R spectroscopy studies show that carbonate ions substitute both phosphate and hydroxyl ions in the crystal structure of BHAp as well as in CHAp, indicating that both of them are mixed AB-type of CHAp. The thermal behaviour and carbonate content were analysed using thermogravimetric and differential thermal analysis. The carbonate content of about 1 wt.% and phase transition, at near 790 °C, from HAp to β-tricalcium phosphate were determined in both samples. The quality of synthesized CHAp powder, particularly, the particle size distribution and uniformity of morphology, was analysed by a particle size analyser based on laser diffraction and field emission scanning electron microscopy, respectively. These data were used to discuss similarity between natural and synthetic CHAp. Good correlation between the unit cell parameters, average crystallite size, morphology, carbonate content and crystallographic positions of carbonate ions in natural and synthetic HAp samples was found.",
publisher = "IOP Publishing",
journal = "Biomedical Materials",
title = "Synthetical bone-like and biological hydroxyapatites: a comparative study of crystal structure and morphology",
pages = "Art. No. 045005",
doi = "10.1088/1748-6041/6/4/045005"
}
Marković, S., Veselinović, L. M., Lukić, M., Karanović, L., Bračko, I., Ignjatović, N. L.,& Uskoković, D.. (2011). Synthetical bone-like and biological hydroxyapatites: a comparative study of crystal structure and morphology. in Biomedical Materials
IOP Publishing..
https://doi.org/10.1088/1748-6041/6/4/045005
Marković S, Veselinović LM, Lukić M, Karanović L, Bračko I, Ignjatović NL, Uskoković D. Synthetical bone-like and biological hydroxyapatites: a comparative study of crystal structure and morphology. in Biomedical Materials. 2011;:null-Art. No. 045005.
doi:10.1088/1748-6041/6/4/045005 .
Marković, Smilja, Veselinović, Ljiljana M., Lukić, Miodrag, Karanović, Ljiljana, Bračko, Ines, Ignjatović, Nenad L., Uskoković, Dragan, "Synthetical bone-like and biological hydroxyapatites: a comparative study of crystal structure and morphology" in Biomedical Materials (2011),
https://doi.org/10.1088/1748-6041/6/4/045005 . .
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Full density calcium phosphate bioceramics from nanopowders by sintering

Lukić, Miodrag; Stojanović, Zoran S.; Veselinović, Ljiljana M.; Bračko, Ines; Škapin, Srečo Davor; Marković, Smilja; Uskoković, Dragan

(2010)

TY  - CONF
AU  - Lukić, Miodrag
AU  - Stojanović, Zoran S.
AU  - Veselinović, Ljiljana M.
AU  - Bračko, Ines
AU  - Škapin, Srečo Davor
AU  - Marković, Smilja
AU  - Uskoković, Dragan
PY  - 2010
UR  - http://dais.sanu.ac.rs/123456789/240
UR  - https://vinar.vin.bg.ac.rs/handle/123456789/7369
AB  - Poster presented at the Adriatic School of Nanoscience – ASON-1, Dubrovnik, Croatia, September 19–23, 2010
T1  - Full density calcium phosphate bioceramics from nanopowders by sintering
UR  - https://hdl.handle.net/21.15107/rcub_vinar_7369
ER  - 
@conference{
author = "Lukić, Miodrag and Stojanović, Zoran S. and Veselinović, Ljiljana M. and Bračko, Ines and Škapin, Srečo Davor and Marković, Smilja and Uskoković, Dragan",
year = "2010",
abstract = "Poster presented at the Adriatic School of Nanoscience – ASON-1, Dubrovnik, Croatia, September 19–23, 2010",
title = "Full density calcium phosphate bioceramics from nanopowders by sintering",
url = "https://hdl.handle.net/21.15107/rcub_vinar_7369"
}
Lukić, M., Stojanović, Z. S., Veselinović, L. M., Bračko, I., Škapin, S. D., Marković, S.,& Uskoković, D.. (2010). Full density calcium phosphate bioceramics from nanopowders by sintering. .
https://hdl.handle.net/21.15107/rcub_vinar_7369
Lukić M, Stojanović ZS, Veselinović LM, Bračko I, Škapin SD, Marković S, Uskoković D. Full density calcium phosphate bioceramics from nanopowders by sintering. 2010;.
https://hdl.handle.net/21.15107/rcub_vinar_7369 .
Lukić, Miodrag, Stojanović, Zoran S., Veselinović, Ljiljana M., Bračko, Ines, Škapin, Srečo Davor, Marković, Smilja, Uskoković, Dragan, "Full density calcium phosphate bioceramics from nanopowders by sintering" (2010),
https://hdl.handle.net/21.15107/rcub_vinar_7369 .

Sintering of different hydroxyapatite nanopowders

Lukić, Miodrag; Stojanović, Zoran S.; Veselinović, Ljiljana M.; Škapin, Srečo Davor; Bračko, Ines; Marković, Smilja; Uskoković, Dragan

(2010)

TY  - CONF
AU  - Lukić, Miodrag
AU  - Stojanović, Zoran S.
AU  - Veselinović, Ljiljana M.
AU  - Škapin, Srečo Davor
AU  - Bračko, Ines
AU  - Marković, Smilja
AU  - Uskoković, Dragan
PY  - 2010
UR  - http://dais.sanu.ac.rs/123456789/250
UR  - https://vinar.vin.bg.ac.rs/handle/123456789/7376
AB  - Poster presented at the Workshop: Processing of Nanostructured Ceramics, Polymers, and Composites, Faculty of Technology and Metallurgy, University of Belgrade, November 29–30, 2010
T1  - Sintering of different hydroxyapatite nanopowders
UR  - https://hdl.handle.net/21.15107/rcub_vinar_7376
ER  - 
@conference{
author = "Lukić, Miodrag and Stojanović, Zoran S. and Veselinović, Ljiljana M. and Škapin, Srečo Davor and Bračko, Ines and Marković, Smilja and Uskoković, Dragan",
year = "2010",
abstract = "Poster presented at the Workshop: Processing of Nanostructured Ceramics, Polymers, and Composites, Faculty of Technology and Metallurgy, University of Belgrade, November 29–30, 2010",
title = "Sintering of different hydroxyapatite nanopowders",
url = "https://hdl.handle.net/21.15107/rcub_vinar_7376"
}
Lukić, M., Stojanović, Z. S., Veselinović, L. M., Škapin, S. D., Bračko, I., Marković, S.,& Uskoković, D.. (2010). Sintering of different hydroxyapatite nanopowders. .
https://hdl.handle.net/21.15107/rcub_vinar_7376
Lukić M, Stojanović ZS, Veselinović LM, Škapin SD, Bračko I, Marković S, Uskoković D. Sintering of different hydroxyapatite nanopowders. 2010;.
https://hdl.handle.net/21.15107/rcub_vinar_7376 .
Lukić, Miodrag, Stojanović, Zoran S., Veselinović, Ljiljana M., Škapin, Srečo Davor, Bračko, Ines, Marković, Smilja, Uskoković, Dragan, "Sintering of different hydroxyapatite nanopowders" (2010),
https://hdl.handle.net/21.15107/rcub_vinar_7376 .

Ultrasonic Deagglomeration and Particle Size Reduction of Hydroxyapatite by Coating With Poly(D,L-Lactide-Co-Glycolide)

Jevtić, Marija; Mitrić, Miodrag; Škapin, Srečo Davor; Bračko, Ines; Ignjatović, Nenad L.; Uskoković, Dragan

(2008)

TY  - CONF
AU  - Jevtić, Marija
AU  - Mitrić, Miodrag
AU  - Škapin, Srečo Davor
AU  - Bračko, Ines
AU  - Ignjatović, Nenad L.
AU  - Uskoković, Dragan
PY  - 2008
UR  - http://dais.sanu.ac.rs/123456789/297
UR  - https://vinar.vin.bg.ac.rs/handle/123456789/7391
AB  - Poster presented at the 10th Conference of the Materials Research Society of Serbia - YUCOMAT 2008, Herceg Novi, Montenegro, September 8-12, 2008.
T1  - Ultrasonic Deagglomeration and Particle Size Reduction of Hydroxyapatite by Coating With Poly(D,L-Lactide-Co-Glycolide)
UR  - https://hdl.handle.net/21.15107/rcub_vinar_7391
ER  - 
@conference{
author = "Jevtić, Marija and Mitrić, Miodrag and Škapin, Srečo Davor and Bračko, Ines and Ignjatović, Nenad L. and Uskoković, Dragan",
year = "2008",
abstract = "Poster presented at the 10th Conference of the Materials Research Society of Serbia - YUCOMAT 2008, Herceg Novi, Montenegro, September 8-12, 2008.",
title = "Ultrasonic Deagglomeration and Particle Size Reduction of Hydroxyapatite by Coating With Poly(D,L-Lactide-Co-Glycolide)",
url = "https://hdl.handle.net/21.15107/rcub_vinar_7391"
}
Jevtić, M., Mitrić, M., Škapin, S. D., Bračko, I., Ignjatović, N. L.,& Uskoković, D.. (2008). Ultrasonic Deagglomeration and Particle Size Reduction of Hydroxyapatite by Coating With Poly(D,L-Lactide-Co-Glycolide). .
https://hdl.handle.net/21.15107/rcub_vinar_7391
Jevtić M, Mitrić M, Škapin SD, Bračko I, Ignjatović NL, Uskoković D. Ultrasonic Deagglomeration and Particle Size Reduction of Hydroxyapatite by Coating With Poly(D,L-Lactide-Co-Glycolide). 2008;.
https://hdl.handle.net/21.15107/rcub_vinar_7391 .
Jevtić, Marija, Mitrić, Miodrag, Škapin, Srečo Davor, Bračko, Ines, Ignjatović, Nenad L., Uskoković, Dragan, "Ultrasonic Deagglomeration and Particle Size Reduction of Hydroxyapatite by Coating With Poly(D,L-Lactide-Co-Glycolide)" (2008),
https://hdl.handle.net/21.15107/rcub_vinar_7391 .