TY  - CONF
AU  - Nikolić, Nebojša D.
AU  - Lović, Jelena
AU  - Maksimović, Vesna
AU  - Stevanović, Sanja
PY  - 2023
UR  - https://vinar.vin.bg.ac.rs/handle/123456789/11759
AB  - Tin dendrites found wide application in various industries.1 They can be obtained by both non-electrochemical and electrochemical methods of synthesis. In this study, they were produced by a galvanostatic regime of electrolysis from alkaline hydroxide solution at a current density of –3 mA cm–2 , 1.5 times larger than the limiting diffusion current density, with an amount of the electricity of 200 and 400 mC. In the dependence of an amount of the passed electricity, Sn dendrites of various morphology and crystal orientation were obtained: the fern-like dendrites predominantly oriented in (220), (440) crystal planes are obtained with 200 mC and the spear-like and the dendrites with prismatic branches showing the strong (200),(400) preferred orientationwere obtained with 400 mC. The strong correlation between morphology and structure of Sn dendrites is established and it can be explained by analysis of chronopotentiometry response obtained at the given current density and by morphological and structural analyses of Sn dendrites obtained by a potentiostatic regime at cathodic potentials corresponding to values attained after the passed amount of the electricity of 200 and 400 mC. The chronopotentiometry response after spent 200 mC was dominantly in the (–1600 – 1740) mV vs. Ag/AgCl range, and the fern-like dendrites with the strong (220), (440) preferred orientation were obtained in this potential range. After spent 400 mC, the chronopotentiometry response was about –1200 mV vs. Ag/AgCl, and the spear-like and the dendrites with prismatic branches with the strong (200),(400) preferred orientationwere obtained at this cathodic potential.
PB  - Society of Chemists and Technologists of Macedonia
C3  - 26th Congress of the Society of Chemists and Technologists of Macedonia : the book of abstracts; September 20-23, Ohrid, Macedonia
T1  - Correlation Between Morphology and Structure of Galvanostatically Electrodeposited Tin Dendrites
SP  - 136
EP  - 136
UR  - https://hdl.handle.net/21.15107/rcub_vinar_11759
ER  - 

@conference{
author = "Nikolić, Nebojša D. and Lović, Jelena and Maksimović, Vesna and Stevanović, Sanja",
year = "2023",
abstract = "Tin dendrites found wide application in various industries.1 They can be obtained by both non-electrochemical and electrochemical methods of synthesis. In this study, they were produced by a galvanostatic regime of electrolysis from alkaline hydroxide solution at a current density of –3 mA cm–2 , 1.5 times larger than the limiting diffusion current density, with an amount of the electricity of 200 and 400 mC. In the dependence of an amount of the passed electricity, Sn dendrites of various morphology and crystal orientation were obtained: the fern-like dendrites predominantly oriented in (220), (440) crystal planes are obtained with 200 mC and the spear-like and the dendrites with prismatic branches showing the strong (200),(400) preferred orientationwere obtained with 400 mC. The strong correlation between morphology and structure of Sn dendrites is established and it can be explained by analysis of chronopotentiometry response obtained at the given current density and by morphological and structural analyses of Sn dendrites obtained by a potentiostatic regime at cathodic potentials corresponding to values attained after the passed amount of the electricity of 200 and 400 mC. The chronopotentiometry response after spent 200 mC was dominantly in the (–1600 – 1740) mV vs. Ag/AgCl range, and the fern-like dendrites with the strong (220), (440) preferred orientation were obtained in this potential range. After spent 400 mC, the chronopotentiometry response was about –1200 mV vs. Ag/AgCl, and the spear-like and the dendrites with prismatic branches with the strong (200),(400) preferred orientationwere obtained at this cathodic potential.",
publisher = "Society of Chemists and Technologists of Macedonia",
journal = "26th Congress of the Society of Chemists and Technologists of Macedonia : the book of abstracts; September 20-23, Ohrid, Macedonia",
title = "Correlation Between Morphology and Structure of Galvanostatically Electrodeposited Tin Dendrites",
pages = "136-136",
url = "https://hdl.handle.net/21.15107/rcub_vinar_11759"
}

Nikolić, N. D., Lović, J., Maksimović, V.,& Stevanović, S.. (2023). Correlation Between Morphology and Structure of Galvanostatically Electrodeposited Tin Dendrites. in 26th Congress of the Society of Chemists and Technologists of Macedonia : the book of abstracts; September 20-23, Ohrid, Macedonia
Society of Chemists and Technologists of Macedonia., 136-136.
https://hdl.handle.net/21.15107/rcub_vinar_11759

Nikolić ND, Lović J, Maksimović V, Stevanović S. Correlation Between Morphology and Structure of Galvanostatically Electrodeposited Tin Dendrites. in 26th Congress of the Society of Chemists and Technologists of Macedonia : the book of abstracts; September 20-23, Ohrid, Macedonia. 2023;:136-136.
https://hdl.handle.net/21.15107/rcub_vinar_11759 .

Nikolić, Nebojša D., Lović, Jelena, Maksimović, Vesna, Stevanović, Sanja, "Correlation Between Morphology and Structure of Galvanostatically Electrodeposited Tin Dendrites" in 26th Congress of the Society of Chemists and Technologists of Macedonia : the book of abstracts; September 20-23, Ohrid, Macedonia (2023):136-136,
https://hdl.handle.net/21.15107/rcub_vinar_11759 .

TY  - JOUR
AU  - Lović, Jelena
AU  - Nikolić, Nebojša D.
AU  - Maksimović, Vesna
PY  - 2023
UR  - https://vinar.vin.bg.ac.rs/handle/123456789/10608
AB  - The influence of chronopotentiometry response on the morphology and structure of galvanostatically synthesized tin dendriticparticles has been investigated. Sn dendrites were electrodeposited at the current density 1.5 times larger than the limiting diffusioncurrent density (− 3 mA cm−2) with various amounts of the electricity (200 and 400 mC), and the obtained morphologyand structure of the particles were characterized by SEM and XRD techniques, respectively. The strong effect of the amountof spent electricity on the morphology and structure of the particles was observed, and it is explained by morphological andstructural analysis of Sn particles produced potentiostatically at various cathodic potentials selected to be in line with therecorded chronopotentiometry response. The strong correlation among chronopotentiometry response, morphology, andstructure of the Sn dendrites was established. The spear-like and the dendrites with prismatic branches possessed the strong(200),(400) preferred orientation, and they were obtained with a chronopotentiometry response of about − 1200 mV vs. Ag/AgCl. The chronopotentiometry responses in the − 1210 ÷ − 1740 mV vs. Ag/AgCl range caused a formation of the fern-likedendrites with the strong (220),(440) preferred orientation. Based on the obtained results, it follows that the chronopotentiometryanalysis represents good diagnostic criteria for obtaining Sn powder particles of desired morphology and structure.
T2  - Journal of Solid State Electrochemistry
T1  - The control of morphology and structure of galvanostatically produced tin dendrites by analysis of chronopotentiometry response
DO  - 10.1007/s10008-023-05380-6
ER  - 

@article{
author = "Lović, Jelena and Nikolić, Nebojša D. and Maksimović, Vesna",
year = "2023",
abstract = "The influence of chronopotentiometry response on the morphology and structure of galvanostatically synthesized tin dendriticparticles has been investigated. Sn dendrites were electrodeposited at the current density 1.5 times larger than the limiting diffusioncurrent density (− 3 mA cm−2) with various amounts of the electricity (200 and 400 mC), and the obtained morphologyand structure of the particles were characterized by SEM and XRD techniques, respectively. The strong effect of the amountof spent electricity on the morphology and structure of the particles was observed, and it is explained by morphological andstructural analysis of Sn particles produced potentiostatically at various cathodic potentials selected to be in line with therecorded chronopotentiometry response. The strong correlation among chronopotentiometry response, morphology, andstructure of the Sn dendrites was established. The spear-like and the dendrites with prismatic branches possessed the strong(200),(400) preferred orientation, and they were obtained with a chronopotentiometry response of about − 1200 mV vs. Ag/AgCl. The chronopotentiometry responses in the − 1210 ÷ − 1740 mV vs. Ag/AgCl range caused a formation of the fern-likedendrites with the strong (220),(440) preferred orientation. Based on the obtained results, it follows that the chronopotentiometryanalysis represents good diagnostic criteria for obtaining Sn powder particles of desired morphology and structure.",
journal = "Journal of Solid State Electrochemistry",
title = "The control of morphology and structure of galvanostatically produced tin dendrites by analysis of chronopotentiometry response",
doi = "10.1007/s10008-023-05380-6"
}

Lović, J., Nikolić, N. D.,& Maksimović, V.. (2023). The control of morphology and structure of galvanostatically produced tin dendrites by analysis of chronopotentiometry response. in Journal of Solid State Electrochemistry.
https://doi.org/10.1007/s10008-023-05380-6

Lović J, Nikolić ND, Maksimović V. The control of morphology and structure of galvanostatically produced tin dendrites by analysis of chronopotentiometry response. in Journal of Solid State Electrochemistry. 2023;.
doi:10.1007/s10008-023-05380-6 .

Lović, Jelena, Nikolić, Nebojša D., Maksimović, Vesna, "The control of morphology and structure of galvanostatically produced tin dendrites by analysis of chronopotentiometry response" in Journal of Solid State Electrochemistry (2023),
https://doi.org/10.1007/s10008-023-05380-6 . .