Ouzo effect-New simple nanoemulsion method for synthesis of strontium hydroxyapatite nanospheres
Samo za registrovane korisnike
2016
Autori
Prekajski, Marija D.Mirković, Miljana M.
Todorović, Bratislav Ž.
Matković, Aleksandar
Marinović-Cincović, Milena
Luković, Jelena M.
Matović, Branko
Članak u časopisu (Objavljena verzija)
Metapodaci
Prikaz svih podataka o dokumentuApstrakt
Nanoemulsion technique was applied for synthesis of carbonated strontium hydroxyapatite (CSrHAp) at room temperature. X-ray powder diffraction analysis accompanied with Rietveld refinement reviled that synthesized powder were single-phase hydroxyapatite. Fourier transform infrared (FTIR) spectroscopy showed that the CSrHAp was A-type substitution. The carbonate amount substituting the hydroxide group in the synthesized apatite was estimated, from the corresponding CO2 weight loss in the range 600-1100 degrees C. According to this empirical formula of as synthesized CHAp is S-10(PO4)(6)(OH)(0.60)(CO3)(0.70). These results were confirmed by the Rietveld refinement analysis. Using scanning electron microscopy analysis it was found that the synthesized CSrHAp particles were spherical in shape and that their sizes were in the nanometer range. Nanoemulsion strategy procedure provides a simple pathway to obtain single-phase CSrHAp. (C) 2015 Elsevier Ltd. All rights reserved.
Ključne reči:
Nanoparticles / Synthesis / Thermogravimetric analysis (TGA) / Infrared spectroscopy / X-ray diffractionIzvor:
Journal of the European Ceramic Society, 2016, 36, 5, 1293-1298Izdavač:
- Elsevier
Finansiranje / projekti:
- Sinteza, procesiranje i karakterizacija nanostrukturnih materijala za primenu u oblasti energije, mehaničkog inženjerstva, zaštite životne stredine i biomedicine (RS-MESTD-Integrated and Interdisciplinary Research (IIR or III)-45012)
- Magmatizam i geodinamika Balkanskog poluostrva od mezozoika do danas: značaj za obrazovanje metaličnih i nemetaličnih rudnih ležišta (RS-MESTD-Basic Research (BR or ON)-176016)
DOI: 10.1016/j.jeurceramsoc.2015.11.045
ISSN: 0955-2219; 1873-619X
WoS: 000369457300020
Scopus: 2-s2.0-84958743933
Kolekcije
Institucija/grupa
VinčaTY - JOUR AU - Prekajski, Marija D. AU - Mirković, Miljana M. AU - Todorović, Bratislav Ž. AU - Matković, Aleksandar AU - Marinović-Cincović, Milena AU - Luković, Jelena M. AU - Matović, Branko PY - 2016 UR - https://vinar.vin.bg.ac.rs/handle/123456789/924 AB - Nanoemulsion technique was applied for synthesis of carbonated strontium hydroxyapatite (CSrHAp) at room temperature. X-ray powder diffraction analysis accompanied with Rietveld refinement reviled that synthesized powder were single-phase hydroxyapatite. Fourier transform infrared (FTIR) spectroscopy showed that the CSrHAp was A-type substitution. The carbonate amount substituting the hydroxide group in the synthesized apatite was estimated, from the corresponding CO2 weight loss in the range 600-1100 degrees C. According to this empirical formula of as synthesized CHAp is S-10(PO4)(6)(OH)(0.60)(CO3)(0.70). These results were confirmed by the Rietveld refinement analysis. Using scanning electron microscopy analysis it was found that the synthesized CSrHAp particles were spherical in shape and that their sizes were in the nanometer range. Nanoemulsion strategy procedure provides a simple pathway to obtain single-phase CSrHAp. (C) 2015 Elsevier Ltd. All rights reserved. PB - Elsevier T2 - Journal of the European Ceramic Society T1 - Ouzo effect-New simple nanoemulsion method for synthesis of strontium hydroxyapatite nanospheres VL - 36 IS - 5 SP - 1293 EP - 1298 DO - 10.1016/j.jeurceramsoc.2015.11.045 ER -
@article{ author = "Prekajski, Marija D. and Mirković, Miljana M. and Todorović, Bratislav Ž. and Matković, Aleksandar and Marinović-Cincović, Milena and Luković, Jelena M. and Matović, Branko", year = "2016", abstract = "Nanoemulsion technique was applied for synthesis of carbonated strontium hydroxyapatite (CSrHAp) at room temperature. X-ray powder diffraction analysis accompanied with Rietveld refinement reviled that synthesized powder were single-phase hydroxyapatite. Fourier transform infrared (FTIR) spectroscopy showed that the CSrHAp was A-type substitution. The carbonate amount substituting the hydroxide group in the synthesized apatite was estimated, from the corresponding CO2 weight loss in the range 600-1100 degrees C. According to this empirical formula of as synthesized CHAp is S-10(PO4)(6)(OH)(0.60)(CO3)(0.70). These results were confirmed by the Rietveld refinement analysis. Using scanning electron microscopy analysis it was found that the synthesized CSrHAp particles were spherical in shape and that their sizes were in the nanometer range. Nanoemulsion strategy procedure provides a simple pathway to obtain single-phase CSrHAp. (C) 2015 Elsevier Ltd. All rights reserved.", publisher = "Elsevier", journal = "Journal of the European Ceramic Society", title = "Ouzo effect-New simple nanoemulsion method for synthesis of strontium hydroxyapatite nanospheres", volume = "36", number = "5", pages = "1293-1298", doi = "10.1016/j.jeurceramsoc.2015.11.045" }
Prekajski, M. D., Mirković, M. M., Todorović, B. Ž., Matković, A., Marinović-Cincović, M., Luković, J. M.,& Matović, B.. (2016). Ouzo effect-New simple nanoemulsion method for synthesis of strontium hydroxyapatite nanospheres. in Journal of the European Ceramic Society Elsevier., 36(5), 1293-1298. https://doi.org/10.1016/j.jeurceramsoc.2015.11.045
Prekajski MD, Mirković MM, Todorović BŽ, Matković A, Marinović-Cincović M, Luković JM, Matović B. Ouzo effect-New simple nanoemulsion method for synthesis of strontium hydroxyapatite nanospheres. in Journal of the European Ceramic Society. 2016;36(5):1293-1298. doi:10.1016/j.jeurceramsoc.2015.11.045 .
Prekajski, Marija D., Mirković, Miljana M., Todorović, Bratislav Ž., Matković, Aleksandar, Marinović-Cincović, Milena, Luković, Jelena M., Matović, Branko, "Ouzo effect-New simple nanoemulsion method for synthesis of strontium hydroxyapatite nanospheres" in Journal of the European Ceramic Society, 36, no. 5 (2016):1293-1298, https://doi.org/10.1016/j.jeurceramsoc.2015.11.045 . .