Compaction pressure's influence on density and electrical properties of sintered cordierite-based ceramics
Апстракт
Mechanical activation is widely used for sample preparation before the sintering process. However, the influence of pressure, which is used for compaction, has not been completely investigated. Cordierite, 2MgO_2Al2O3_5SiO2, is a very attractive high-temperature ceramic material, due to its outstanding electrical characteristics, such as the low temperature expansion coefficient, low dielectric constant and good mechanical properties. Based on our previous investigation, the mechanical activation of the starting mixtures with 5.00 mass% TiO2 was performed in a high energy ball mill during 10 minutes. Compaction pressure varied from 0.5 to 6 t/cm2. Differential thermal analysis (DTA) was used in order to determine characteristic temperatures within the system during heating. Sintering process was performed at 1350 °C for 4 h in air atmosphere. The phase composition of activated and sintered samples was analyzed by the X-ray diffraction method. Scanning electron microscopy was performed ...to analyze both compacted and sintered sample microstructure. This paper deals with the influence of compaction pressure on the densities of green bodies as well as on the sintered samples, along with electrical properties
Кључне речи:
cordierite / ceramic materials / mechanical activation / ball millingИзвор:
Joint Event of the 11th Young Researchers’ Conference: Materials Science and Engineering and the 1st European Early Stage Researches’ Conference on Hydrogen Storage: Program and the Book of Abstracts, 2012, 61-61Издавач:
- Belgrade : Materials Research Society of Serbia; Institute of Technical Sciences of SASA; Vinča Institute of Nuclear Sciences, University of Belgrade
Финансирање / пројекти:
- Усмерена синтеза, структура и својства мултифункционалних материјала (RS-MESTD-Basic Research (BR or ON)-172057)
Колекције
Институција/група
VinčaTY - CONF AU - Obradović, Nina AU - Đorđević, N. AU - Peleš, Adriana AU - Mitrić, Miodrag AU - Pavlović, Vladimir B. PY - 2012 UR - http://dais.sanu.ac.rs/123456789/525 UR - https://vinar.vin.bg.ac.rs/handle/123456789/7468 AB - Mechanical activation is widely used for sample preparation before the sintering process. However, the influence of pressure, which is used for compaction, has not been completely investigated. Cordierite, 2MgO_2Al2O3_5SiO2, is a very attractive high-temperature ceramic material, due to its outstanding electrical characteristics, such as the low temperature expansion coefficient, low dielectric constant and good mechanical properties. Based on our previous investigation, the mechanical activation of the starting mixtures with 5.00 mass% TiO2 was performed in a high energy ball mill during 10 minutes. Compaction pressure varied from 0.5 to 6 t/cm2. Differential thermal analysis (DTA) was used in order to determine characteristic temperatures within the system during heating. Sintering process was performed at 1350 °C for 4 h in air atmosphere. The phase composition of activated and sintered samples was analyzed by the X-ray diffraction method. Scanning electron microscopy was performed to analyze both compacted and sintered sample microstructure. This paper deals with the influence of compaction pressure on the densities of green bodies as well as on the sintered samples, along with electrical properties PB - Belgrade : Materials Research Society of Serbia; Institute of Technical Sciences of SASA; Vinča Institute of Nuclear Sciences, University of Belgrade C3 - Joint Event of the 11th Young Researchers’ Conference: Materials Science and Engineering and the 1st European Early Stage Researches’ Conference on Hydrogen Storage: Program and the Book of Abstracts T1 - Compaction pressure's influence on density and electrical properties of sintered cordierite-based ceramics SP - 61 EP - 61 UR - https://hdl.handle.net/21.15107/rcub_vinar_7468 ER -
@conference{ author = "Obradović, Nina and Đorđević, N. and Peleš, Adriana and Mitrić, Miodrag and Pavlović, Vladimir B.", year = "2012", abstract = "Mechanical activation is widely used for sample preparation before the sintering process. However, the influence of pressure, which is used for compaction, has not been completely investigated. Cordierite, 2MgO_2Al2O3_5SiO2, is a very attractive high-temperature ceramic material, due to its outstanding electrical characteristics, such as the low temperature expansion coefficient, low dielectric constant and good mechanical properties. Based on our previous investigation, the mechanical activation of the starting mixtures with 5.00 mass% TiO2 was performed in a high energy ball mill during 10 minutes. Compaction pressure varied from 0.5 to 6 t/cm2. Differential thermal analysis (DTA) was used in order to determine characteristic temperatures within the system during heating. Sintering process was performed at 1350 °C for 4 h in air atmosphere. The phase composition of activated and sintered samples was analyzed by the X-ray diffraction method. Scanning electron microscopy was performed to analyze both compacted and sintered sample microstructure. This paper deals with the influence of compaction pressure on the densities of green bodies as well as on the sintered samples, along with electrical properties", publisher = "Belgrade : Materials Research Society of Serbia; Institute of Technical Sciences of SASA; Vinča Institute of Nuclear Sciences, University of Belgrade", journal = "Joint Event of the 11th Young Researchers’ Conference: Materials Science and Engineering and the 1st European Early Stage Researches’ Conference on Hydrogen Storage: Program and the Book of Abstracts", title = "Compaction pressure's influence on density and electrical properties of sintered cordierite-based ceramics", pages = "61-61", url = "https://hdl.handle.net/21.15107/rcub_vinar_7468" }
Obradović, N., Đorđević, N., Peleš, A., Mitrić, M.,& Pavlović, V. B.. (2012). Compaction pressure's influence on density and electrical properties of sintered cordierite-based ceramics. in Joint Event of the 11th Young Researchers’ Conference: Materials Science and Engineering and the 1st European Early Stage Researches’ Conference on Hydrogen Storage: Program and the Book of Abstracts Belgrade : Materials Research Society of Serbia; Institute of Technical Sciences of SASA; Vinča Institute of Nuclear Sciences, University of Belgrade., 61-61. https://hdl.handle.net/21.15107/rcub_vinar_7468
Obradović N, Đorđević N, Peleš A, Mitrić M, Pavlović VB. Compaction pressure's influence on density and electrical properties of sintered cordierite-based ceramics. in Joint Event of the 11th Young Researchers’ Conference: Materials Science and Engineering and the 1st European Early Stage Researches’ Conference on Hydrogen Storage: Program and the Book of Abstracts. 2012;:61-61. https://hdl.handle.net/21.15107/rcub_vinar_7468 .
Obradović, Nina, Đorđević, N., Peleš, Adriana, Mitrić, Miodrag, Pavlović, Vladimir B., "Compaction pressure's influence on density and electrical properties of sintered cordierite-based ceramics" in Joint Event of the 11th Young Researchers’ Conference: Materials Science and Engineering and the 1st European Early Stage Researches’ Conference on Hydrogen Storage: Program and the Book of Abstracts (2012):61-61, https://hdl.handle.net/21.15107/rcub_vinar_7468 .