Structural and thermal characterization of Fe(III) and Fe(II) complexes with tridentate ono pyridoxal semicarbazone
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Jacimovic, Z. K.Leovac, Vukadin M.
Giester, Gerald
Tomić, Zoran D.
Szesenyi, Katalin Meszaros
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Molecular and crystal structure of diaqua-sulphato(pyfidoxal semicarbazone-ONO)iron(II) and dichloroaqua(pyridoxal semicarbazone-ONO)iron(III) complexes with tridentate ONO pyridoxal sernicarbazone ligand, PLSC, of formula [Fe-II(PLSC)(H2O)(2)SO4] and [Fe-III(PLSC)(H2O)Cl-2]Cl is reported. Thermal decomposition of the compounds was followed in argon and air gas carriers. The deaquation mechanism is discussed in the view of the crystal structure, emphasizing the complexity of the related parameters and processes.
Keywords:
crystal structure / deaquation mechanism / iron(II) and iron(III) complexes / pyridoxal semicarbazone thermal decompositionSource:
Journal of Thermal Analysis and Calorimetry, 2007, 90, 2, 549-555Note:
- 32nd Workshop on Heterogeneous Equilibria between Phases (JEEP 2006), Mar 30-31, 2006, Univ Rouen, Rouen, France
DOI: 10.1007/s10973-006-8267-x
ISSN: 1388-6150
WoS: 000251088600037
Scopus: 2-s2.0-36949008760
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VinčaTY - JOUR AU - Jacimovic, Z. K. AU - Leovac, Vukadin M. AU - Giester, Gerald AU - Tomić, Zoran D. AU - Szesenyi, Katalin Meszaros PY - 2007 UR - https://vinar.vin.bg.ac.rs/handle/123456789/6705 AB - Molecular and crystal structure of diaqua-sulphato(pyfidoxal semicarbazone-ONO)iron(II) and dichloroaqua(pyridoxal semicarbazone-ONO)iron(III) complexes with tridentate ONO pyridoxal sernicarbazone ligand, PLSC, of formula [Fe-II(PLSC)(H2O)(2)SO4] and [Fe-III(PLSC)(H2O)Cl-2]Cl is reported. Thermal decomposition of the compounds was followed in argon and air gas carriers. The deaquation mechanism is discussed in the view of the crystal structure, emphasizing the complexity of the related parameters and processes. T2 - Journal of Thermal Analysis and Calorimetry T1 - Structural and thermal characterization of Fe(III) and Fe(II) complexes with tridentate ono pyridoxal semicarbazone VL - 90 IS - 2 SP - 549 EP - 555 DO - 10.1007/s10973-006-8267-x ER -
@article{ author = "Jacimovic, Z. K. and Leovac, Vukadin M. and Giester, Gerald and Tomić, Zoran D. and Szesenyi, Katalin Meszaros", year = "2007", abstract = "Molecular and crystal structure of diaqua-sulphato(pyfidoxal semicarbazone-ONO)iron(II) and dichloroaqua(pyridoxal semicarbazone-ONO)iron(III) complexes with tridentate ONO pyridoxal sernicarbazone ligand, PLSC, of formula [Fe-II(PLSC)(H2O)(2)SO4] and [Fe-III(PLSC)(H2O)Cl-2]Cl is reported. Thermal decomposition of the compounds was followed in argon and air gas carriers. The deaquation mechanism is discussed in the view of the crystal structure, emphasizing the complexity of the related parameters and processes.", journal = "Journal of Thermal Analysis and Calorimetry", title = "Structural and thermal characterization of Fe(III) and Fe(II) complexes with tridentate ono pyridoxal semicarbazone", volume = "90", number = "2", pages = "549-555", doi = "10.1007/s10973-006-8267-x" }
Jacimovic, Z. K., Leovac, V. M., Giester, G., Tomić, Z. D.,& Szesenyi, K. M.. (2007). Structural and thermal characterization of Fe(III) and Fe(II) complexes with tridentate ono pyridoxal semicarbazone. in Journal of Thermal Analysis and Calorimetry, 90(2), 549-555. https://doi.org/10.1007/s10973-006-8267-x
Jacimovic ZK, Leovac VM, Giester G, Tomić ZD, Szesenyi KM. Structural and thermal characterization of Fe(III) and Fe(II) complexes with tridentate ono pyridoxal semicarbazone. in Journal of Thermal Analysis and Calorimetry. 2007;90(2):549-555. doi:10.1007/s10973-006-8267-x .
Jacimovic, Z. K., Leovac, Vukadin M., Giester, Gerald, Tomić, Zoran D., Szesenyi, Katalin Meszaros, "Structural and thermal characterization of Fe(III) and Fe(II) complexes with tridentate ono pyridoxal semicarbazone" in Journal of Thermal Analysis and Calorimetry, 90, no. 2 (2007):549-555, https://doi.org/10.1007/s10973-006-8267-x . .