Combustion synthesis as a novel approach in preparation of polycrystalline Y2Cu2O5
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Gebrel, Z.Blanuša, Jovan
Spasojević, Vojislav
Kusigerski, Vladan
Mraković, Ana Đ.
Alqat, A.
Perović, Marija M.
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Polycrystalline samples of Y2Cu2O5 were for the first time sintered from precursors obtained by two combustion routes - the glycine-nitrate method (sample S1) and a modified self-propagating high-temperature synthesis (sample S2). The detailed X-ray diffraction analysis has confirmed that both samples are well crystallized and single phase, with the high crystallization degree and cation ordering within a Cu sublattice. Magnetic characterization has shown magnetic behavior typical of pure Y2Cu2O5. The distinctive advantages of these new synthesis routes in comparison to the ceramic sintering are in simplification of the overall procedure as well as in a significant reduction of synthesis duration from several days down to 31 h (S1) or 12 h (S2). (C) 2013 Elsevier B.V. All rights reserved.
Keywords:
Transition metal alloys and compounds / Solid state reactions / Magnetization / X-ray diffractionSource:
Journal of Alloys and Compounds, 2013, 568, 55-59Funding / projects:
- Magnetic and radionuclide labeled nanostructured materials for medical applications (RS-MESTD-Integrated and Interdisciplinary Research (IIR or III)-45015)
DOI: 10.1016/j.jallcom.2013.03.133
ISSN: 0925-8388
WoS: 000319208000010
Scopus: 2-s2.0-84875979636
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VinčaTY - JOUR AU - Gebrel, Z. AU - Blanuša, Jovan AU - Spasojević, Vojislav AU - Kusigerski, Vladan AU - Mraković, Ana Đ. AU - Alqat, A. AU - Perović, Marija M. PY - 2013 UR - https://vinar.vin.bg.ac.rs/handle/123456789/5515 AB - Polycrystalline samples of Y2Cu2O5 were for the first time sintered from precursors obtained by two combustion routes - the glycine-nitrate method (sample S1) and a modified self-propagating high-temperature synthesis (sample S2). The detailed X-ray diffraction analysis has confirmed that both samples are well crystallized and single phase, with the high crystallization degree and cation ordering within a Cu sublattice. Magnetic characterization has shown magnetic behavior typical of pure Y2Cu2O5. The distinctive advantages of these new synthesis routes in comparison to the ceramic sintering are in simplification of the overall procedure as well as in a significant reduction of synthesis duration from several days down to 31 h (S1) or 12 h (S2). (C) 2013 Elsevier B.V. All rights reserved. T2 - Journal of Alloys and Compounds T1 - Combustion synthesis as a novel approach in preparation of polycrystalline Y2Cu2O5 VL - 568 SP - 55 EP - 59 DO - 10.1016/j.jallcom.2013.03.133 ER -
@article{ author = "Gebrel, Z. and Blanuša, Jovan and Spasojević, Vojislav and Kusigerski, Vladan and Mraković, Ana Đ. and Alqat, A. and Perović, Marija M.", year = "2013", abstract = "Polycrystalline samples of Y2Cu2O5 were for the first time sintered from precursors obtained by two combustion routes - the glycine-nitrate method (sample S1) and a modified self-propagating high-temperature synthesis (sample S2). The detailed X-ray diffraction analysis has confirmed that both samples are well crystallized and single phase, with the high crystallization degree and cation ordering within a Cu sublattice. Magnetic characterization has shown magnetic behavior typical of pure Y2Cu2O5. The distinctive advantages of these new synthesis routes in comparison to the ceramic sintering are in simplification of the overall procedure as well as in a significant reduction of synthesis duration from several days down to 31 h (S1) or 12 h (S2). (C) 2013 Elsevier B.V. All rights reserved.", journal = "Journal of Alloys and Compounds", title = "Combustion synthesis as a novel approach in preparation of polycrystalline Y2Cu2O5", volume = "568", pages = "55-59", doi = "10.1016/j.jallcom.2013.03.133" }
Gebrel, Z., Blanuša, J., Spasojević, V., Kusigerski, V., Mraković, A. Đ., Alqat, A.,& Perović, M. M.. (2013). Combustion synthesis as a novel approach in preparation of polycrystalline Y2Cu2O5. in Journal of Alloys and Compounds, 568, 55-59. https://doi.org/10.1016/j.jallcom.2013.03.133
Gebrel Z, Blanuša J, Spasojević V, Kusigerski V, Mraković AĐ, Alqat A, Perović MM. Combustion synthesis as a novel approach in preparation of polycrystalline Y2Cu2O5. in Journal of Alloys and Compounds. 2013;568:55-59. doi:10.1016/j.jallcom.2013.03.133 .
Gebrel, Z., Blanuša, Jovan, Spasojević, Vojislav, Kusigerski, Vladan, Mraković, Ana Đ., Alqat, A., Perović, Marija M., "Combustion synthesis as a novel approach in preparation of polycrystalline Y2Cu2O5" in Journal of Alloys and Compounds, 568 (2013):55-59, https://doi.org/10.1016/j.jallcom.2013.03.133 . .