Gel combustion synthesis of transition metal ions doped Zn2SiO4 powder
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Lukić, Svetlana R.Petrović, Dragoslav M.
Đačanin, Ljubica
Marinović-Cincović, Milena
Antić, Željka
Krsmanović, Radenka
Dramićanin, Miroslav
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We present here the synthesis procedure for obtaining Zn2SiO4:M2+ (M = Mn, Ni, Co) powder based on the combination of so-gel and combustion methods. Combustion is performed both in a conventional furnace and in a microwave oven in order to evaluate the influence of combustion conditions on the properties of synthesized material. X-ray diffraction analysis confirmed that obtained material has crystallized in rhombohedral structure of Zn2SiO4 (willemite) with traces of ZnO. The effects of combustion conditions are investigated further by means of thermogravimetric analysis, differential thermal analysis, infrared spectroscopy, diffuse reflectance optical spectroscopy and photoluminescence spectroscopy. Based on these results we could conclude that microwave combustion synthesis can be successfully applied for Zn2SiO4-based products.
Keywords:
Materials / Experimental methods / Zn(2)SiO(4)power / Optical properties / Ultraviolet spectroscopy / Gel combustion synthesisSource:
Journal of Optoelectronics and Advanced Materials, 2008, 10, 10, 2748-2752Funding / projects:
- Sinteza i karakterizacija nanočestica i nanokompozita (RS-MESTD-MPN2006-2010-142066)
- Amorphous and nanostructural chalcogenides (RS-MESTD-MPN2006-2010-141026)
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VinčaTY - JOUR AU - Lukić, Svetlana R. AU - Petrović, Dragoslav M. AU - Đačanin, Ljubica AU - Marinović-Cincović, Milena AU - Antić, Željka AU - Krsmanović, Radenka AU - Dramićanin, Miroslav PY - 2008 UR - https://vinar.vin.bg.ac.rs/handle/123456789/3556 AB - We present here the synthesis procedure for obtaining Zn2SiO4:M2+ (M = Mn, Ni, Co) powder based on the combination of so-gel and combustion methods. Combustion is performed both in a conventional furnace and in a microwave oven in order to evaluate the influence of combustion conditions on the properties of synthesized material. X-ray diffraction analysis confirmed that obtained material has crystallized in rhombohedral structure of Zn2SiO4 (willemite) with traces of ZnO. The effects of combustion conditions are investigated further by means of thermogravimetric analysis, differential thermal analysis, infrared spectroscopy, diffuse reflectance optical spectroscopy and photoluminescence spectroscopy. Based on these results we could conclude that microwave combustion synthesis can be successfully applied for Zn2SiO4-based products. T2 - Journal of Optoelectronics and Advanced Materials T1 - Gel combustion synthesis of transition metal ions doped Zn2SiO4 powder VL - 10 IS - 10 SP - 2748 EP - 2752 UR - https://hdl.handle.net/21.15107/rcub_vinar_3556 ER -
@article{ author = "Lukić, Svetlana R. and Petrović, Dragoslav M. and Đačanin, Ljubica and Marinović-Cincović, Milena and Antić, Željka and Krsmanović, Radenka and Dramićanin, Miroslav", year = "2008", abstract = "We present here the synthesis procedure for obtaining Zn2SiO4:M2+ (M = Mn, Ni, Co) powder based on the combination of so-gel and combustion methods. Combustion is performed both in a conventional furnace and in a microwave oven in order to evaluate the influence of combustion conditions on the properties of synthesized material. X-ray diffraction analysis confirmed that obtained material has crystallized in rhombohedral structure of Zn2SiO4 (willemite) with traces of ZnO. The effects of combustion conditions are investigated further by means of thermogravimetric analysis, differential thermal analysis, infrared spectroscopy, diffuse reflectance optical spectroscopy and photoluminescence spectroscopy. Based on these results we could conclude that microwave combustion synthesis can be successfully applied for Zn2SiO4-based products.", journal = "Journal of Optoelectronics and Advanced Materials", title = "Gel combustion synthesis of transition metal ions doped Zn2SiO4 powder", volume = "10", number = "10", pages = "2748-2752", url = "https://hdl.handle.net/21.15107/rcub_vinar_3556" }
Lukić, S. R., Petrović, D. M., Đačanin, L., Marinović-Cincović, M., Antić, Ž., Krsmanović, R.,& Dramićanin, M.. (2008). Gel combustion synthesis of transition metal ions doped Zn2SiO4 powder. in Journal of Optoelectronics and Advanced Materials, 10(10), 2748-2752. https://hdl.handle.net/21.15107/rcub_vinar_3556
Lukić SR, Petrović DM, Đačanin L, Marinović-Cincović M, Antić Ž, Krsmanović R, Dramićanin M. Gel combustion synthesis of transition metal ions doped Zn2SiO4 powder. in Journal of Optoelectronics and Advanced Materials. 2008;10(10):2748-2752. https://hdl.handle.net/21.15107/rcub_vinar_3556 .
Lukić, Svetlana R., Petrović, Dragoslav M., Đačanin, Ljubica, Marinović-Cincović, Milena, Antić, Željka, Krsmanović, Radenka, Dramićanin, Miroslav, "Gel combustion synthesis of transition metal ions doped Zn2SiO4 powder" in Journal of Optoelectronics and Advanced Materials, 10, no. 10 (2008):2748-2752, https://hdl.handle.net/21.15107/rcub_vinar_3556 .