Electrochemical synthesis and characterization of hydroxyapatite powders
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Djosic, M. S.Mišković-Stanković, Vesna B.
Milonjić, Slobodan K.
Kačarević-Popović, Zorica M.
Bibić, Nataša M.
Stojanovic, J.
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Electrochemical synthesis of hydroxyapatite powders was performed galvanostatically from homogeneous solution of Na(2)H(2)EDTA center dot 2H(2)O, NaH2PO4 and CaCl2 at a concentration relationship Ca/EDTA/PO43- of 0.25/0.25/0.15 M at current densities of 137 and 207 mA cm(-2) and pH values of 9.0 and 12.0. The hydroxyapatite powders were characterized by X-ray diffraction, size distribution measurements, transmission electron microscopy, scanning electron microscopy and thermogravimetric and differential thermal analysis. The influence of the electrochemical synthesis parameters, e.g. applied current density and pH value, on the phase composition, crystallite size, morphology and thermal characteristics of hydroxyapatite powders were investigated. (c) 2008 Elsevier B.V. All rights reserved.
Keywords:
biomaterials / nanostructures / differential thermal analysis / electron microscopySource:
Materials Chemistry and Physics, 2008, 111, 1, 137-142
DOI: 10.1016/j.matchemphys.2008.03.045
ISSN: 0254-0584
WoS: 000257450300027
Scopus: 2-s2.0-44349139489
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VinčaTY - JOUR AU - Djosic, M. S. AU - Mišković-Stanković, Vesna B. AU - Milonjić, Slobodan K. AU - Kačarević-Popović, Zorica M. AU - Bibić, Nataša M. AU - Stojanovic, J. PY - 2008 UR - https://vinar.vin.bg.ac.rs/handle/123456789/3487 AB - Electrochemical synthesis of hydroxyapatite powders was performed galvanostatically from homogeneous solution of Na(2)H(2)EDTA center dot 2H(2)O, NaH2PO4 and CaCl2 at a concentration relationship Ca/EDTA/PO43- of 0.25/0.25/0.15 M at current densities of 137 and 207 mA cm(-2) and pH values of 9.0 and 12.0. The hydroxyapatite powders were characterized by X-ray diffraction, size distribution measurements, transmission electron microscopy, scanning electron microscopy and thermogravimetric and differential thermal analysis. The influence of the electrochemical synthesis parameters, e.g. applied current density and pH value, on the phase composition, crystallite size, morphology and thermal characteristics of hydroxyapatite powders were investigated. (c) 2008 Elsevier B.V. All rights reserved. T2 - Materials Chemistry and Physics T1 - Electrochemical synthesis and characterization of hydroxyapatite powders VL - 111 IS - 1 SP - 137 EP - 142 DO - 10.1016/j.matchemphys.2008.03.045 ER -
@article{ author = "Djosic, M. S. and Mišković-Stanković, Vesna B. and Milonjić, Slobodan K. and Kačarević-Popović, Zorica M. and Bibić, Nataša M. and Stojanovic, J.", year = "2008", abstract = "Electrochemical synthesis of hydroxyapatite powders was performed galvanostatically from homogeneous solution of Na(2)H(2)EDTA center dot 2H(2)O, NaH2PO4 and CaCl2 at a concentration relationship Ca/EDTA/PO43- of 0.25/0.25/0.15 M at current densities of 137 and 207 mA cm(-2) and pH values of 9.0 and 12.0. The hydroxyapatite powders were characterized by X-ray diffraction, size distribution measurements, transmission electron microscopy, scanning electron microscopy and thermogravimetric and differential thermal analysis. The influence of the electrochemical synthesis parameters, e.g. applied current density and pH value, on the phase composition, crystallite size, morphology and thermal characteristics of hydroxyapatite powders were investigated. (c) 2008 Elsevier B.V. All rights reserved.", journal = "Materials Chemistry and Physics", title = "Electrochemical synthesis and characterization of hydroxyapatite powders", volume = "111", number = "1", pages = "137-142", doi = "10.1016/j.matchemphys.2008.03.045" }
Djosic, M. S., Mišković-Stanković, V. B., Milonjić, S. K., Kačarević-Popović, Z. M., Bibić, N. M.,& Stojanovic, J.. (2008). Electrochemical synthesis and characterization of hydroxyapatite powders. in Materials Chemistry and Physics, 111(1), 137-142. https://doi.org/10.1016/j.matchemphys.2008.03.045
Djosic MS, Mišković-Stanković VB, Milonjić SK, Kačarević-Popović ZM, Bibić NM, Stojanovic J. Electrochemical synthesis and characterization of hydroxyapatite powders. in Materials Chemistry and Physics. 2008;111(1):137-142. doi:10.1016/j.matchemphys.2008.03.045 .
Djosic, M. S., Mišković-Stanković, Vesna B., Milonjić, Slobodan K., Kačarević-Popović, Zorica M., Bibić, Nataša M., Stojanovic, J., "Electrochemical synthesis and characterization of hydroxyapatite powders" in Materials Chemistry and Physics, 111, no. 1 (2008):137-142, https://doi.org/10.1016/j.matchemphys.2008.03.045 . .