Inorganic analysis of herbal drugs. Part I. Metal determination in herbal drugs originating from medicinal plants of the family Lamiacae
Апстракт
Elemental profiles of the total analyte content of major, minor and trace elements (Cu, Zn, Mn, Fe, K, Ca, Mg, Al, Ba and 13) in 8 herbal drugs, originating from medicinal plants of the family Lamiacae, were determined. Flame atomic absorption/emission spectroscopy (FAAS/FAES), inductively coupled plasma atomic emission spectroscopy (ICP-AES) and energy dispersive X-ray fluorescence (EDXRF) were applied, and the advantages and limitations of these techniques are also discussed. The whole procedure, from sample preparation via dissolution to the actual measurements, was validated byusing CRM (NIST 1573a-Tomato leaves). The recovery values obtained were in the range 90.64 - 101.58%. A high degree of similarity in their elemental profiles was noticed from the results of qualitative analysis, while quantitative analysis shows significant diversity due to the variety of the influencing sources. The medicinal plants investigated in this work contained Cu (5.92 - 14.79 mg kg(-1)), Zn (15.0 - ...43.0 mg kg(-1)), Mn (25 - 111 mg kg(-1)), Fe (74 - 546 mg kg(-1)), K (1.80 - 6.24 %), Ca (0.90 - 1.43 %), Mg (0. 17 - 0.67 %), Al (49 - 378 mg kg(-1)), Ba (15.53 - 69.84 mg kg(-1)) and B (34.7 - 56.5 mg kg(-1)).
Кључне речи:
major / minor and trace elements / FAAS / FAES / ICP-AES / EDXRF / herbal drugs / LamiacaeИзвор:
Journal of the Serbian Chemical Society, 2005, 70, 11, 1347-1355
DOI: 10.2298/JSC0511347R
ISSN: 0352-5139
WoS: 000234277000012
Scopus: 2-s2.0-31544475454
Колекције
Институција/група
VinčaTY - JOUR AU - Ražić, Slavica AU - Đogo, Svetlana AU - Slavković, Latinka J. AU - Popović, Aleksandar R. PY - 2005 UR - https://vinar.vin.bg.ac.rs/handle/123456789/2961 AB - Elemental profiles of the total analyte content of major, minor and trace elements (Cu, Zn, Mn, Fe, K, Ca, Mg, Al, Ba and 13) in 8 herbal drugs, originating from medicinal plants of the family Lamiacae, were determined. Flame atomic absorption/emission spectroscopy (FAAS/FAES), inductively coupled plasma atomic emission spectroscopy (ICP-AES) and energy dispersive X-ray fluorescence (EDXRF) were applied, and the advantages and limitations of these techniques are also discussed. The whole procedure, from sample preparation via dissolution to the actual measurements, was validated byusing CRM (NIST 1573a-Tomato leaves). The recovery values obtained were in the range 90.64 - 101.58%. A high degree of similarity in their elemental profiles was noticed from the results of qualitative analysis, while quantitative analysis shows significant diversity due to the variety of the influencing sources. The medicinal plants investigated in this work contained Cu (5.92 - 14.79 mg kg(-1)), Zn (15.0 - 43.0 mg kg(-1)), Mn (25 - 111 mg kg(-1)), Fe (74 - 546 mg kg(-1)), K (1.80 - 6.24 %), Ca (0.90 - 1.43 %), Mg (0. 17 - 0.67 %), Al (49 - 378 mg kg(-1)), Ba (15.53 - 69.84 mg kg(-1)) and B (34.7 - 56.5 mg kg(-1)). T2 - Journal of the Serbian Chemical Society T1 - Inorganic analysis of herbal drugs. Part I. Metal determination in herbal drugs originating from medicinal plants of the family Lamiacae VL - 70 IS - 11 SP - 1347 EP - 1355 DO - 10.2298/JSC0511347R ER -
@article{ author = "Ražić, Slavica and Đogo, Svetlana and Slavković, Latinka J. and Popović, Aleksandar R.", year = "2005", abstract = "Elemental profiles of the total analyte content of major, minor and trace elements (Cu, Zn, Mn, Fe, K, Ca, Mg, Al, Ba and 13) in 8 herbal drugs, originating from medicinal plants of the family Lamiacae, were determined. Flame atomic absorption/emission spectroscopy (FAAS/FAES), inductively coupled plasma atomic emission spectroscopy (ICP-AES) and energy dispersive X-ray fluorescence (EDXRF) were applied, and the advantages and limitations of these techniques are also discussed. The whole procedure, from sample preparation via dissolution to the actual measurements, was validated byusing CRM (NIST 1573a-Tomato leaves). The recovery values obtained were in the range 90.64 - 101.58%. A high degree of similarity in their elemental profiles was noticed from the results of qualitative analysis, while quantitative analysis shows significant diversity due to the variety of the influencing sources. The medicinal plants investigated in this work contained Cu (5.92 - 14.79 mg kg(-1)), Zn (15.0 - 43.0 mg kg(-1)), Mn (25 - 111 mg kg(-1)), Fe (74 - 546 mg kg(-1)), K (1.80 - 6.24 %), Ca (0.90 - 1.43 %), Mg (0. 17 - 0.67 %), Al (49 - 378 mg kg(-1)), Ba (15.53 - 69.84 mg kg(-1)) and B (34.7 - 56.5 mg kg(-1)).", journal = "Journal of the Serbian Chemical Society", title = "Inorganic analysis of herbal drugs. Part I. Metal determination in herbal drugs originating from medicinal plants of the family Lamiacae", volume = "70", number = "11", pages = "1347-1355", doi = "10.2298/JSC0511347R" }
Ražić, S., Đogo, S., Slavković, L. J.,& Popović, A. R.. (2005). Inorganic analysis of herbal drugs. Part I. Metal determination in herbal drugs originating from medicinal plants of the family Lamiacae. in Journal of the Serbian Chemical Society, 70(11), 1347-1355. https://doi.org/10.2298/JSC0511347R
Ražić S, Đogo S, Slavković LJ, Popović AR. Inorganic analysis of herbal drugs. Part I. Metal determination in herbal drugs originating from medicinal plants of the family Lamiacae. in Journal of the Serbian Chemical Society. 2005;70(11):1347-1355. doi:10.2298/JSC0511347R .
Ražić, Slavica, Đogo, Svetlana, Slavković, Latinka J., Popović, Aleksandar R., "Inorganic analysis of herbal drugs. Part I. Metal determination in herbal drugs originating from medicinal plants of the family Lamiacae" in Journal of the Serbian Chemical Society, 70, no. 11 (2005):1347-1355, https://doi.org/10.2298/JSC0511347R . .