Mechanochemical synthesis of nanostructured fluorapatite/fluorhydroxyapatite and carbonated fluorapatite/fluorhydroxyapatite
Nema prikaza
Autori
Nikcevic, IJokanović, Vukoman R.
Mitrić, Miodrag
Nedić, Zoran
Makovec, Darko
Uskoković, Dragan
Članak u časopisu
Metapodaci
Prikaz svih podataka o dokumentuApstrakt
Powder mixture of Ca(OH)(2)-P2O5-CaF2 were milled in planetary ball mill. A carbonated fluorhydroxyapatite, FHA Ca-10(PO4)(1-y)(CO3)(y)(PO4)(5)(OH)(2-2x1)(F)(2x1) was formed after 5 h of milling and carbonated fluoroapatite Ca-10(PO4)(1-y)(CO3)(y)(PO4)(5)(F)(2) was formed after 9 h of milling. Complete transformation of the carbonated form of FA into then single phase of FA occurred after 9 h milling and thermally treating. The various experimental techniques like X-ray Diffraction (XRD), Differential Thermal Analysis (DTA), Infrared Spectroscopy (IR), Transmission Electron Microscopy and Scanning Electron Microscopy (SEM) were used to characterize the synthesized powders and to postulate reaction mechanisms steps- transformations of reactants involved. (C) 2004 Elsevier Inc. All rights reserved.
Ključne reči:
fluorapatitie / carbonated fluorhydroxyapatite / hydroxyapatite / mechanochemical synthesisIzvor:
Journal of Solid State Chemistry, 2004, 177, 7, 2565-2574
DOI: 10.1016/j.jssc.2004.03.024
ISSN: 0022-4596
WoS: 000222314700047
Scopus: 2-s2.0-2942654770
Kolekcije
Institucija/grupa
VinčaTY - JOUR AU - Nikcevic, I AU - Jokanović, Vukoman R. AU - Mitrić, Miodrag AU - Nedić, Zoran AU - Makovec, Darko AU - Uskoković, Dragan PY - 2004 UR - https://vinar.vin.bg.ac.rs/handle/123456789/2778 AB - Powder mixture of Ca(OH)(2)-P2O5-CaF2 were milled in planetary ball mill. A carbonated fluorhydroxyapatite, FHA Ca-10(PO4)(1-y)(CO3)(y)(PO4)(5)(OH)(2-2x1)(F)(2x1) was formed after 5 h of milling and carbonated fluoroapatite Ca-10(PO4)(1-y)(CO3)(y)(PO4)(5)(F)(2) was formed after 9 h of milling. Complete transformation of the carbonated form of FA into then single phase of FA occurred after 9 h milling and thermally treating. The various experimental techniques like X-ray Diffraction (XRD), Differential Thermal Analysis (DTA), Infrared Spectroscopy (IR), Transmission Electron Microscopy and Scanning Electron Microscopy (SEM) were used to characterize the synthesized powders and to postulate reaction mechanisms steps- transformations of reactants involved. (C) 2004 Elsevier Inc. All rights reserved. T2 - Journal of Solid State Chemistry T1 - Mechanochemical synthesis of nanostructured fluorapatite/fluorhydroxyapatite and carbonated fluorapatite/fluorhydroxyapatite VL - 177 IS - 7 SP - 2565 EP - 2574 DO - 10.1016/j.jssc.2004.03.024 ER -
@article{ author = "Nikcevic, I and Jokanović, Vukoman R. and Mitrić, Miodrag and Nedić, Zoran and Makovec, Darko and Uskoković, Dragan", year = "2004", abstract = "Powder mixture of Ca(OH)(2)-P2O5-CaF2 were milled in planetary ball mill. A carbonated fluorhydroxyapatite, FHA Ca-10(PO4)(1-y)(CO3)(y)(PO4)(5)(OH)(2-2x1)(F)(2x1) was formed after 5 h of milling and carbonated fluoroapatite Ca-10(PO4)(1-y)(CO3)(y)(PO4)(5)(F)(2) was formed after 9 h of milling. Complete transformation of the carbonated form of FA into then single phase of FA occurred after 9 h milling and thermally treating. The various experimental techniques like X-ray Diffraction (XRD), Differential Thermal Analysis (DTA), Infrared Spectroscopy (IR), Transmission Electron Microscopy and Scanning Electron Microscopy (SEM) were used to characterize the synthesized powders and to postulate reaction mechanisms steps- transformations of reactants involved. (C) 2004 Elsevier Inc. All rights reserved.", journal = "Journal of Solid State Chemistry", title = "Mechanochemical synthesis of nanostructured fluorapatite/fluorhydroxyapatite and carbonated fluorapatite/fluorhydroxyapatite", volume = "177", number = "7", pages = "2565-2574", doi = "10.1016/j.jssc.2004.03.024" }
Nikcevic, I., Jokanović, V. R., Mitrić, M., Nedić, Z., Makovec, D.,& Uskoković, D.. (2004). Mechanochemical synthesis of nanostructured fluorapatite/fluorhydroxyapatite and carbonated fluorapatite/fluorhydroxyapatite. in Journal of Solid State Chemistry, 177(7), 2565-2574. https://doi.org/10.1016/j.jssc.2004.03.024
Nikcevic I, Jokanović VR, Mitrić M, Nedić Z, Makovec D, Uskoković D. Mechanochemical synthesis of nanostructured fluorapatite/fluorhydroxyapatite and carbonated fluorapatite/fluorhydroxyapatite. in Journal of Solid State Chemistry. 2004;177(7):2565-2574. doi:10.1016/j.jssc.2004.03.024 .
Nikcevic, I, Jokanović, Vukoman R., Mitrić, Miodrag, Nedić, Zoran, Makovec, Darko, Uskoković, Dragan, "Mechanochemical synthesis of nanostructured fluorapatite/fluorhydroxyapatite and carbonated fluorapatite/fluorhydroxyapatite" in Journal of Solid State Chemistry, 177, no. 7 (2004):2565-2574, https://doi.org/10.1016/j.jssc.2004.03.024 . .