Validation and uncertainty estimation of UPLC-PDA method for the analysis of polycyclic aromatic hydrocarbons in concrete
Само за регистроване кориснике
2017
Аутори
Aćimović, Danka D.Nikolić, Željka
Tošić, Miloš S.
Milovanović, Dubravka S.
Nikolić, Vladimir M.
Brdarić, Tanja
Marčeta Kaninski, Milica
Чланак у часопису (Објављена верзија)
Метаподаци
Приказ свих података о документуАпстракт
Human exposure to persistent organic contaminants, from building materials, negatively affects peoples health and overall quality of life. This paper presents the validation and uncertainty assessment of the analytical method, developed for the simultaneous determination of 16 EPA polycyclic aromatic hydrocarbons (PAHs) in solid-solid concrete by ultra-performance liquid chromatography with photo diode-array detector. Linearity of calibration curves was good over the whole range of calibration. Limits of detection varied between 0.2 and 2.9 mu gkg(-1). The accuracy in terms of recovery of the validated method is within the range from 54 to 106%. The developed method proved to be appropriate for analysis of PAHs and can be used for the quality control testing of concrete during the construction of new buildings, the old residences and related buildings associated with sick-building syndrome. In addition, this is the first reported method described for the evaluation of PAHs in solid-sol...id concrete. (C) 2016 Elsevier B.V. All rights reserved.
Кључне речи:
Concrete / PAH / Uncertainty / Validation / UPLC-PDA / Building materialsИзвор:
Journal of Hazardous Materials, 2017, 325, 271-278Финансирање / пројекти:
- Водонична енергија - развој нових материјала: електролитичко добијање водоника, водоничне горивне ћелије, изотопски ефекти (RS-172045)
- Испитивање и верификација метода за мултидисциплинарне форензичке анализе у функцији непролиферације оружја за масовно уништење (RS-37021)
DOI: 10.1016/j.jhazmat.2016.12.008
ISSN: 0304-3894; 1873-3336
PubMed: 27940116
WoS: 000392165700027
Scopus: 2-s2.0-85003828415
Колекције
Институција/група
VinčaTY - JOUR AU - Aćimović, Danka D. AU - Nikolić, Željka AU - Tošić, Miloš S. AU - Milovanović, Dubravka S. AU - Nikolić, Vladimir M. AU - Brdarić, Tanja AU - Marčeta Kaninski, Milica PY - 2017 UR - https://vinar.vin.bg.ac.rs/handle/123456789/1390 AB - Human exposure to persistent organic contaminants, from building materials, negatively affects peoples health and overall quality of life. This paper presents the validation and uncertainty assessment of the analytical method, developed for the simultaneous determination of 16 EPA polycyclic aromatic hydrocarbons (PAHs) in solid-solid concrete by ultra-performance liquid chromatography with photo diode-array detector. Linearity of calibration curves was good over the whole range of calibration. Limits of detection varied between 0.2 and 2.9 mu gkg(-1). The accuracy in terms of recovery of the validated method is within the range from 54 to 106%. The developed method proved to be appropriate for analysis of PAHs and can be used for the quality control testing of concrete during the construction of new buildings, the old residences and related buildings associated with sick-building syndrome. In addition, this is the first reported method described for the evaluation of PAHs in solid-solid concrete. (C) 2016 Elsevier B.V. All rights reserved. T2 - Journal of Hazardous Materials T1 - Validation and uncertainty estimation of UPLC-PDA method for the analysis of polycyclic aromatic hydrocarbons in concrete VL - 325 SP - 271 EP - 278 DO - 10.1016/j.jhazmat.2016.12.008 ER -
@article{ author = "Aćimović, Danka D. and Nikolić, Željka and Tošić, Miloš S. and Milovanović, Dubravka S. and Nikolić, Vladimir M. and Brdarić, Tanja and Marčeta Kaninski, Milica", year = "2017", abstract = "Human exposure to persistent organic contaminants, from building materials, negatively affects peoples health and overall quality of life. This paper presents the validation and uncertainty assessment of the analytical method, developed for the simultaneous determination of 16 EPA polycyclic aromatic hydrocarbons (PAHs) in solid-solid concrete by ultra-performance liquid chromatography with photo diode-array detector. Linearity of calibration curves was good over the whole range of calibration. Limits of detection varied between 0.2 and 2.9 mu gkg(-1). The accuracy in terms of recovery of the validated method is within the range from 54 to 106%. The developed method proved to be appropriate for analysis of PAHs and can be used for the quality control testing of concrete during the construction of new buildings, the old residences and related buildings associated with sick-building syndrome. In addition, this is the first reported method described for the evaluation of PAHs in solid-solid concrete. (C) 2016 Elsevier B.V. All rights reserved.", journal = "Journal of Hazardous Materials", title = "Validation and uncertainty estimation of UPLC-PDA method for the analysis of polycyclic aromatic hydrocarbons in concrete", volume = "325", pages = "271-278", doi = "10.1016/j.jhazmat.2016.12.008" }
Aćimović, D. D., Nikolić, Ž., Tošić, M. S., Milovanović, D. S., Nikolić, V. M., Brdarić, T.,& Marčeta Kaninski, M.. (2017). Validation and uncertainty estimation of UPLC-PDA method for the analysis of polycyclic aromatic hydrocarbons in concrete. in Journal of Hazardous Materials, 325, 271-278. https://doi.org/10.1016/j.jhazmat.2016.12.008
Aćimović DD, Nikolić Ž, Tošić MS, Milovanović DS, Nikolić VM, Brdarić T, Marčeta Kaninski M. Validation and uncertainty estimation of UPLC-PDA method for the analysis of polycyclic aromatic hydrocarbons in concrete. in Journal of Hazardous Materials. 2017;325:271-278. doi:10.1016/j.jhazmat.2016.12.008 .
Aćimović, Danka D., Nikolić, Željka, Tošić, Miloš S., Milovanović, Dubravka S., Nikolić, Vladimir M., Brdarić, Tanja, Marčeta Kaninski, Milica, "Validation and uncertainty estimation of UPLC-PDA method for the analysis of polycyclic aromatic hydrocarbons in concrete" in Journal of Hazardous Materials, 325 (2017):271-278, https://doi.org/10.1016/j.jhazmat.2016.12.008 . .