Solvothermal synthesis of magnetite nanoparticles suitable for application in magnetic hyperthermia
2015
Preuzimanje 🢃
Autori
Nikolić, VioletaMraković, Ana
Perović, Marija
Bošković, Marko
Spasojević, Vojislav
Kusigerski, Vladan
Blanuša, Jovan
Konferencijski prilog (Objavljena verzija)
Metapodaci
Prikaz svih podataka o dokumentuApstrakt
In this paper, spherical Fe3O4@OA nanoparticles were prepared via solvothermal method, in which iron sulphate, sodium hydroxide and oleic acid were used as precursors. The main idea of this research was to develop the method for preparation of nanoparticles with magnetic properties suitable for application in magnetic hyperthermia. We have tried to tailor size, shape and the degree of interparticle interactions by varying experimental conditions during the synthesis route. Obtained samples were structurally and magnetically characterized by means of different experimental probes such as: X-ray diffraction, SQUID magnetometry, FTIR and Mossbauer spectroscopy. Structural characterization asserts that the obtained phase is magnetite, Fe3O4, while FTIR spectra support the presence of oleic acid coating on the particle surface. Detailed magnetic characterization done by SQUID measurements and Mossbauer spectroscopy confirmed the presence of the strong and weak interactions in the nanopartic...les system, depending on the synthesis conditions.
Izvor:
11th Conference for Young Scientists in Ceramics (SM-2015, and ESR Workshop, COST MP1208) : programme and the book of abstracts, 2015, 35-36Izdavač:
- University of Novi Sad : Faculty of Technology
Napomena:
- 11th Conference for Young Scientists in Ceramics (SM-2015, and ESR Workshop, COST MP1208) : programme and the book of abstracts, October 21-24, Novi Sad
Kolekcije
Institucija/grupa
VinčaTY - CONF AU - Nikolić, Violeta AU - Mraković, Ana AU - Perović, Marija AU - Bošković, Marko AU - Spasojević, Vojislav AU - Kusigerski, Vladan AU - Blanuša, Jovan PY - 2015 UR - https://vinar.vin.bg.ac.rs/handle/123456789/13209 AB - In this paper, spherical Fe3O4@OA nanoparticles were prepared via solvothermal method, in which iron sulphate, sodium hydroxide and oleic acid were used as precursors. The main idea of this research was to develop the method for preparation of nanoparticles with magnetic properties suitable for application in magnetic hyperthermia. We have tried to tailor size, shape and the degree of interparticle interactions by varying experimental conditions during the synthesis route. Obtained samples were structurally and magnetically characterized by means of different experimental probes such as: X-ray diffraction, SQUID magnetometry, FTIR and Mossbauer spectroscopy. Structural characterization asserts that the obtained phase is magnetite, Fe3O4, while FTIR spectra support the presence of oleic acid coating on the particle surface. Detailed magnetic characterization done by SQUID measurements and Mossbauer spectroscopy confirmed the presence of the strong and weak interactions in the nanoparticles system, depending on the synthesis conditions. PB - University of Novi Sad : Faculty of Technology C3 - 11th Conference for Young Scientists in Ceramics (SM-2015, and ESR Workshop, COST MP1208) : programme and the book of abstracts T1 - Solvothermal synthesis of magnetite nanoparticles suitable for application in magnetic hyperthermia SP - 35 EP - 36 UR - https://hdl.handle.net/21.15107/rcub_vinar_13209 ER -
@conference{ author = "Nikolić, Violeta and Mraković, Ana and Perović, Marija and Bošković, Marko and Spasojević, Vojislav and Kusigerski, Vladan and Blanuša, Jovan", year = "2015", abstract = "In this paper, spherical Fe3O4@OA nanoparticles were prepared via solvothermal method, in which iron sulphate, sodium hydroxide and oleic acid were used as precursors. The main idea of this research was to develop the method for preparation of nanoparticles with magnetic properties suitable for application in magnetic hyperthermia. We have tried to tailor size, shape and the degree of interparticle interactions by varying experimental conditions during the synthesis route. Obtained samples were structurally and magnetically characterized by means of different experimental probes such as: X-ray diffraction, SQUID magnetometry, FTIR and Mossbauer spectroscopy. Structural characterization asserts that the obtained phase is magnetite, Fe3O4, while FTIR spectra support the presence of oleic acid coating on the particle surface. Detailed magnetic characterization done by SQUID measurements and Mossbauer spectroscopy confirmed the presence of the strong and weak interactions in the nanoparticles system, depending on the synthesis conditions.", publisher = "University of Novi Sad : Faculty of Technology", journal = "11th Conference for Young Scientists in Ceramics (SM-2015, and ESR Workshop, COST MP1208) : programme and the book of abstracts", title = "Solvothermal synthesis of magnetite nanoparticles suitable for application in magnetic hyperthermia", pages = "35-36", url = "https://hdl.handle.net/21.15107/rcub_vinar_13209" }
Nikolić, V., Mraković, A., Perović, M., Bošković, M., Spasojević, V., Kusigerski, V.,& Blanuša, J.. (2015). Solvothermal synthesis of magnetite nanoparticles suitable for application in magnetic hyperthermia. in 11th Conference for Young Scientists in Ceramics (SM-2015, and ESR Workshop, COST MP1208) : programme and the book of abstracts University of Novi Sad : Faculty of Technology., 35-36. https://hdl.handle.net/21.15107/rcub_vinar_13209
Nikolić V, Mraković A, Perović M, Bošković M, Spasojević V, Kusigerski V, Blanuša J. Solvothermal synthesis of magnetite nanoparticles suitable for application in magnetic hyperthermia. in 11th Conference for Young Scientists in Ceramics (SM-2015, and ESR Workshop, COST MP1208) : programme and the book of abstracts. 2015;:35-36. https://hdl.handle.net/21.15107/rcub_vinar_13209 .
Nikolić, Violeta, Mraković, Ana, Perović, Marija, Bošković, Marko, Spasojević, Vojislav, Kusigerski, Vladan, Blanuša, Jovan, "Solvothermal synthesis of magnetite nanoparticles suitable for application in magnetic hyperthermia" in 11th Conference for Young Scientists in Ceramics (SM-2015, and ESR Workshop, COST MP1208) : programme and the book of abstracts (2015):35-36, https://hdl.handle.net/21.15107/rcub_vinar_13209 .