Sinteza i karakterizacija nanostrukturnog Ca0.9 Er0.1 MnO3
Synthesis and characterization of nanostructured Ca0.9Er0.1MnO3
2023
Preuzimanje 🢃
Autori
Vlašković, TijanaLaban, Bojana
Milošević, Maja
Čebela, Maria
Dodevski, Vladimir
Rosić, Milena
Konferencijski prilog (Objavljena verzija)
Metapodaci
Prikaz svih podataka o dokumentuApstrakt
Nanostrukturni Ca0.9Er0.1MnO3 je sintetisan saharoza-nitratnon procedurom (SNP). Tokom ove metode sagorevanja su korišćene sledeće hemikalije: saharoza C12H22O11 koja ima dvostruku ulogu i goriva i kompleksanta, kalcijum-nitrat tetrahidrat, mangan(II)-nitrat hidrat i erbijum(III)-nitrat pentahidrat. Nitrati metala i saharoza su kombinovani u njihovim odgovarajućim stehiometrijskim odnosima da bi se pripremio složeni oksid perovskitske nanostrukture. Dobijeni prah Ca0.9Er0.1MnO3 je kalcinisan u temperaturnom opsegu od 800-1000°C tokom 15 min. Ispitani su veličina čestica, parametri rešetke, strukturne promene i površina. Za karakterizaciju sintetisanih uzoraka korišćena je diferencijalno termijska analiza (DTA), rendgenska difrakciona analiza (XRD), Furijeova transformaciona infracrvena spektroskopija (FTIR) i skenirajuća elektronska mikroskopija (SEM).
Nanostructured Ca0.9Er0.1MnO3 was synthesized by the sucrose-nitrate procedure (SNP). During this combustion method, sucrose C12H22O11 which is both fuel and complexant and metal ions in the form of calcium nitrate tetrahydrate, manganese(II) nitrate hydrate, erbium(III) nitrate pentahydrate were used. Metal nitrates and sucrose were combined to prepare this nanostructured in their appropriate stoichiometric ratios. Obtained Ca0,9Er0,1MnO3 powder was calcined in a temperature range of 800-1000 °C for 15min. Particle size, lattice parameters, structural changes, and specific surface area were investigated. DTA, X-ray diffraction (XRD), FTIR, and Field emission scanning electron microscopy (SEM) were used to characterize the synthesized samples at room temperature.
Izvor:
59th Meeting of the Serbian Chemical Society : Book of Abstracts, Proceedings, 2023, 95-95Izdavač:
- Belgrade : Serbian Chemical Society
Finansiranje / projekti:
- Ministarstvo nauke, tehnološkog razvoja i inovacija Republike Srbije, institucionalno finansiranje - 200123 (Univerzitet u Prištini sa privremenim sedištem u Kosovskoj Mitrovici, Prirodno-matematički fakultet) (RS-MESTD-inst-2020-200123)
Napomena:
- 59th Meeting of the Serbian Chemical Society; June 1-2, 2023, Novi Sad, Serbia
Kolekcije
Institucija/grupa
VinčaTY - CONF AU - Vlašković, Tijana AU - Laban, Bojana AU - Milošević, Maja AU - Čebela, Maria AU - Dodevski, Vladimir AU - Rosić, Milena PY - 2023 UR - https://vinar.vin.bg.ac.rs/handle/123456789/13035 AB - Nanostrukturni Ca0.9Er0.1MnO3 je sintetisan saharoza-nitratnon procedurom (SNP). Tokom ove metode sagorevanja su korišćene sledeće hemikalije: saharoza C12H22O11 koja ima dvostruku ulogu i goriva i kompleksanta, kalcijum-nitrat tetrahidrat, mangan(II)-nitrat hidrat i erbijum(III)-nitrat pentahidrat. Nitrati metala i saharoza su kombinovani u njihovim odgovarajućim stehiometrijskim odnosima da bi se pripremio složeni oksid perovskitske nanostrukture. Dobijeni prah Ca0.9Er0.1MnO3 je kalcinisan u temperaturnom opsegu od 800-1000°C tokom 15 min. Ispitani su veličina čestica, parametri rešetke, strukturne promene i površina. Za karakterizaciju sintetisanih uzoraka korišćena je diferencijalno termijska analiza (DTA), rendgenska difrakciona analiza (XRD), Furijeova transformaciona infracrvena spektroskopija (FTIR) i skenirajuća elektronska mikroskopija (SEM). AB - Nanostructured Ca0.9Er0.1MnO3 was synthesized by the sucrose-nitrate procedure (SNP). During this combustion method, sucrose C12H22O11 which is both fuel and complexant and metal ions in the form of calcium nitrate tetrahydrate, manganese(II) nitrate hydrate, erbium(III) nitrate pentahydrate were used. Metal nitrates and sucrose were combined to prepare this nanostructured in their appropriate stoichiometric ratios. Obtained Ca0,9Er0,1MnO3 powder was calcined in a temperature range of 800-1000 °C for 15min. Particle size, lattice parameters, structural changes, and specific surface area were investigated. DTA, X-ray diffraction (XRD), FTIR, and Field emission scanning electron microscopy (SEM) were used to characterize the synthesized samples at room temperature. PB - Belgrade : Serbian Chemical Society C3 - 59th Meeting of the Serbian Chemical Society : Book of Abstracts, Proceedings T1 - Sinteza i karakterizacija nanostrukturnog Ca0.9 Er0.1 MnO3 T1 - Synthesis and characterization of nanostructured Ca0.9Er0.1MnO3 SP - 95 EP - 95 UR - https://hdl.handle.net/21.15107/rcub_vinar_13035 ER -
@conference{ author = "Vlašković, Tijana and Laban, Bojana and Milošević, Maja and Čebela, Maria and Dodevski, Vladimir and Rosić, Milena", year = "2023", abstract = "Nanostrukturni Ca0.9Er0.1MnO3 je sintetisan saharoza-nitratnon procedurom (SNP). Tokom ove metode sagorevanja su korišćene sledeće hemikalije: saharoza C12H22O11 koja ima dvostruku ulogu i goriva i kompleksanta, kalcijum-nitrat tetrahidrat, mangan(II)-nitrat hidrat i erbijum(III)-nitrat pentahidrat. Nitrati metala i saharoza su kombinovani u njihovim odgovarajućim stehiometrijskim odnosima da bi se pripremio složeni oksid perovskitske nanostrukture. Dobijeni prah Ca0.9Er0.1MnO3 je kalcinisan u temperaturnom opsegu od 800-1000°C tokom 15 min. Ispitani su veličina čestica, parametri rešetke, strukturne promene i površina. Za karakterizaciju sintetisanih uzoraka korišćena je diferencijalno termijska analiza (DTA), rendgenska difrakciona analiza (XRD), Furijeova transformaciona infracrvena spektroskopija (FTIR) i skenirajuća elektronska mikroskopija (SEM)., Nanostructured Ca0.9Er0.1MnO3 was synthesized by the sucrose-nitrate procedure (SNP). During this combustion method, sucrose C12H22O11 which is both fuel and complexant and metal ions in the form of calcium nitrate tetrahydrate, manganese(II) nitrate hydrate, erbium(III) nitrate pentahydrate were used. Metal nitrates and sucrose were combined to prepare this nanostructured in their appropriate stoichiometric ratios. Obtained Ca0,9Er0,1MnO3 powder was calcined in a temperature range of 800-1000 °C for 15min. Particle size, lattice parameters, structural changes, and specific surface area were investigated. DTA, X-ray diffraction (XRD), FTIR, and Field emission scanning electron microscopy (SEM) were used to characterize the synthesized samples at room temperature.", publisher = "Belgrade : Serbian Chemical Society", journal = "59th Meeting of the Serbian Chemical Society : Book of Abstracts, Proceedings", title = "Sinteza i karakterizacija nanostrukturnog Ca0.9 Er0.1 MnO3, Synthesis and characterization of nanostructured Ca0.9Er0.1MnO3", pages = "95-95", url = "https://hdl.handle.net/21.15107/rcub_vinar_13035" }
Vlašković, T., Laban, B., Milošević, M., Čebela, M., Dodevski, V.,& Rosić, M.. (2023). Sinteza i karakterizacija nanostrukturnog Ca0.9 Er0.1 MnO3. in 59th Meeting of the Serbian Chemical Society : Book of Abstracts, Proceedings Belgrade : Serbian Chemical Society., 95-95. https://hdl.handle.net/21.15107/rcub_vinar_13035
Vlašković T, Laban B, Milošević M, Čebela M, Dodevski V, Rosić M. Sinteza i karakterizacija nanostrukturnog Ca0.9 Er0.1 MnO3. in 59th Meeting of the Serbian Chemical Society : Book of Abstracts, Proceedings. 2023;:95-95. https://hdl.handle.net/21.15107/rcub_vinar_13035 .
Vlašković, Tijana, Laban, Bojana, Milošević, Maja, Čebela, Maria, Dodevski, Vladimir, Rosić, Milena, "Sinteza i karakterizacija nanostrukturnog Ca0.9 Er0.1 MnO3" in 59th Meeting of the Serbian Chemical Society : Book of Abstracts, Proceedings (2023):95-95, https://hdl.handle.net/21.15107/rcub_vinar_13035 .