Surface structural heterogeneity of high power plasma-sprayed hydroxyapatite coatings
Samo za registrovane korisnike
2016
Autori
Gligorijević, Bojan R.Vilotijević, Miroljub N.
Šćepanović, Maja
Vidovic, Dragoslav
Radović, Nenad A.
Članak u časopisu (Objavljena verzija)
,
© 2016 Elsevier B.V.
Metapodaci
Prikaz svih podataka o dokumentuApstrakt
The aim of this work was to examine the dependence of the local surface structure (surface structural heterogeneity) on the local thickness (thickness uniformity) and structure properties along the thickness of hydroxyapatite coatings (HACs) deposited by using the high power (52 kW) laminar plasma jet. For the deposition process, a relatively small size of the feedstock hydroxyapatite powder (HAP) (33 mu m) was used. The HACs were deposited at different stand-off distances (SODs) (80, 100, and 150 mm) without preheating of substrates. The thickness measurements were performed by using the calibrated micrometer and light microscopy (LM). The surface micro-structure was analyzed by using the micro-Raman spectroscopy (MRS), whereas the micro-structure along the thickness of HACs was studied by using the MRS, X-ray powder diffractometry (XRPD), and LM (combined with chemical etching). The results showed a heterogeneous phase distribution on the surface of each HAC analyzed as well as the n...on-uniform thickness of HACs. Apparently, a correlation existed between the local surface structure and the local thickness of HACs. However, the MRS, XRPD, and LM analyses of micro-structure along the thickness of HACs indicated that the differences in the local surface structure could be related to the different recrystallization established during the plasma deposition process in the different parts along the thickness of each HAC analyzed. (C) 2016 Elsevier B.V. All rights reserved.
Ključne reči:
Hydroxyapatite coatings / Plasma spraying / Surface structure / Thickness / Micro-Raman spectroscopyIzvor:
Journal of Alloys and Compounds, 2016, 687, 421-430Finansiranje / projekti:
- Sinteza dijamantskih prevlaka iz plamena ugljovodonika tehnikom ravnog plamena (RS-MESTD-Technological Development (TD or TR)-34022)
- Plasma Jet Co, Serbia
DOI: 10.1016/j.jallcom.2016.06.163
ISSN: 0925-8388; 1873-4669
WoS: 000383525400056
Scopus: 2-s2.0-84975893276
Kolekcije
Institucija/grupa
VinčaTY - JOUR AU - Gligorijević, Bojan R. AU - Vilotijević, Miroljub N. AU - Šćepanović, Maja AU - Vidovic, Dragoslav AU - Radović, Nenad A. PY - 2016 UR - https://vinar.vin.bg.ac.rs/handle/123456789/1245 AB - The aim of this work was to examine the dependence of the local surface structure (surface structural heterogeneity) on the local thickness (thickness uniformity) and structure properties along the thickness of hydroxyapatite coatings (HACs) deposited by using the high power (52 kW) laminar plasma jet. For the deposition process, a relatively small size of the feedstock hydroxyapatite powder (HAP) (33 mu m) was used. The HACs were deposited at different stand-off distances (SODs) (80, 100, and 150 mm) without preheating of substrates. The thickness measurements were performed by using the calibrated micrometer and light microscopy (LM). The surface micro-structure was analyzed by using the micro-Raman spectroscopy (MRS), whereas the micro-structure along the thickness of HACs was studied by using the MRS, X-ray powder diffractometry (XRPD), and LM (combined with chemical etching). The results showed a heterogeneous phase distribution on the surface of each HAC analyzed as well as the non-uniform thickness of HACs. Apparently, a correlation existed between the local surface structure and the local thickness of HACs. However, the MRS, XRPD, and LM analyses of micro-structure along the thickness of HACs indicated that the differences in the local surface structure could be related to the different recrystallization established during the plasma deposition process in the different parts along the thickness of each HAC analyzed. (C) 2016 Elsevier B.V. All rights reserved. T2 - Journal of Alloys and Compounds T1 - Surface structural heterogeneity of high power plasma-sprayed hydroxyapatite coatings VL - 687 SP - 421 EP - 430 DO - 10.1016/j.jallcom.2016.06.163 ER -
@article{ author = "Gligorijević, Bojan R. and Vilotijević, Miroljub N. and Šćepanović, Maja and Vidovic, Dragoslav and Radović, Nenad A.", year = "2016", abstract = "The aim of this work was to examine the dependence of the local surface structure (surface structural heterogeneity) on the local thickness (thickness uniformity) and structure properties along the thickness of hydroxyapatite coatings (HACs) deposited by using the high power (52 kW) laminar plasma jet. For the deposition process, a relatively small size of the feedstock hydroxyapatite powder (HAP) (33 mu m) was used. The HACs were deposited at different stand-off distances (SODs) (80, 100, and 150 mm) without preheating of substrates. The thickness measurements were performed by using the calibrated micrometer and light microscopy (LM). The surface micro-structure was analyzed by using the micro-Raman spectroscopy (MRS), whereas the micro-structure along the thickness of HACs was studied by using the MRS, X-ray powder diffractometry (XRPD), and LM (combined with chemical etching). The results showed a heterogeneous phase distribution on the surface of each HAC analyzed as well as the non-uniform thickness of HACs. Apparently, a correlation existed between the local surface structure and the local thickness of HACs. However, the MRS, XRPD, and LM analyses of micro-structure along the thickness of HACs indicated that the differences in the local surface structure could be related to the different recrystallization established during the plasma deposition process in the different parts along the thickness of each HAC analyzed. (C) 2016 Elsevier B.V. All rights reserved.", journal = "Journal of Alloys and Compounds", title = "Surface structural heterogeneity of high power plasma-sprayed hydroxyapatite coatings", volume = "687", pages = "421-430", doi = "10.1016/j.jallcom.2016.06.163" }
Gligorijević, B. R., Vilotijević, M. N., Šćepanović, M., Vidovic, D.,& Radović, N. A.. (2016). Surface structural heterogeneity of high power plasma-sprayed hydroxyapatite coatings. in Journal of Alloys and Compounds, 687, 421-430. https://doi.org/10.1016/j.jallcom.2016.06.163
Gligorijević BR, Vilotijević MN, Šćepanović M, Vidovic D, Radović NA. Surface structural heterogeneity of high power plasma-sprayed hydroxyapatite coatings. in Journal of Alloys and Compounds. 2016;687:421-430. doi:10.1016/j.jallcom.2016.06.163 .
Gligorijević, Bojan R., Vilotijević, Miroljub N., Šćepanović, Maja, Vidovic, Dragoslav, Radović, Nenad A., "Surface structural heterogeneity of high power plasma-sprayed hydroxyapatite coatings" in Journal of Alloys and Compounds, 687 (2016):421-430, https://doi.org/10.1016/j.jallcom.2016.06.163 . .