Investigation of nanostructured Ca0.9Er0.1MnO3 obtained by sucrose nitrate procedure
Authors
Vlašković, TijanaLaban, Bojana
Milošević, Maja
Čebela, Maria
Dodevski, Vladimir
Rosić, Milena
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Nano-crystalline Ca0.9Er0.1MnO3 oxide with a perovskite structure was synthesized by the sucrose nitrate procedure (SNP), with the help of sucrose, which plays the role of fuel and complexant. Other chemicals used are calcium nitrate tetrahydrate Ca(NO3)2×4H2O, manganese nitrate hydrate Mn(NO3)2×H2O, erbium nitrate pentahydrate Er(NO3)3×5H2O. Metal nitrates and sucrose were mixed in stoichiometric ratios, in order to obtain a perovskite with a crystalline structure. The resulting Ca0.9Er0.1MnO3 is calcined for 15 minutes in the temperature range from 800°C to 1000°C. Diffraction thermal analysis (DTA), X-ray diffraction analysis (XRD), Fourier transform infrared spectroscopy (FTIR), scanning electron microscopy (SEM) and inductively coupled plasma ICP were used to characterize the obtained powder.
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Advanced Ceramics and Application :11th Serbian Ceramic Society Conference : program and the book of abstracts; September 18-20, 2023; Belgrade, 2023, 74-Publisher:
- Belgrade : Serbian Ceramic Society
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VinčaTY - CONF AU - Vlašković, Tijana AU - Laban, Bojana AU - Milošević, Maja AU - Čebela, Maria AU - Dodevski, Vladimir AU - Rosić, Milena PY - 2023 UR - https://vinar.vin.bg.ac.rs/handle/123456789/11648 AB - Nano-crystalline Ca0.9Er0.1MnO3 oxide with a perovskite structure was synthesized by the sucrose nitrate procedure (SNP), with the help of sucrose, which plays the role of fuel and complexant. Other chemicals used are calcium nitrate tetrahydrate Ca(NO3)2×4H2O, manganese nitrate hydrate Mn(NO3)2×H2O, erbium nitrate pentahydrate Er(NO3)3×5H2O. Metal nitrates and sucrose were mixed in stoichiometric ratios, in order to obtain a perovskite with a crystalline structure. The resulting Ca0.9Er0.1MnO3 is calcined for 15 minutes in the temperature range from 800°C to 1000°C. Diffraction thermal analysis (DTA), X-ray diffraction analysis (XRD), Fourier transform infrared spectroscopy (FTIR), scanning electron microscopy (SEM) and inductively coupled plasma ICP were used to characterize the obtained powder. PB - Belgrade : Serbian Ceramic Society C3 - Advanced Ceramics and Application :11th Serbian Ceramic Society Conference : program and the book of abstracts; September 18-20, 2023; Belgrade T1 - Investigation of nanostructured Ca0.9Er0.1MnO3 obtained by sucrose nitrate procedure SP - 74 UR - https://hdl.handle.net/21.15107/rcub_vinar_11648 ER -
@conference{ author = "Vlašković, Tijana and Laban, Bojana and Milošević, Maja and Čebela, Maria and Dodevski, Vladimir and Rosić, Milena", year = "2023", abstract = "Nano-crystalline Ca0.9Er0.1MnO3 oxide with a perovskite structure was synthesized by the sucrose nitrate procedure (SNP), with the help of sucrose, which plays the role of fuel and complexant. Other chemicals used are calcium nitrate tetrahydrate Ca(NO3)2×4H2O, manganese nitrate hydrate Mn(NO3)2×H2O, erbium nitrate pentahydrate Er(NO3)3×5H2O. Metal nitrates and sucrose were mixed in stoichiometric ratios, in order to obtain a perovskite with a crystalline structure. The resulting Ca0.9Er0.1MnO3 is calcined for 15 minutes in the temperature range from 800°C to 1000°C. Diffraction thermal analysis (DTA), X-ray diffraction analysis (XRD), Fourier transform infrared spectroscopy (FTIR), scanning electron microscopy (SEM) and inductively coupled plasma ICP were used to characterize the obtained powder.", publisher = "Belgrade : Serbian Ceramic Society", journal = "Advanced Ceramics and Application :11th Serbian Ceramic Society Conference : program and the book of abstracts; September 18-20, 2023; Belgrade", title = "Investigation of nanostructured Ca0.9Er0.1MnO3 obtained by sucrose nitrate procedure", pages = "74", url = "https://hdl.handle.net/21.15107/rcub_vinar_11648" }
Vlašković, T., Laban, B., Milošević, M., Čebela, M., Dodevski, V.,& Rosić, M.. (2023). Investigation of nanostructured Ca0.9Er0.1MnO3 obtained by sucrose nitrate procedure. in Advanced Ceramics and Application :11th Serbian Ceramic Society Conference : program and the book of abstracts; September 18-20, 2023; Belgrade Belgrade : Serbian Ceramic Society., 74. https://hdl.handle.net/21.15107/rcub_vinar_11648
Vlašković T, Laban B, Milošević M, Čebela M, Dodevski V, Rosić M. Investigation of nanostructured Ca0.9Er0.1MnO3 obtained by sucrose nitrate procedure. in Advanced Ceramics and Application :11th Serbian Ceramic Society Conference : program and the book of abstracts; September 18-20, 2023; Belgrade. 2023;:74. https://hdl.handle.net/21.15107/rcub_vinar_11648 .
Vlašković, Tijana, Laban, Bojana, Milošević, Maja, Čebela, Maria, Dodevski, Vladimir, Rosić, Milena, "Investigation of nanostructured Ca0.9Er0.1MnO3 obtained by sucrose nitrate procedure" in Advanced Ceramics and Application :11th Serbian Ceramic Society Conference : program and the book of abstracts; September 18-20, 2023; Belgrade (2023):74, https://hdl.handle.net/21.15107/rcub_vinar_11648 .