Characterization of hydrothermaly synthesized zirconia nanopowders
Конференцијски прилог (Објављена верзија)
,
Society of Physical Chemists of Serbia
Метаподаци
Приказ свих података о документуАпстракт
In this paper,a hydrothermal method for synthesis of zirconia nanopowders: pure and with incorporated Si4+ions is presented. Zirconyl chloride and tetraethyl orthosilicate were used as precursors. As prepared powders were annealed at 600 °C and their structural (XRD), morphological (TEM) and textural (BET method) properties were obtained.It has been shown that by using hydrothermal synthesis method pure monoclinic ZrO2highly crystalline powder can be obtainedwithcrystallites of about 25nm. Incorporation of Si4+ions induced stabilization of tetragonal crystalline phase at room temperature, decreasing particle sizes to about 3-6 nm and increasing specific surface area of nanopowders.
Извор:
Physical chemistry 2016 : 13th international conference on fundamental and applied aspects of physical chemistry, 2016, 553-556Издавач:
- Society of Physical Chemists of Serbia
Финансирање / пројекти:
- Утицај величине, облика и структуре наночестица на њихова својства и својства нанокомпозита (RS-MESTD-Basic Research (BR or ON)-172056)
Напомена:
- Physical chemistry 2016 : 13th international conference on fundamental and applied aspects of physical chemistry; Belgrade (Serbia); 26-30 September 2016
Колекције
Институција/група
VinčaTY - CONF AU - Carević, Milica AU - Abazović, Nadica AU - Savić, Tatjana D. AU - Novaković, Tatjana AU - Čomor, Mirjana PY - 2016 UR - https://vinar.vin.bg.ac.rs/handle/123456789/9217 AB - In this paper,a hydrothermal method for synthesis of zirconia nanopowders: pure and with incorporated Si4+ions is presented. Zirconyl chloride and tetraethyl orthosilicate were used as precursors. As prepared powders were annealed at 600 °C and their structural (XRD), morphological (TEM) and textural (BET method) properties were obtained.It has been shown that by using hydrothermal synthesis method pure monoclinic ZrO2highly crystalline powder can be obtainedwithcrystallites of about 25nm. Incorporation of Si4+ions induced stabilization of tetragonal crystalline phase at room temperature, decreasing particle sizes to about 3-6 nm and increasing specific surface area of nanopowders. PB - Society of Physical Chemists of Serbia C3 - Physical chemistry 2016 : 13th international conference on fundamental and applied aspects of physical chemistry T1 - Characterization of hydrothermaly synthesized zirconia nanopowders SP - 553 EP - 556 UR - https://hdl.handle.net/21.15107/rcub_vinar_9217 ER -
@conference{ author = "Carević, Milica and Abazović, Nadica and Savić, Tatjana D. and Novaković, Tatjana and Čomor, Mirjana", year = "2016", abstract = "In this paper,a hydrothermal method for synthesis of zirconia nanopowders: pure and with incorporated Si4+ions is presented. Zirconyl chloride and tetraethyl orthosilicate were used as precursors. As prepared powders were annealed at 600 °C and their structural (XRD), morphological (TEM) and textural (BET method) properties were obtained.It has been shown that by using hydrothermal synthesis method pure monoclinic ZrO2highly crystalline powder can be obtainedwithcrystallites of about 25nm. Incorporation of Si4+ions induced stabilization of tetragonal crystalline phase at room temperature, decreasing particle sizes to about 3-6 nm and increasing specific surface area of nanopowders.", publisher = "Society of Physical Chemists of Serbia", journal = "Physical chemistry 2016 : 13th international conference on fundamental and applied aspects of physical chemistry", title = "Characterization of hydrothermaly synthesized zirconia nanopowders", pages = "553-556", url = "https://hdl.handle.net/21.15107/rcub_vinar_9217" }
Carević, M., Abazović, N., Savić, T. D., Novaković, T.,& Čomor, M.. (2016). Characterization of hydrothermaly synthesized zirconia nanopowders. in Physical chemistry 2016 : 13th international conference on fundamental and applied aspects of physical chemistry Society of Physical Chemists of Serbia., 553-556. https://hdl.handle.net/21.15107/rcub_vinar_9217
Carević M, Abazović N, Savić TD, Novaković T, Čomor M. Characterization of hydrothermaly synthesized zirconia nanopowders. in Physical chemistry 2016 : 13th international conference on fundamental and applied aspects of physical chemistry. 2016;:553-556. https://hdl.handle.net/21.15107/rcub_vinar_9217 .
Carević, Milica, Abazović, Nadica, Savić, Tatjana D., Novaković, Tatjana, Čomor, Mirjana, "Characterization of hydrothermaly synthesized zirconia nanopowders" in Physical chemistry 2016 : 13th international conference on fundamental and applied aspects of physical chemistry (2016):553-556, https://hdl.handle.net/21.15107/rcub_vinar_9217 .