Colloidal chemistry-based synthesis of quantized CuInS2/Se-2 nanoparticles
2012
Authors
Abazović, NadicaJovanović, Dragana J.
Stoiljković, Milovan
Mitrić, Miodrag
Ahrenkiel, Scott Phillip
Nedeljković, Jovan
Čomor, Mirjana
Article
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Ternary chalcogenide nanoparticles, CuInS2 and CuInSe2, were synthesized in a high-temperature boiling non-polar organic solvent. X-Ray diffraction analysis revealed that both materials had a tetragonal (chalcopyrite) crystal structure. The morphology of the obtained materials was revealed by transmission electron microscopy. Agglomerated spherical CuInS2 nanoparticles with broad size distribution in the range from 2 to 20 nm were obtained. In the case of CuInSe2, isolated particles with a spherical or prismatic shape in the size range from 10 to 25 nm were obtained, as well as agglomerates consisting of much smaller particles with a diameter of about 2-5 nm. The particles with the smallest diameters of both materials exhibited quantum size effects.
Keywords:
I-III-VI2 semiconductors / quantization / X-ray diffraction / optical propertiesSource:
Journal of the Serbian Chemical Society, 2012, 77, 6, 789-797Funding / projects:
- Size-, shape- and structure- dependent properties of nanoparticles and nanocomposites (RS-MESTD-Basic Research (BR or ON)-172056)
DOI: 10.2298/JSC110420220A
ISSN: 0352-5139
WoS: 000306093300008
Scopus: 2-s2.0-84864561410
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VinčaTY - JOUR AU - Abazović, Nadica AU - Jovanović, Dragana J. AU - Stoiljković, Milovan AU - Mitrić, Miodrag AU - Ahrenkiel, Scott Phillip AU - Nedeljković, Jovan AU - Čomor, Mirjana PY - 2012 UR - https://vinar.vin.bg.ac.rs/handle/123456789/4938 AB - Ternary chalcogenide nanoparticles, CuInS2 and CuInSe2, were synthesized in a high-temperature boiling non-polar organic solvent. X-Ray diffraction analysis revealed that both materials had a tetragonal (chalcopyrite) crystal structure. The morphology of the obtained materials was revealed by transmission electron microscopy. Agglomerated spherical CuInS2 nanoparticles with broad size distribution in the range from 2 to 20 nm were obtained. In the case of CuInSe2, isolated particles with a spherical or prismatic shape in the size range from 10 to 25 nm were obtained, as well as agglomerates consisting of much smaller particles with a diameter of about 2-5 nm. The particles with the smallest diameters of both materials exhibited quantum size effects. T2 - Journal of the Serbian Chemical Society T1 - Colloidal chemistry-based synthesis of quantized CuInS2/Se-2 nanoparticles VL - 77 IS - 6 SP - 789 EP - 797 DO - 10.2298/JSC110420220A ER -
@article{ author = "Abazović, Nadica and Jovanović, Dragana J. and Stoiljković, Milovan and Mitrić, Miodrag and Ahrenkiel, Scott Phillip and Nedeljković, Jovan and Čomor, Mirjana", year = "2012", abstract = "Ternary chalcogenide nanoparticles, CuInS2 and CuInSe2, were synthesized in a high-temperature boiling non-polar organic solvent. X-Ray diffraction analysis revealed that both materials had a tetragonal (chalcopyrite) crystal structure. The morphology of the obtained materials was revealed by transmission electron microscopy. Agglomerated spherical CuInS2 nanoparticles with broad size distribution in the range from 2 to 20 nm were obtained. In the case of CuInSe2, isolated particles with a spherical or prismatic shape in the size range from 10 to 25 nm were obtained, as well as agglomerates consisting of much smaller particles with a diameter of about 2-5 nm. The particles with the smallest diameters of both materials exhibited quantum size effects.", journal = "Journal of the Serbian Chemical Society", title = "Colloidal chemistry-based synthesis of quantized CuInS2/Se-2 nanoparticles", volume = "77", number = "6", pages = "789-797", doi = "10.2298/JSC110420220A" }
Abazović, N., Jovanović, D. J., Stoiljković, M., Mitrić, M., Ahrenkiel, S. P., Nedeljković, J.,& Čomor, M.. (2012). Colloidal chemistry-based synthesis of quantized CuInS2/Se-2 nanoparticles. in Journal of the Serbian Chemical Society, 77(6), 789-797. https://doi.org/10.2298/JSC110420220A
Abazović N, Jovanović DJ, Stoiljković M, Mitrić M, Ahrenkiel SP, Nedeljković J, Čomor M. Colloidal chemistry-based synthesis of quantized CuInS2/Se-2 nanoparticles. in Journal of the Serbian Chemical Society. 2012;77(6):789-797. doi:10.2298/JSC110420220A .
Abazović, Nadica, Jovanović, Dragana J., Stoiljković, Milovan, Mitrić, Miodrag, Ahrenkiel, Scott Phillip, Nedeljković, Jovan, Čomor, Mirjana, "Colloidal chemistry-based synthesis of quantized CuInS2/Se-2 nanoparticles" in Journal of the Serbian Chemical Society, 77, no. 6 (2012):789-797, https://doi.org/10.2298/JSC110420220A . .