Optimization of Active Carbonaceous Material Obtained by Low Hydrothermal Carbonization of Plane Tree Seed with H3PO4
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2017
Authors
Dodevski, VladimirKaluđerović, Branka V.
Krstić, Sanja S.
Spasojević, Vuk D.
Trifunović, Snežana
Uskokovic, Petar
Marinković, Aleksandar D.
Stojmenović, Marija
Article (Published version)
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Activated carbons (ACs) were successfully prepared using plane tree seed (PTS) as a cheap and renewable raw material. The plane tree seeds were firstly treated combining magnetic (MM) and ultrasonic mixing (USM) during 0.5, 1 and 3 h in 1 M, 3 M and 6 M of H3PO4 solutions, and then activated at 260 degrees C during 20 h (low temperature hydrothermal carbonization-low HTC) in above mentioned solutions of the same molarity. The influence of combined mixing and activation processes on physical, structural and morphological properties, and their optimization was studied by X-ray powder diffraction (XRPD), Raman spectroscopy, nitrogen adsorption-desorption isotherms, fourier transform infrared spectroscopy (FTIR) and scanning electron microscopy (SEM) analysis.
Keywords:
Activated carbon / plane tree seed / hydrothermal carbonization / micro/mesoporositySource:
Journal of Nano Research, 2017, 48, 71-84Funding / projects:
- Functional, Functionalized and Advanced Nanomaterials (RS-MESTD-Integrated and Interdisciplinary Research (IIR or III)-45005)
- Serbian Ministry of Education, Science
DOI: 10.4028/www.scientific.net/JNanoR.48.71
ISSN: 1662-5250; 1661-9897
WoS: 000409162900008
Scopus: 2-s2.0-85026311813
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VinčaTY - JOUR AU - Dodevski, Vladimir AU - Kaluđerović, Branka V. AU - Krstić, Sanja S. AU - Spasojević, Vuk D. AU - Trifunović, Snežana AU - Uskokovic, Petar AU - Marinković, Aleksandar D. AU - Stojmenović, Marija PY - 2017 UR - https://vinar.vin.bg.ac.rs/handle/123456789/1714 AB - Activated carbons (ACs) were successfully prepared using plane tree seed (PTS) as a cheap and renewable raw material. The plane tree seeds were firstly treated combining magnetic (MM) and ultrasonic mixing (USM) during 0.5, 1 and 3 h in 1 M, 3 M and 6 M of H3PO4 solutions, and then activated at 260 degrees C during 20 h (low temperature hydrothermal carbonization-low HTC) in above mentioned solutions of the same molarity. The influence of combined mixing and activation processes on physical, structural and morphological properties, and their optimization was studied by X-ray powder diffraction (XRPD), Raman spectroscopy, nitrogen adsorption-desorption isotherms, fourier transform infrared spectroscopy (FTIR) and scanning electron microscopy (SEM) analysis. T2 - Journal of Nano Research T1 - Optimization of Active Carbonaceous Material Obtained by Low Hydrothermal Carbonization of Plane Tree Seed with H3PO4 VL - 48 SP - 71 EP - 84 DO - 10.4028/www.scientific.net/JNanoR.48.71 ER -
@article{ author = "Dodevski, Vladimir and Kaluđerović, Branka V. and Krstić, Sanja S. and Spasojević, Vuk D. and Trifunović, Snežana and Uskokovic, Petar and Marinković, Aleksandar D. and Stojmenović, Marija", year = "2017", abstract = "Activated carbons (ACs) were successfully prepared using plane tree seed (PTS) as a cheap and renewable raw material. The plane tree seeds were firstly treated combining magnetic (MM) and ultrasonic mixing (USM) during 0.5, 1 and 3 h in 1 M, 3 M and 6 M of H3PO4 solutions, and then activated at 260 degrees C during 20 h (low temperature hydrothermal carbonization-low HTC) in above mentioned solutions of the same molarity. The influence of combined mixing and activation processes on physical, structural and morphological properties, and their optimization was studied by X-ray powder diffraction (XRPD), Raman spectroscopy, nitrogen adsorption-desorption isotherms, fourier transform infrared spectroscopy (FTIR) and scanning electron microscopy (SEM) analysis.", journal = "Journal of Nano Research", title = "Optimization of Active Carbonaceous Material Obtained by Low Hydrothermal Carbonization of Plane Tree Seed with H3PO4", volume = "48", pages = "71-84", doi = "10.4028/www.scientific.net/JNanoR.48.71" }
Dodevski, V., Kaluđerović, B. V., Krstić, S. S., Spasojević, V. D., Trifunović, S., Uskokovic, P., Marinković, A. D.,& Stojmenović, M.. (2017). Optimization of Active Carbonaceous Material Obtained by Low Hydrothermal Carbonization of Plane Tree Seed with H3PO4. in Journal of Nano Research, 48, 71-84. https://doi.org/10.4028/www.scientific.net/JNanoR.48.71
Dodevski V, Kaluđerović BV, Krstić SS, Spasojević VD, Trifunović S, Uskokovic P, Marinković AD, Stojmenović M. Optimization of Active Carbonaceous Material Obtained by Low Hydrothermal Carbonization of Plane Tree Seed with H3PO4. in Journal of Nano Research. 2017;48:71-84. doi:10.4028/www.scientific.net/JNanoR.48.71 .
Dodevski, Vladimir, Kaluđerović, Branka V., Krstić, Sanja S., Spasojević, Vuk D., Trifunović, Snežana, Uskokovic, Petar, Marinković, Aleksandar D., Stojmenović, Marija, "Optimization of Active Carbonaceous Material Obtained by Low Hydrothermal Carbonization of Plane Tree Seed with H3PO4" in Journal of Nano Research, 48 (2017):71-84, https://doi.org/10.4028/www.scientific.net/JNanoR.48.71 . .