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dc.creatorAvramović, Ljiljana
dc.creatorPavlović, Miroslav M.
dc.creatorMaksimović, Vesna
dc.creatorVuković, Marina
dc.creatorStevanovic, Jasmina S.
dc.creatorBugarin, Mile
dc.creatorNikolic, Nebojsa D.
dc.date.accessioned2018-03-01T17:40:45Z
dc.date.available2018-03-01T17:40:45Z
dc.date.issued2017
dc.identifier.issn2075-4701 (print)
dc.identifier.urihttp://vinar.vin.bg.ac.rs/handle/123456789/1612
dc.description.abstractSilver powders chemically synthesized by reduction with hydrazine and those produced by electrolysis from the basic ( nitrate) and complex ( ammonium) electrolytes were examined by X-ray diffraction (XRD) and scanning electron microscopic (SEM) analysis of the produced particles. Morphologies of the obtained particles were very different at the macro level. The needle-like dendrites, as well as the mixture of irregular and regular crystals, were formed from the nitrate electrolyte, while the highly-branched pine-like dendrites with clearly noticeable spherical grains were formed from the ammonium electrolyte. The agglomerates of spherical grains were formed by reduction with hydrazine. In the particles obtained from the nitrate electrolyte, Ag crystallites were strongly oriented in the (111) plane. Although morphologies of Ag particles were very different at the macro level, the similarity at the micro level was observed between chemically-synthesized particles and those obtained by electrolysis from the ammonium electrolyte. Both types of particles were constructed from the spherical grains. This similarity at the micro level was accompanied by the similar XRD patterns, which were very close to the Ag standard with a random orientation of Ag crystallites. For the first time, morphologies of powder particles were correlated with their crystal structure.en
dc.relationinfo:eu-repo/grantAgreement/MESTD/Basic Research (BR or ON)/172046/RS//
dc.rightsopenAccessen
dc.sourceMetalsen
dc.subjectsilveren
dc.subjectpowder particlesen
dc.subjectchemical synthesisen
dc.subjectelectrolysisen
dc.subjectscanning electron microscope (SEM)en
dc.subjectX-ray diffraction (XRD) analysisen
dc.titleComparative Morphological and Crystallographic Analysis of Electrochemically- and Chemically-Produced Silver Powder Particlesen
dc.typearticleen
dcterms.abstractСтевановиц, Јасмина С.; Павловиц, Мирослав М.; Бугарин, Миле; Максимовић Весна; Николиц, Небојса Д.; Вуковиц, Марина; Aврамовиц, Љиљана;
dc.citation.volume7
dc.citation.issue5
dc.identifier.wos000404052600009
dc.identifier.doi10.3390/met7050160
dc.citation.otherArticle Number: 160
dc.identifier.scopus2-s2.0-85019144669
dc.identifier.fulltexthttp://vinar.vin.bg.ac.rs//bitstream/id/11967/1608.pdf


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