A comparative study of two different methods of sample preparation for polyolefins commonly used in medical devices
Апстракт
Polyolefins (POs) are currently the most widely used engineering plastics due to their
relatively low cost, durability, and ease of processing. A feature such as inertness makes
polyolefins suitable for applications such as food packaging and medical devices. For
the purpose of this study, polyethylene (PE) with good rigidity, hardness, impact
strength, environmental stress cracking resistance, and excellent processability, and
polypropylene (PP), with high fluidity and very good transparency, were selected
polyolefins [1,2]. Knowing that most of the polymer applications are strongly dependent
on the initial state of the products, i.e., their morphology, thermal properties, and
crystallinity, it is possible to obtain a great variety of morphologies and supermolecular
formations by varying different conditions in the preparation process, e.g. cooling
conditions during the crystallization process from the melt.
One of the aims of this work was to compare the results obtained f...or two different
methods of sample preparation, quenching, and slow cooling. Initial preparation was
performed for selected POs by rapid quenching in ice water and slow air cooling after
compression molding. Further, the prepared samples were characterized by SEM,
WAXD, FTIR, and mechanical measurements.
The obtained results indicated that PP is much more sensitive to the method of sample
preparation than PE, as well as that the initial preparation of samples plays a decisive
role in the final properties of materials for polymeric medical devices.
Извор:
8th Conference of Young Chemists of Serbia : Book of abstracts, 2022, 91-91Издавач:
- Belgrade : Serbian Chemical Society and Serbian Young Chemists’ Club
Финансирање / пројекти:
- Министарство науке, технолошког развоја и иновација Републике Србије, институционално финансирање - 200017 (Универзитет у Београду, Институт за нуклеарне науке Винча, Београд-Винча) (RS-MESTD-inst-2020-200017)
- IAEA Research [Contract No. 24728]
Напомена:
- 8th Conference of Young Chemists of Serbia; 29th October, Belgrade, Serbia
Колекције
Институција/група
VinčaTY - CONF AU - Jolić, Anđelka AU - Miličević, Dejan AU - Rogić Miladinović, Zorana AU - Suljovrujić, Edin PY - 2022 UR - https://vinar.vin.bg.ac.rs/handle/123456789/12407 AB - Polyolefins (POs) are currently the most widely used engineering plastics due to their relatively low cost, durability, and ease of processing. A feature such as inertness makes polyolefins suitable for applications such as food packaging and medical devices. For the purpose of this study, polyethylene (PE) with good rigidity, hardness, impact strength, environmental stress cracking resistance, and excellent processability, and polypropylene (PP), with high fluidity and very good transparency, were selected polyolefins [1,2]. Knowing that most of the polymer applications are strongly dependent on the initial state of the products, i.e., their morphology, thermal properties, and crystallinity, it is possible to obtain a great variety of morphologies and supermolecular formations by varying different conditions in the preparation process, e.g. cooling conditions during the crystallization process from the melt. One of the aims of this work was to compare the results obtained for two different methods of sample preparation, quenching, and slow cooling. Initial preparation was performed for selected POs by rapid quenching in ice water and slow air cooling after compression molding. Further, the prepared samples were characterized by SEM, WAXD, FTIR, and mechanical measurements. The obtained results indicated that PP is much more sensitive to the method of sample preparation than PE, as well as that the initial preparation of samples plays a decisive role in the final properties of materials for polymeric medical devices. PB - Belgrade : Serbian Chemical Society and Serbian Young Chemists’ Club C3 - 8th Conference of Young Chemists of Serbia : Book of abstracts T1 - A comparative study of two different methods of sample preparation for polyolefins commonly used in medical devices SP - 91 EP - 91 UR - https://hdl.handle.net/21.15107/rcub_vinar_12407 ER -
@conference{ author = "Jolić, Anđelka and Miličević, Dejan and Rogić Miladinović, Zorana and Suljovrujić, Edin", year = "2022", abstract = "Polyolefins (POs) are currently the most widely used engineering plastics due to their relatively low cost, durability, and ease of processing. A feature such as inertness makes polyolefins suitable for applications such as food packaging and medical devices. For the purpose of this study, polyethylene (PE) with good rigidity, hardness, impact strength, environmental stress cracking resistance, and excellent processability, and polypropylene (PP), with high fluidity and very good transparency, were selected polyolefins [1,2]. Knowing that most of the polymer applications are strongly dependent on the initial state of the products, i.e., their morphology, thermal properties, and crystallinity, it is possible to obtain a great variety of morphologies and supermolecular formations by varying different conditions in the preparation process, e.g. cooling conditions during the crystallization process from the melt. One of the aims of this work was to compare the results obtained for two different methods of sample preparation, quenching, and slow cooling. Initial preparation was performed for selected POs by rapid quenching in ice water and slow air cooling after compression molding. Further, the prepared samples were characterized by SEM, WAXD, FTIR, and mechanical measurements. The obtained results indicated that PP is much more sensitive to the method of sample preparation than PE, as well as that the initial preparation of samples plays a decisive role in the final properties of materials for polymeric medical devices.", publisher = "Belgrade : Serbian Chemical Society and Serbian Young Chemists’ Club", journal = "8th Conference of Young Chemists of Serbia : Book of abstracts", title = "A comparative study of two different methods of sample preparation for polyolefins commonly used in medical devices", pages = "91-91", url = "https://hdl.handle.net/21.15107/rcub_vinar_12407" }
Jolić, A., Miličević, D., Rogić Miladinović, Z.,& Suljovrujić, E.. (2022). A comparative study of two different methods of sample preparation for polyolefins commonly used in medical devices. in 8th Conference of Young Chemists of Serbia : Book of abstracts Belgrade : Serbian Chemical Society and Serbian Young Chemists’ Club., 91-91. https://hdl.handle.net/21.15107/rcub_vinar_12407
Jolić A, Miličević D, Rogić Miladinović Z, Suljovrujić E. A comparative study of two different methods of sample preparation for polyolefins commonly used in medical devices. in 8th Conference of Young Chemists of Serbia : Book of abstracts. 2022;:91-91. https://hdl.handle.net/21.15107/rcub_vinar_12407 .
Jolić, Anđelka, Miličević, Dejan, Rogić Miladinović, Zorana, Suljovrujić, Edin, "A comparative study of two different methods of sample preparation for polyolefins commonly used in medical devices" in 8th Conference of Young Chemists of Serbia : Book of abstracts (2022):91-91, https://hdl.handle.net/21.15107/rcub_vinar_12407 .