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dc.creatorMatović, Branko
dc.creatorPrekajski, Marija D.
dc.creatorPantić, Jelena R.
dc.creatorBraeuniger, Thomas
dc.creatorRosić, Milena
dc.creatorZagorac, Dejan
dc.creatorMilivojević, Dušan
dc.date.accessioned2018-03-01T17:07:09Z
dc.date.available2018-03-01T17:07:09Z
dc.date.issued2016
dc.identifier.issn0955-2219 (print)
dc.identifier.issn1873-619X (electronic)
dc.identifier.urihttp://vinar.vin.bg.ac.rs/handle/123456789/1227
dc.description.abstractMayenite (C12A7) powders have been synthesized by self-combustion method (glycine/nitrate procedure - GNP and a newly suggested modified glycine/nitrate procedure - MGNP). The MGNP is derived from the GNP by substituting a portion of Al-nitrate with the less expensive Al-acetate. The effect of synthesis conditions of both procedures on the phase evolution was studied. Mayenite samples, obtained by using GNP and MGNP, followed by thermal treatment in air, were analyzed by using XRD method. The obtained results showed that crystallization started at 900 degrees C for the GNP and at 750 degrees C for the MGNP while below these temperatures samples are amorphous. Also, only observed phase was mayenite for MGNP, while a secondary phase is present in samples synthesized by using GNP. Scanning electron microscopy (SEM), electron paramagnetic resonance (EPR) and nuclear magnetic resonance spectroscopy (NMR) were used to characterize the pure mayenite phase at room temperature. Sintering behavior was studied by dilatometry. A relative density of 94% is obtained at 1300 degrees C. (C) 2016 Elsevier Ltd. All rights reserved.en
dc.relationMinistry of Education, Science and Technological Development of Serbia
dc.rightsrestrictedAccessen
dc.sourceJournal of the European Ceramic Societyen
dc.subjectMayeniteen
dc.subjectSynthesisen
dc.subjectSinteringen
dc.subjectX-ray methodsen
dc.subjectMicrostructureen
dc.titleSynthesis and densification of single-phase mayenite (C12A7)en
dc.typearticleen
dcterms.abstractПантиц, Јелена; Матовић Бранко; Загорац, Дејан; Прекајски-Ђорђевић Марија; Браеунигер, Тхомас; Росић Милена; Миливојевић Душан;
dc.citation.volume36
dc.citation.issue16
dc.citation.spage4237
dc.citation.epage4241
dc.identifier.wos000382595600048
dc.identifier.doi10.1016/j.jeurceramsoc.2016.06.014
dc.citation.rankM21a
dc.identifier.scopus2-s2.0-84977472231


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