Synthesis of Monetite (CaHPO4) by mechanochemical treatment of Brushite (CaHPO4∙2H2O)
Authors
Mirković, MiljanaDošen, Anja
Babić, Biljana
Čebela, Maria
Vulić, Predrag
Rosić, Aleksandra
Matović, Branko
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Synthesis of monetite (CaHPO4) by means of mechanochemical treatment of brushite (CaHPO4∙2H2O) was studied. Start sample (Brushite) was obtained by precipitation method at room temperature. Particle size of brushite was reduced using vibromilling. The powders were analyzed by X-ray powder diffraction (XRPD). Microstructure and morphology was determined by means of scanning electron microscopy (SEM). Brunauer-Emmett-Teller (BET) method was used for examining specific surface area of obtained powders. It was found that five minutes of milling induces brushite-monetite phase transformation. This type of synthesis is cost-effective compared to the other used methods for synthesis of monetite.
Source:
11th Conference for Young Scientists in Ceramics (SM-2015, and ESR Workshop, COST MP1208) : programme and the book of abstracts, 2015, 71-Publisher:
- Novi Sad : University of Novi Sad, Faculty of Technology
Note:
- 11th Conference for Young Scientists in Ceramics (SM-2015, and ESR Workshop, COST MP1208) : programme and the book of abstracts; October 21-24, 2018; Novi Sad
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VinčaTY - CONF AU - Mirković, Miljana AU - Došen, Anja AU - Babić, Biljana AU - Čebela, Maria AU - Vulić, Predrag AU - Rosić, Aleksandra AU - Matović, Branko PY - 2015 UR - https://vinar.vin.bg.ac.rs/handle/123456789/11542 AB - Synthesis of monetite (CaHPO4) by means of mechanochemical treatment of brushite (CaHPO4∙2H2O) was studied. Start sample (Brushite) was obtained by precipitation method at room temperature. Particle size of brushite was reduced using vibromilling. The powders were analyzed by X-ray powder diffraction (XRPD). Microstructure and morphology was determined by means of scanning electron microscopy (SEM). Brunauer-Emmett-Teller (BET) method was used for examining specific surface area of obtained powders. It was found that five minutes of milling induces brushite-monetite phase transformation. This type of synthesis is cost-effective compared to the other used methods for synthesis of monetite. PB - Novi Sad : University of Novi Sad, Faculty of Technology C3 - 11th Conference for Young Scientists in Ceramics (SM-2015, and ESR Workshop, COST MP1208) : programme and the book of abstracts T1 - Synthesis of Monetite (CaHPO4) by mechanochemical treatment of Brushite (CaHPO4∙2H2O) SP - 71 UR - https://hdl.handle.net/21.15107/rcub_vinar_11542 ER -
@conference{ author = "Mirković, Miljana and Došen, Anja and Babić, Biljana and Čebela, Maria and Vulić, Predrag and Rosić, Aleksandra and Matović, Branko", year = "2015", abstract = "Synthesis of monetite (CaHPO4) by means of mechanochemical treatment of brushite (CaHPO4∙2H2O) was studied. Start sample (Brushite) was obtained by precipitation method at room temperature. Particle size of brushite was reduced using vibromilling. The powders were analyzed by X-ray powder diffraction (XRPD). Microstructure and morphology was determined by means of scanning electron microscopy (SEM). Brunauer-Emmett-Teller (BET) method was used for examining specific surface area of obtained powders. It was found that five minutes of milling induces brushite-monetite phase transformation. This type of synthesis is cost-effective compared to the other used methods for synthesis of monetite.", publisher = "Novi Sad : University of Novi Sad, Faculty of Technology", journal = "11th Conference for Young Scientists in Ceramics (SM-2015, and ESR Workshop, COST MP1208) : programme and the book of abstracts", title = "Synthesis of Monetite (CaHPO4) by mechanochemical treatment of Brushite (CaHPO4∙2H2O)", pages = "71", url = "https://hdl.handle.net/21.15107/rcub_vinar_11542" }
Mirković, M., Došen, A., Babić, B., Čebela, M., Vulić, P., Rosić, A.,& Matović, B.. (2015). Synthesis of Monetite (CaHPO4) by mechanochemical treatment of Brushite (CaHPO4∙2H2O). in 11th Conference for Young Scientists in Ceramics (SM-2015, and ESR Workshop, COST MP1208) : programme and the book of abstracts Novi Sad : University of Novi Sad, Faculty of Technology., 71. https://hdl.handle.net/21.15107/rcub_vinar_11542
Mirković M, Došen A, Babić B, Čebela M, Vulić P, Rosić A, Matović B. Synthesis of Monetite (CaHPO4) by mechanochemical treatment of Brushite (CaHPO4∙2H2O). in 11th Conference for Young Scientists in Ceramics (SM-2015, and ESR Workshop, COST MP1208) : programme and the book of abstracts. 2015;:71. https://hdl.handle.net/21.15107/rcub_vinar_11542 .
Mirković, Miljana, Došen, Anja, Babić, Biljana, Čebela, Maria, Vulić, Predrag, Rosić, Aleksandra, Matović, Branko, "Synthesis of Monetite (CaHPO4) by mechanochemical treatment of Brushite (CaHPO4∙2H2O)" in 11th Conference for Young Scientists in Ceramics (SM-2015, and ESR Workshop, COST MP1208) : programme and the book of abstracts (2015):71, https://hdl.handle.net/21.15107/rcub_vinar_11542 .