Synthesis and crystal structure of Ca0.9Er0.1MnO3
Апстракт
Ca0.9Er0.1MnO3 nanopowders with perovskite type crystal structure were synthesized by sucrose-nitrate procedure (SNP). SNP is a combustion method in which sucrose C12H22O11 was used as fuel, while calcium nitrate tetrahydrate Ca(NO3)2×4H2O, manganese(II) nitrate hydrate Mn(NO3)2×H2O, erbium(III) nitrate pentahydrate Er(NO3)3×5H2O were used as oxidants. Obtained powder Ca0,9Er0,1MnO3 were calcinated at a temperature between 800–1000 °C. Powder properties have been studied, such as crystallite and particle size, lattice parameters, structural changes, and specific surface area. X-ray diffraction (XRD), Field emission scanning electron microscopy (FESEM), and Brunauer-Emmet-Teller (BET) method were used to characterize the synthesized samples at room temperature. Also, high temperature treatment (up to 1000 °C) was used to follow the stability of solid solutions and the growth of crystallites.
Извор:
Programme and the Book of Abstracts / 7th Conference of The Serbian Society for Ceramic Materials, 7CSCS-2023, June 14-16, 2023 Belgrade, 2023, 82-82Издавач:
- Belgrade : University of Belgrade, Institute for Multidisciplinary Research
Колекције
Институција/група
VinčaTY - CONF AU - Vlašković, Tijana B. AU - Laban, Bojana AU - Čebela, Maria AU - Dodevski, Vladimir AU - Rosić, Milena PY - 2023 UR - https://vinar.vin.bg.ac.rs/handle/123456789/11489 AB - Ca0.9Er0.1MnO3 nanopowders with perovskite type crystal structure were synthesized by sucrose-nitrate procedure (SNP). SNP is a combustion method in which sucrose C12H22O11 was used as fuel, while calcium nitrate tetrahydrate Ca(NO3)2×4H2O, manganese(II) nitrate hydrate Mn(NO3)2×H2O, erbium(III) nitrate pentahydrate Er(NO3)3×5H2O were used as oxidants. Obtained powder Ca0,9Er0,1MnO3 were calcinated at a temperature between 800–1000 °C. Powder properties have been studied, such as crystallite and particle size, lattice parameters, structural changes, and specific surface area. X-ray diffraction (XRD), Field emission scanning electron microscopy (FESEM), and Brunauer-Emmet-Teller (BET) method were used to characterize the synthesized samples at room temperature. Also, high temperature treatment (up to 1000 °C) was used to follow the stability of solid solutions and the growth of crystallites. PB - Belgrade : University of Belgrade, Institute for Multidisciplinary Research C3 - Programme and the Book of Abstracts / 7th Conference of The Serbian Society for Ceramic Materials, 7CSCS-2023, June 14-16, 2023 Belgrade T1 - Synthesis and crystal structure of Ca0.9Er0.1MnO3 SP - 82 EP - 82 UR - https://hdl.handle.net/21.15107/rcub_vinar_11489 ER -
@conference{ author = "Vlašković, Tijana B. and Laban, Bojana and Čebela, Maria and Dodevski, Vladimir and Rosić, Milena", year = "2023", abstract = "Ca0.9Er0.1MnO3 nanopowders with perovskite type crystal structure were synthesized by sucrose-nitrate procedure (SNP). SNP is a combustion method in which sucrose C12H22O11 was used as fuel, while calcium nitrate tetrahydrate Ca(NO3)2×4H2O, manganese(II) nitrate hydrate Mn(NO3)2×H2O, erbium(III) nitrate pentahydrate Er(NO3)3×5H2O were used as oxidants. Obtained powder Ca0,9Er0,1MnO3 were calcinated at a temperature between 800–1000 °C. Powder properties have been studied, such as crystallite and particle size, lattice parameters, structural changes, and specific surface area. X-ray diffraction (XRD), Field emission scanning electron microscopy (FESEM), and Brunauer-Emmet-Teller (BET) method were used to characterize the synthesized samples at room temperature. Also, high temperature treatment (up to 1000 °C) was used to follow the stability of solid solutions and the growth of crystallites.", publisher = "Belgrade : University of Belgrade, Institute for Multidisciplinary Research", journal = "Programme and the Book of Abstracts / 7th Conference of The Serbian Society for Ceramic Materials, 7CSCS-2023, June 14-16, 2023 Belgrade", title = "Synthesis and crystal structure of Ca0.9Er0.1MnO3", pages = "82-82", url = "https://hdl.handle.net/21.15107/rcub_vinar_11489" }
Vlašković, T. B., Laban, B., Čebela, M., Dodevski, V.,& Rosić, M.. (2023). Synthesis and crystal structure of Ca0.9Er0.1MnO3. in Programme and the Book of Abstracts / 7th Conference of The Serbian Society for Ceramic Materials, 7CSCS-2023, June 14-16, 2023 Belgrade Belgrade : University of Belgrade, Institute for Multidisciplinary Research., 82-82. https://hdl.handle.net/21.15107/rcub_vinar_11489
Vlašković TB, Laban B, Čebela M, Dodevski V, Rosić M. Synthesis and crystal structure of Ca0.9Er0.1MnO3. in Programme and the Book of Abstracts / 7th Conference of The Serbian Society for Ceramic Materials, 7CSCS-2023, June 14-16, 2023 Belgrade. 2023;:82-82. https://hdl.handle.net/21.15107/rcub_vinar_11489 .
Vlašković, Tijana B., Laban, Bojana, Čebela, Maria, Dodevski, Vladimir, Rosić, Milena, "Synthesis and crystal structure of Ca0.9Er0.1MnO3" in Programme and the Book of Abstracts / 7th Conference of The Serbian Society for Ceramic Materials, 7CSCS-2023, June 14-16, 2023 Belgrade (2023):82-82, https://hdl.handle.net/21.15107/rcub_vinar_11489 .