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4-[(Dimethylamino)methylene]-2-ferrocenyl-5-oxo-4, 5-dihydrofuran-3-carboxaldehyde: Synthesis, spectral characterization and single crystal X-ray analysis
dc.creator | Ratković, Zoran R. | |
dc.creator | Muškinja, Jovana | |
dc.creator | Novaković, Slađana B. | |
dc.creator | Bogdanović, Goran A. | |
dc.creator | Micskei, Karoly | |
dc.creator | Vukićević, Rastko D. | |
dc.date.accessioned | 2018-03-01T15:22:22Z | |
dc.date.available | 2018-03-01T15:22:22Z | |
dc.date.issued | 2014 | |
dc.identifier.issn | 0277-5387 | |
dc.identifier.uri | https://vinar.vin.bg.ac.rs/handle/123456789/101 | |
dc.description.abstract | The title compound 4-[(dimethylamino)methylene]-2-ferrocenyl-5-oxo-4,5-dihydrofuran-3-carboxaldehyde was synthesized by reacting 3-ferrocenoylpropionic acid with Vilsmeier reagent. This result is rather unexpected, since 3-aroylpropanoic acids under these conditions usually give the corresponding 2-aryl-4-chloro-3-formylfurans. 3-Ferrocenoylpropanoic acid is not the only 3-aroylpropanoic acid that exhibit an unusual behavior under the same conditions: 3-thenoylpropanoic acid gave 4-[(dimethylamino)-methylene]-2-(2-thienyl)-5-oxo-4,5-dihydrofuran-3-carboxaldehyde and 4-[(dimethylamino) methylene]-2-(2-thienyl-5-formyl)-5-oxo-4,5-dihydrofuran-3-carboxaldehyde, whereas 3-(4-methoxybenzoyl)propanoic acid yielded 4-[(dimethylamino)methylene]-2-(4-methoxyphenyl)-5-oxo-4,5-dihydrofuran-3-carboxaldehyde and 2-(4-methoxyphenyl)-5-chloro-furan-3,4-dicarboxaldehyde. Single crystal X-ray analysis was successfully performed for 4-[(dimethylamino)methylene]-2-ferrocenyl-5-oxo-4,5-dihydrofuran-3-carboxaldehyde and 4-[(dimethylamino)methylene]-2-(2-thienyl)-5-oxo-4, 5-dihydrofuran-3-carboxaldehyde and their structures were compared. (C) 2014 Elsevier Ltd. All rights reserved. | en |
dc.relation | info:eu-repo/grantAgreement/MESTD/Basic Research (BR or ON)/172034/RS// | |
dc.relation | info:eu-repo/grantAgreement/MESTD/Basic Research (BR or ON)/172014/RS// | |
dc.rights | restrictedAccess | en |
dc.source | Polyhedron | en |
dc.subject | 3-Aroylpropanoic acids | en |
dc.subject | 3-Ferocenoylpropanoic acid | en |
dc.subject | Vilsmeier reagent | en |
dc.subject | Furan derivatives | en |
dc.subject | Crystal structure | en |
dc.title | 4-[(Dimethylamino)methylene]-2-ferrocenyl-5-oxo-4, 5-dihydrofuran-3-carboxaldehyde: Synthesis, spectral characterization and single crystal X-ray analysis | en |
dc.type | article | en |
dcterms.abstract | Новаковић Слађана; Мускиња, Јована; Ратковиц, Зоран; Вукицевиц, Растко Д.; Мицскеи, Каролy; Богдановић Горан; | |
dc.citation.volume | 80 | |
dc.citation.issue | SI | |
dc.citation.spage | 193 | |
dc.citation.epage | 197 | |
dc.identifier.wos | 000341348300025 | |
dc.identifier.doi | 10.1016/j.poly.2014.03.038 | |
dc.citation.other | Special Issue: SI | |
dc.citation.rank | M22 | |
dc.type.version | publishedVersion | |
dc.identifier.scopus | 2-s2.0-84905442719 |
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